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An In Situ , multi-electrode electrochemical method to assess the open circuit potential corrosion of Cr in unpurified molten FLiNaK
An in situ electrochemical method to investigate the time-dependent spontaneous corrosion of pure Cr in an unpurified LiF-NaF-KF eutectic salt at 600 °C was developed. A multi-electrode electrochemical cell and a dual-electrode method were utilized to detect Cr(II) and Cr(III) ions on a platinum working electrode using cyclic voltammetry as a function of exposure time and compensating for the distance from the Cr electrode. XRD was performed to characterize the crystalline composition of the exposed FLiNaK and the salt films formed on the working electrodes. The fate of all electro-oxidized Cr must be accounted for to quantify corrosion rates. The concentrations of Cr(II) and Cr(III) species obtained were compared with the gravimetric mass change and ICP-OES analysis of the residual salt. Finally, outcomes, difficulties, and limitations are discussed.
WO 3 /CuWO 4 Ratio Controls Open-Circuit Photovoltage and Photocurrent in Type II Heterojunction Solar Fuel Photoelectrodes
WO 3 /CuWO 4 photoelectrodes for the oxygen evolution reaction benefit from a type II heterojunction for charge separation. However, the impact of the WO 3 /CuWO 4 ratio on the photocurrent and the photovoltage is not clear. To probe the effect of composition, Cu x W 1-x O y thin films with variable W:Cu ratio were prepared on FTO by reactive magnetron co-sputtering of W and Cu, followed by air annealing at 500ºC. EDS, XRD, Rietveld refinement, and Raman spectroscopy confirm the presence of crystalline WO 3 and CuWO 4 in the W rich films and increasing amounts of amorphous copper oxides in the Cu rich films. Bandgaps were determined by optical absorption spectroscopy, surface photovoltage spectroscopy (SPS), and photoaction spectra and are found to decrease from 2.7 eV to 1.2 eV with increasing copper oxide content. SPS reveals n-type semiconductor photoanode behavior for WO 3 /CuWO 4 samples and p-type photocathode behavior for CuO x rich films. Photoelectrochemical experiments confirm stable water oxidation with Faraday efficiency near unity for all W rich films and photocurrents that are increasing with CuWO 4 content. Optimal performance is seen for WO 3 /CuWO 4 mixed phases containing 47-75 mass% CuWO 4 . These compositions maximize charge separation at the type II heterojunction interface between the two materials. Additionally, according to incident photon to current efficiency (IPCE) data, the WO 3 improves photon conversion below 350 nm, while CuWO 4 improves conversion at 450-525 nm. Overall, this work shows for the first time how the WO 3 /CuWO 4 ratio controls the photovoltage and the photocurrent in type II heterojunction solar fuel photoelectrodes, and how copper oxides in the copper rich films severely degrade the performance. Furthermore, these results are useful in the context of bulk-heterojunction electrodes for the conversion of solar energy into fuels.
Urbach Energy and Open-Circuit Voltage Deficit for Mixed Anion–Cation Perovskite Solar Cells
Not provided.
Origin of Low Open-Circuit Voltage in Surfactant-Stabilized Organic-Nanoparticle-Based Solar Cells
Not provided.
Surface photovoltage predicts open circuit voltage in GaP/PEDOT:PSS and GaP/CuSCN heterojunction solar cells
Surface photovoltage spectroscopy measures the contribution of solution-processed hole transport layers to the photovoltage of GaP solar cells.
Open Circuit Switch Fault Management Method of a Multi-Phase Synchronous Buck Converter for EV Charging Application
Multi-phase synchronous buck converter (MSBC) is becoming popular for the electric vehicle (EV) charging application because of its higher efficiency, smaller passive component sizes, bidirectional power flow, and output current ripple reduction through interleaving. This converter also provides higher reliability than the traditional single phase converter since its modular structure enables fault tolerant operation. Fault management in the converter requires the detection of switch fault, shut down of the faulty phase, and reconfiguration of the PWM signals for the healthy phases to avoid circulating current and high output current ripple. In addition, it is desirable that the fault management method can be implemented using the micro-controller unit (MCU) or digital signal processor (DSP), which are widely used to control power converters. This paper presents a fault management method for detecting switch faults and reconfiguring healthy phases using a DSP. The method is validated through simulations and experiments using a commercial off-the-shelf power stack.
Stress corrosion cracking of titanium alloys - Potential transients at open circuit during SCC and pitting corrosion, and chloride absorption during formation of TiO sub 2 Quarterly progress report, Jul. 1 - 30 Sep. 1967
Stress corrosion cracking of titanium alloys and chloride absorption during formation of titanium oxide
Evaluation program for secondary spacecraft cells. Evaluation of storage methods, open circuit versus continuous trickle charge, Sonotone 3.5 ampere-hour sealed nickel- cadmium secondary spacecraft cells
Storage methods for secondary nickel cadmium spacecraft batteries
Evaluation program for secondary spacecraft cells. Evaluation of storage methods, open circuit versus continuous trickle charge, sonotone 3.5 ampere-hour sealed nickel- cadmium secondary spacecraft cells
Performance tests of nickel cadmium batteries for evaluation of storage methods
Development of an open circuit cryogenic life support system for use in neutral buoyancy space simulation
Cryogenic underwater life support system for supplying breathing gas to buoyancy test subjects in submerged vehicle
Two-dimensional wake characteristics of inlet vanes for open-circuit wind tunnels
This paper summarizes the near-field flow characteristics measured downstream of a half-scale two-dimensional wind-tunnel model of the inlet vanes designed for the National Full-Scale Facilities Complex at NASA Ames Research Center. Variations on this baseline were tested to determine how the downstream flow field is affected. Evaluations of the various configurations were made by the use of hot-wire surveys across the flow-field. These traverses yielded the properties of total pressure, boundary layers, and turbulence in the wake of the vanes. It was found that large variations in the flow field characteristics downstream of the vanes are achieved by the use of various arrangements of splitter vanes, vortex generators, screens, tail extensions, and honeycomb. Separation on the boat-tails of the vanes can be controlled and turbulence reduced by suitable combinations of screens or honeycomb or both. The penalties associated with each modification in terms of increased pressure loss are also presented.
Effect of solar-cell junction geometry on open-circuit voltage
Simple analytical models have been found that adequately describe the voltage behavior of both the stripe junction and dot junction grating cells as a function of junction area. While the voltage in the former case is found to be insensitive to junction area reduction, significant voltage increases are shown to be possible for the dot junction cell. With regard to cells in which the junction area has been increased in a quest for better performance, it was found that (1) texturation does not affect the average saturation current density J0, indicating that the texturation process is equivalent to a simple extension of junction area by a factor of square root of 3 and (2) the vertical junction cell geometry produces a sizable decrease in J0 that, unfortunately, is more than offset by the effects of attendant areal increases.
An open-circuit and a short-circuit in the Pacific Ocean subtropical-tropical exchange
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