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DOE OSTI2023

Photonically active bowtie nanoassemblies with chirality continuum

Chirality is a geometrical property described by continuous mathematical functions. However, in chemical disciplines, chirality is often treated as a binary left or right characteristic of molecules rather than a continuity of chiral shapes. Although they are theoretically possible, a family of stable chemical structures with similar shapes and progressively tuneable chirality is yet unknown. Here we show that nanostructured microparticles with an anisotropic bowtie shape display chirality continuum and can be made with widely tuneable twist angle, pitch, width, thickness and length. The self-limited assembly of the bowties enables high synthetic reproducibility, size monodispersity and computational predictability of their geometries for different assembly conditions. The bowtie nanoassemblies show several strong circular dichroism peaks originating from absorptive and scattering phenomena. Unlike classical chiral molecules, these particles show a continuum of chirality measures that correlate exponentially with the spectral positions of the circular dichroism peaks. Finally, Bowtie particles with variable polarization rotation were used to print photonically active metasurfaces with spectrally tuneable positive or negative polarization signatures for light detection and ranging (LIDAR) devices.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS2011

On Interplanetary Shocks Driven by Coronal Mass Ejections

Traveling interplanetary (IP) shocks were first detected in the early 1960s, but their solar origin has been controversial. Early research focused on solar flares as the source of the shocks, but when CMEs were discovered, it became clear that fast CMEs are the shock drivers. Type radio II bursts are excellent signatures of shocks near the Sun (Type II radio bursts were known long before the detection of shocks and CMEs). The excellent correspondence between type II bursts and solar energetic particle (SEP) events made it clear that the same shock accelerates ions and electrons. Shocks near the Sun are also seen occasionally in white-light coronagraphic images. In the solar wind, shocks are observed as discontinuities in plasma parameters such as density and speed. Energetic storm particle events and sudden commencement of geomagnetic storm are also indicators of shocks arriving at Earth. After an overview on these shock signatures, I will summarize the results of a recent investigation of a large number of IP shocks. The study revealed that about 35% of IP shocks do not produce type II bursts (radio quiet - RQ) or SEPs. Comparing the RQ shocks with the radio loud (RL) ones revealed some interesting results: (1) There is no evidence for blast wave shocks. (2) A small fraction (20%) of RQ shocks is associated with ion enhancements at the shock when the shock passes the spacecraft. (3) The primary difference between the RQ and RL shocks can be traced to the different kinematic properties of the associated CMEs. On the other hand the shock properties measured at 1 AU are not too different for the RQ and RL cases. This can be attributed to the interaction with the IP medium, which seems to erase the difference between the shocks.

Gopalswarmy, Nat↗

DOE OSTI2020

In situ liquid SIMS analysis of uranium oxide

Trace analysis of nuclear materials in solid particles collected in the environment or particles in liquid slurry generated in nuclear material manufacturing processes can pinpoint elemental, organic, and isotopic signatures of nuclear fuel cycle activities and processes. Such information can support nuclear safeguards programs by increasing our ability to detect undeclared nuclear materials, routine activities for safeguarding at declared facilities, and illicit activities. However, trace radioactive material analysis in liquids and slurries is challenging using bulk approaches. For example, one drawback of sensitive analysis such as inductively coupled plasma mass spectrometry (ICP-MS) is that sample is consumed or destroyed as a result of the technical approach. We developed a vacuum compatible microfluidic interface to enable surface analysis of liquids and liquid-solid interactions using time-of-flight secondary ion mass spectrometry (ToF-SIMS). In this work, we illustrate initial results of liquid standards containing uranium using in situ liquid SIMS. Specifically a series of diluted uranium standards used for ICPMS analysis were studied and the limit of detection was estimated. Since the liquid SIMS analysis is almost nondestructive, the same sample can be analyzed by other more destructive approaches afterwards or saved for future references. Consequently, multimodal analysis is possible. Our results demonstrate that in situ liquid SIMS can be used as a new approach to analyze radioactive materials in liquid and slurry forms of relevance to the IAEA safeguards missions.

In situ liquid ToF-SIMS, uranium, limit of detecti↗

DOE OSTI2021

Prospects for measuring dark matter microphysics with observations of dwarf spheroidal galaxies

Dark matter annihilation in dwarf spheroidal (dSph) galaxies near the Milky Way has the potential to produce a detectable signature in gamma-rays. The amplitude of this signal depends on the dark matter density in a dSph, the dark matter particle mass, the number of photons produced in an annihilation, and the possibly velocity-dependent dark matter annihilation cross section. We argue that if the amplitude of the annihilation signal from multiple dSphs can be measured, it is possible to determine the velocity-dependence of the annihilation cross section. However, we show that doing so will require improved constraints on the dSph density profiles, including control of possible sources of systematic uncertainty. Making reasonable assumptions about future improvements, we make forecasts for the ability of current and future experiments — including Fermi, CTA and AMEGO — to constrain the dark matter annihilation velocity dependence.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

NASA NTRS1993

An alternative representation of the ice canopy for calculating microwave brightness temperatures over a thunderstorm

Passive microwave brightness temperatures (TBs) at 92 and 183 GHz from an aircraft thunderstorm overflight are compared with values calculated from radar-derived hydrometeor profiles and a modified proximity sounding. Two methods for modeling particles in the ice canopy are contrasted. The first is a 'traditional' approach employing Marshall-Palmer ice spheres. The second, or 'alternative', method partitions 20 percent of the ice water content into a Marshall-Palmer component for graupel and hail, and 80 percent into a modified gamma spherical particle size distribution function representing ice crystals. Results from the alternative approach are superior to those from the traditional method in the anvil and mature convective core. In the decaying convective region, the traditional approach yields better agreement with observed magnitudes. Neither method, however, matches the geometry of the observed TB depression associated with the decaying convective core. This is likely due to the presence of graupel, which is not detected as a special signature in radar reflectivity, but does diminish TBs through scattering. Brightness temperatures at the relatively high microwave frequencies considered are shown to be very sensitive to the ice-particle size distribution.

Muller, Bradley M.↗

DOE OSTI2022

Report of the Topical Group on Physics Beyond the Standard Model at Energy Frontier for Snowmass 2021

This is the Snowmass2021 Energy Frontier (EF) Beyond the Standard Model (BSM) report. It combines the EF topical group reports of EF08 (Model-specific explorations), EF09 (More general explorations), and EF10 (Dark Matter at Colliders). The report includes a general introduction to BSM motivations and the comparative prospects for proposed future experiments for a broad range of potential BSM models and signatures, including compositeness, SUSY, leptoquarks, more general new bosons and fermions, long-lived particles, dark matter, charged-lepton flavor violation, and anomaly detection.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2020

Freeze-in dark matter from secret neutrino interactions

We investigate a simplified freeze-in dark-matter model in which the dark matter only interacts with the standard-model neutrinos via a light scalar. The extremely small coupling for the freeze-in mechanism is naturally realized in several neutrino-portal scenarios with the secret neutrino interactions. We study possible evolution history of the hidden sector: the dark sector would undergo pure freeze-in production if the interactions between the dark-sector particles are negligible, while thermal equilibrium within the dark sector could occur if the reannihilation of the dark matter and the scalar mediator is rapid enough. We investigate the relic abundance in the freeze-in and dark freeze-out regimes, calculate evolution of the dark temperature, and study its phenomenological aspects on BBN and CMB constraints, the indirect-detection signature, as well as the potential to solve the small scale structure problem.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2024

Spectroscopy in Nanoscopic Cavities: Models and Recent Experiments

The ability of nanophotonic cavities to confine and store light to nanoscale dimensions has important implications for enhancing molecular, excitonic, phononic, and plasmonic optical responses. Spectroscopic signatures of processes that are ordinarily exceedingly weak such as pure absorption and Raman scattering have been brought to the single-particle limit of detection, while new emergent polaritonic states of optical matter have been realized through coupling material and photonic cavity degrees of freedom across a wide range of experimentally accessible interaction strengths. In this review, we discuss both optical and electron beam spectroscopies of cavity-coupled material systems in weak, strong, and ultrastrong coupling regimes, providing a theoretical basis for understanding the physics inherent to each while highlighting recent experimental advances and exciting future directions.

Chemistry↗

DOE OSTI2023

Collaborative Research Towards a tonne-scale bolometer-based neutrinoless double beta decay experiment (Final Report)

Cryogenic bolometers are an excellent technology for neutrinoless double beta decay searches owing to their very high energy resolution and potential for high radiopurity. The current most advanced large-scale experiment using these detectors is the Cryogenic Underground Observatory for Rare Events (CUORE). The largest source of background in CUORE is degraded alpha particles, emitted from shallow depths of the detector holders, which can deposit a thermal energy signature similar to neutrinoless double beta decay. To mitigate this background, the CUPID concept (CUORE Upgrade with Particle IDentification) proposes to use scintillating cryogenic detectors. Detecting both the scintillation light and the thermal signal allows discrimination between alpha particle events and beta/gamma events. We report on the design and execution of R&D tests to optimize the design of the single detector module, in particular the scintillation light collection efficiency at cryogenic temperatures.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

NASA NTRS1982

The acceleration and propagation of solar flare energetic particles

Observations and theories of particle acceleration in solar flares are reviewed. The most direct signatures of particle acceleration in flares are gamma rays, X-rays and radio emissions produced by the energetic particles in the solar atmosphere and energetic particles detected in interplanetary space and in the Earth's atmosphere. The implication of these observations are discussed. Stochastic and shock acceleration as well as acceleration in direct electric fields are considered. Interplanetary particle propagation is discussed and an overview of the highlights of both current and promising future research is presented.

Forman, M. A.↗

NASA NTRS1986

Detection of Machining Chips by Pressure Reversal

Inaccessible interior spaces inspected acoustically. In acoustic inspection, inlet and outlet ports of component connected to pneumatic hoses of apparatus that rapidly reverses induced pressure differential. If loose particles inside this component, they will generate noise detected by series of contact microphones attached to component. Noise indicates general location of contaminants, and its characteristic helps in identifying particles from their acoustic signatures.

Wyett, L. M.↗

NASA NTRS2008

Method and system for sensing and identifying foreign particles in a gaseous environment

An optical method and system sense and identify a foreign particle in a gaseous environment. A light source generates light. An electrically-conductive sheet has an array of holes formed through the sheet. Each hole has a diameter that is less than one quarter of the light's wavelength. The sheet is positioned relative to the light source such that the light is incident on one face of the sheet. An optical detector is positioned adjacent the sheet's opposing face and is spaced apart therefrom such that a gaseous environment is adapted to be disposed there between. Alterations in the light pattern detected by the optical detector indicate the presence of a foreign particle in the holes or on the sheet, while a laser induced fluorescence (LIF) signature associated with the foreign particle indicates the identity of the foreign particle.

Choi, Sang H.↗

NASA NTRS2005

TEM and NanoSIMS Study of Hydrated/Anhydrous Phase Mixed IDPs: Cometary or Asteroidal Origin?

Chondritic interplanetary dust particles (IDPs) are subdivided into (1) particles that form highly porous aggregates (chondritic porous "CP" IDPs), and (2) smooth particles ("CS" IDPs). Infrared (IR) spectroscopy has been a valuable tool for non-destructively determining the bulk mineralogy of IDPs. Most IDPs fall within three distinct IR groups: (1) olivine-rich particles, (2) pyroxene-rich particles, and (3) phyllosilicate-rich particles. From the IR studies, IDPs dominated by anhydrous minerals tend to be fine grained (CP), while phyllosilicate-rich IDPs are mostly CS. CP IDPs have been linked to cometary sources based on their compositions, spectral properties, and atmospheric entry velocities. Since no spectral signatures of hydrated minerals have been detected in comets, CS IDPs are thought to derive from primitive asteroids. Transmission electron microscopy (TEM) studies have revealed that the mineralogical distinctions between CP and CS IDPs are not always clear. Previous investigators have reported trace amounts of hydrous minerals in dominantly anhydrous particles. A better understanding of these particles will help to elucidate whether there is a genetic relationship between anhydrous and hydrated IDPs, provide insight into the earliest stages of aqueous alteration of primitive materials, and may help to determine whether comets have experienced any aqueous processing. Here we report a combined TEM and isotopic imaging study of an unusual anhydrous IDP with hydrated phases. Additional information is included in the original extended abstract.

Nakamura, K.↗

DOE OSTI2022

IceCube at the frontier of macroscopic dark matter direct detection

For a class of macroscopic dark matter models, inelastic scattering of dark matter off a nucleus can generate electromagnetic signatures with GeV-scale energy. The IceCube detector, with its kilometer-scale size, is ideal for directly detecting such inelastic scattering. Based on the slow particle trigger for the DeepCore detector, we perform a detailed signal and background simulation to estimate the discovery potential. For order 1 GeV deposited energy in each interaction, we find that IceCube can probe the dark matter masses up to one gram.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2020

Plasmon production from dark matter scattering

We present a first calculation of the rate for plasmon production in semiconductors from nuclei recoiling against dark matter. The process is analogous to bremsstrahlung of transverse photon modes, but with a longitudinal plasmon mode emitted instead. For dark matter in the 10 MeV—1 GeV mass range, we find that the plasmon bremsstrahlung rate is 4–5 orders of magnitude smaller than that for elastic scattering, but 4–5 orders of magnitude larger than the transverse bremsstrahlung rate. Because the plasmon can decay into electronic excitations and has characteristic energy given by the plasma frequency ω p , with ω p ≈ 16 eV in Si crystals, plasmon production provides a new signature and method to detect nuclear recoils from sub-GeV dark matter.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2026

Instantaneous difference frequency locking observed during toroidicity-induced Alfvén eigenmode coupling in the DIII-D tokamak

In magnetic confinement fusion, toroidicity-induced Alfvén eigenmodes (TAEs) are well-studied, weakly stable solutions of the linearized ideal magnetohydrodynamic equations. Driven unstable by suprathermal populations of energetic particles, TAE pose a key vulnerability to the confinement of high-energy alpha particles generated by fusion reactions. Hence, it is paramount to understand TAE dynamics if a working reactor is to be realized. In this work, we detect and characterize signatures of nonstationary nonlinear coupling between TAE using a novel, time-resolved bispectral analysis; results are supported by analytic signal of band-passed data. Crucially, a stationary phase relationship between two TAE and a nascent low frequency fluctuation is observed precisely when the triple product of magnetic fluctuation amplitudes is enhanced. Local mode number and frequency spectrum, gleaned from beam-emission spectroscopy, corroborates simultaneous satisfaction of nonlinear matching conditions, and provides a tool to identify theorized pathways of energy transfer, e.g. TAE parametric instability.

bispectral analysis↗

DOE OSTI2025

Detecting thermodynamic phase transition via explainable machine learning of photoemission spectroscopy

Identifying thermodynamic signatures of electronic phases, such as superconductivity, is challenging in low-dimensional materials due to strong fluctuations and low probing volume. Spectroscopic methods are often used to identify new bulk phases, but their main measurable quantity—electronic energy gaps—is no longer an effective order parameter in low-dimensional and fluctuating systems. Combining angle-resolved photoemission with a domain-adversarial neural network, we report a data-driven method to identify thermodynamic phase transitions solely based on single-particle spectra. We demonstrate 97.6% accuracy in cuprate superconductor Bi 2 Sr 2 CaCu 2 O 8+δ with strong superconducting fluctuations. This model notably compensates for the scarcity of experimental data by leveraging virtually inexhaustible simulated data. Further, its explainability reveals the crucial role of in-gap spectral weight in detecting phase fluctuations and thermodynamic transitions. Our work pinpoints the spectroscopic signatures of fluctuating orders and enables using spectroscopy for machine-learning-assisted material discovery for low-dimensional and strong coupling systems.

2D materials↗

DOE OSTI2022

Low-Energy Physics in Neutrino LArTPCs

In this white paper, we outline some of the scientific opportunities and challenges related to detection and reconstruction of low-energy (less than 100 MeV) signatures in liquid argon time-projection chamber (LArTPC) detectors. Key takeaways are summarized as follows. 1) LArTPCs have unique sensitivity to a range of physics and astrophysics signatures via detection of event features at and below the few tens of MeV range. 2) Low-energy signatures are an integral part of GeV-scale accelerator neutrino interaction final states, and their reconstruction can enhance the oscillation physics sensitivities of LArTPC experiments. 3) BSM signals from accelerator and natural sources also generate diverse signatures in the low-energy range, and reconstruction of these signatures can increase the breadth of BSM scenarios accessible in LArTPC-based searches. 4) Neutrino interaction cross sections and other nuclear physics processes in argon relevant to sub-hundred-MeV LArTPC signatures are poorly understood. Improved theory and experimental measurements are needed. Pion decay-at-rest sources and charged particle and neutron test beams are ideal facilities for experimentally improving this understanding. 5) There are specific calibration needs in the low-energy range, as well as specific needs for control and understanding of radiological and cosmogenic backgrounds. 6) Novel ideas for future LArTPC technology that enhance low-energy capabilities should be explored. These include novel charge enhancement and readout systems, enhanced photon detection, low radioactivity argon, and xenon doping. 7) Low-energy signatures, whether steady-state or part of a supernova burst or larger GeV-scale event topology, have specific triggering, DAQ and reconstruction requirements that must be addressed outside the scope of conventional GeV-scale data collection and analysis pathways.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗