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High-Speed Transport of Fluid Drops and Solid Particles via Surface Acoustic Waves

A compact sampling tool mechanism that can operate at various temperatures, and transport and sieve particle sizes of powdered cuttings and soil grains with no moving parts, has been created using traveling surface acoustic waves (SAWs) that are emitted by an inter-digital transducer (IDT). The generated waves are driven at about 10 MHz, and it causes powder to move towards the IDT at high speed with different speeds for different sizes of particles, which enables these particles to be sieved. This design is based on the use of SAWs and their propelling effect on powder particles and fluids along the path of the waves. Generally, SAWs are elastic waves propagating in a shallow layer of about one wavelength beneath the surface of a solid substrate. To generate SAWs, a piezoelectric plate is used that is made of LiNbO3 crystal cut along the x-axis with rotation of 127.8 along the y-axis. On this plate are printed pairs of fingerlike electrodes in the form of a grating that are activated by subjecting the gap between the electrodes to electric field. This configuration of a surface wave transmitter is called IDT. The IDT that was used consists of 20 pairs of fingers with 0.4-mm spacing, a total length of 12.5 mm. The surface wave is produced by the nature of piezoelectric material to contract or expand when subjected to an electric field. Driving the IDT to generate wave at high amplitudes provides an actuation mechanism where the surface particles move elliptically, pulling powder particles on the surface toward the wavesource and pushing liquids in the opposite direction. This behavior allows the innovation to separate large particles and fluids that are mixed. Fluids are removed at speed (7.5 to 15 cm/s), enabling this innovation of acting as a bladeless wiper for raindrops. For the windshield design, the electrodes could be made transparent so that they do not disturb the driver or pilot. Multiple IDTs can be synchronized to transport water or powder over larger distances. To demonstrate the transporting action, a video camera was used to record the movement. The speed of particles was measured from the video images.

Bar-Cohen, Yoseph↗

Preparation of a Frozen Regolith Simulant Bed for ISRU Component Testing in a Vacuum Chamber

In-Situ Resource Utilization (ISRU) systems and components have undergone extensive laboratory and field tests to expose hardware to relevant soil environments. The next step is to combine these soil environments with relevant pressure and temperature conditions. Previous testing has demonstrated how to incorporate large bins of unconsolidated lunar regolith into sufficiently sized vacuum chambers. In order to create appropriate depth dependent soil characteristics that are needed to test drilling operations for the lunar surface, the regolith simulant bed must by properly compacted and frozen. While small cryogenic simulant beds have been created for laboratory tests, this scale effort will allow testing of a full 1m drill which has been developed for a potential lunar prospector mission. Compacted bulk densities were measured at various moisture contents for GRC-3 and Chenobi regolith simulants. Vibrational compaction methods were compared with the previously used hammer compaction, or "Proctor", method. All testing was done per ASTM standard methods. A full 6.13 m3 simulant bed with 6 percent moisture by weight was prepared, compacted in layers, and frozen in a commercial freezer. Temperature and desiccation data was collected to determine logistics for preparation and transport of the simulant bed for thermal vacuum testing. Once in the vacuum facility, the simulant bed will be cryogenically frozen with liquid nitrogen. These cryogenic vacuum tests are underway, but results will not be included in this manuscript.

Klenhenz, Julie↗

Terrain Physical Properties Derived from Orbital Data and the First 360 Sols of Mars Science Laboratory Curiosity Rover Observations in Gale Crater

Physical properties of terrains encountered by the Curiosity rover during the rst 360 sols of operations have been inferred from analysis of the scour zones produced by Sky Crane Landing System engine plumes, wheel touch down dynamics, pits produced by Chemical Camera (ChemCam) laser shots, rover wheel traverses over rocks, the extent of sinkage into soils, and the magnitude and sign of rover-based slippage during drives. Results have been integrated with morphologic, mineralogic, and thermophysical properties derived from orbital data, and Curiosity-based measurements, to understand the nature and origin of physical properties of traversed terrains. The hummocky plains (HP) landing site and traverse locations consist ofmoderately to well-consolidated bedrock of alluvial origin variably covered by slightly cohesive, hard-packedbasaltic sand and dust, with both embedded and surface-strewn rock clasts. Rock clasts have been addedthrough local bedrock weathering and impact ejecta emplacement and form a pavement-like surface in whichonly small clasts (5 to 10 cm wide) have been pressed into the soil during wheel passages. The beddedfractured (BF) unit, site of Curiositys rst drilling activity, exposes several alluvial-lacustrine bedrock unitswith little to no soil cover and varying degrees of lithication. Small wheel sinkage values (1 cm) for both HPand BF surfaces demonstrate that compaction resistance countering driven-wheel thrust has been minimaland that rover slippage while traversing across horizontal surfaces or going uphill, and skid going downhill,have been dominated by terrain tilts and wheel-surface material shear modulus values.

Mars Science Laboratory Curiosity Gale Crater↗

In-Situ Water Vapor Probe for a Robot Arm-Mounted, Compact Water Vapor Analyzer: Preliminary Results

This work describes the ongoing development of an instrument package for the in-situ detection and isotopic analysis of water (from ice, icy soils, and hydrated minerals) on future lunar, asteroid, or martian exploration missions. This instrument is intended to be mounted on a robotic arm and be brought to the sample, rather than necessitating expensive and complicated sample handling to bring the sample to the instrument.

Socki, Richard A.↗

Improved Instrument for Detecting Water and Ice in Soil

An instrument measures electrical properties of relatively dry soils to determine their liquid water and/or ice contents. Designed as a prototype of instruments for measuring the liquid-water and ice contents of lunar and planetary soils, the apparatus could also be utilized for similar purposes in research and agriculture involving terrestrial desert soils and sands, and perhaps for measuring ice buildup on aircraft surfaces. This instrument is an improved version of the apparatus described in Measuring Low Concentrations of Liquid Water and Ice in Soil (NPO-41822), NASA Tech Briefs, Vol. 33, No. 2 (February 2009), page 22. The designs of both versions are based on the fact that the electrical behavior of a typical soil sample is well approximated by a network of resistors and capacitors in which resistances decrease and capacitances increase (and the magnitude and phase angle of impedance changes accordingly) with increasing water content. The previous version included an impedance spectrometer and a jar into which a sample of soil was placed. Four stainless-steel screws at the bottom of the jar were used as electrodes of a fourpoint impedance probe connected to the spectrometer. The present instrument does not include a sample jar and can be operated without acquiring or handling samples. Its impedance probe consists of a compact assembly of electrodes housed near the tip of a cylinder. The electrodes protrude slightly from the cylinder (see Figure 1). In preparation for measurements, the cylinder is simply pushed into the ground to bring the soil into contact with the electrodes.

Buehler, Martin↗

Lunar and Planetary Science XXXV: Missions and Instruments: Hopes and Hope Fulfilled

The titles in this section include: 1) Mars Global Surveyor Mars Orbiter Camera in the Extended Mission: The MOC Toolkit; 2) Mars Odyssey THEMIS-VIS Calibration; 3) Early Science Operations and Results from the ESA Mars Express Mission: Focus on Imaging and Spectral Mapping; 4) The Mars Express/NASA Project at JPL; 5) Beagle 2: Mission to Mars - Current Status; 6) The Beagle 2 Microscope; 7) Mars Environmental Chamber for Dynamic Dust Deposition and Statics Analysis; 8) Locating Targets for CRISM Based on Surface Morphology and Interpretation of THEMIS Data; 9) The Phoenix Mission to Mars; 10) First Studies of Possible Landing Sites for the Phoenix Mars Scout Mission Using the BMST; 11) The 2009 Mars Telecommunications Orbiter; 12) The Aurora Exploration Program - The ExoMars Mission; 13) Electron-induced Luminescence and X-Ray Spectrometer (ELXS) System Development; 14) Remote-Raman and Micro-Raman Studies of Solid CO2, CH4, Gas Hydrates and Ice; 15) The Compact Microimaging Spectrometer (CMIS): A New Tool for In-Situ Planetary Science; 16) Preliminary Results of a New Type of Surface Property Measurement Ideal for a Future Mars Rover Mission; 17) Electrodynamic Dust Shield for Solar Panels on Mars; 18) Sensor Web for Spatio-Temporal Monitoring of a Hydrological Environment; 19) Field Testing of an In-Situ Neutron Spectrometer for Planetary Exploration: First Results; 20) A Miniature Solid-State Spectrometer for Space Applications - Field Tests; 21) Application of Laser Induced Breakdown Spectroscopy (LIBS) to Mars Polar Exploration: LIBS Analysis of Water Ice and Water Ice/Soil Mixtures; 22) LIBS Analysis of Geological Samples at Low Pressures: Application to Mars, the Moon, and Asteroids; 23) In-Situ 1-D and 2-D Mapping of Soil Core and Rock Samples Using the LIBS Long Spark; 24) Rocks Analysis at Stand Off Distance by LIBS in Martian Conditions; 25) Evaluation of a Compact Spectrograph/Detection System for a LIBS Instrument for In-Situ and Stand-Off Detection; 26) Analysis of Organic Compounds in Mars Analog Samples; 27) Report of the Organic Contamination Science Steering Group; 28) The Water-Wheel IR (WIR) - A Contact Survey Experiment for Water and Carbonates on Mars; 29) Mid-IR Fiber Optic Probe for In Situ Water Detection and Characterization; 30) Effects of Subsurface Sampling & Processing on Martian Simulant Containing Varying Quantities of Water; 31) The Subsurface Ice Probe (SIPR): A Low-Power Thermal Probe for the Martian Polar Layered Deposits; 32) Deploying Ground Penetrating Radar in Planetary Analog Sites to Evaluate Potential Instrument Capabilities on Future Mars Missions; 33) Evaluation of Rock Powdering Methods to Obtain Fine-grained Samples for CHEMIN, a Combined XRD/XRF Instrument; 34) Novel Sample-handling Approach for XRD Analysis with Minimal Sample Preparation; 35) A New Celestial Navigation Method for Mars Landers; 36) Mars Mineral Spectroscopy Web Site: A Resource for Remote Planetary Spectroscopy.

Source record↗

Pancam Multispectral and APXS Chemical Examination of Rocks and Soils in Marathon Valley and Points South Along the Rim of Endeavour Crater

The Mars Exploration Rover Opportunity has concluded its exploration of Marathon Valley, a 100-meter-wide valley in the western rim of the 22-kilometer-diameter Endeavour crater. Orbital observations from CRISM (Compact Reconnaissance Imaging Spectrometer for Mars) indicated the presence of Fe smectites in Marathon Valley. Since leaving the valley, Opportunity has been traversing along the inner rim of the crater, and currently towards the outer rim. This presentation describes the Pancam 430 to 1009 nanometer (VNIR - Visible and Near Infared) multispectral reflectance and APXS (Alpha Particle X-ray Spectrometer) chemical compositions of rock and soil units observed during the latter portions of the Marathon Valley campaign on the Knudson Ridge area and observations of those materi-als along the traverse to the south. Full Pancam spectral coverage of rock targets consists of 13 filter (13f) data collections with 11 spectrally unique channels with data processing. Data were examined using spectral parameters, decorrelation stretch composites, and spectral mixture analysis. Note that color terms used here refer to colors in various false-color renditions, not true colors. The APXS determines major and select trace element compositions of targets.

Farrand, W. H.↗

Mega-geomorphology and neotectonics

For several decades, subtle neotectonic effects involving several square kilometers have been studied in detail using remote sensing, primarily various types of stereo-aerial photographs at scales of 1:10,000 to 1:80,000. These subtle effects, especially local uplifts associated with growing structures of differential compaction, have been detected by the effect on drainage patterns, changes in hydraulic geometry of individuals channels or groups of channels, tonal halos (soil) and fracture patterns. The studies were extended with the advent of thermal IR imagery particularly in tonal analysis, and SLAR primarily in fracture pattern studies. Lately, quantitative efforts have begun attempting to link measured uplift over known structures with measured changes in hydraulic geometry and alluvial deposition. Thus, efforts are now underway attempting to quantify the relationship between neo- (micro-) tectonic changes and geomorphic parameters of drainage systems.

Lattman, L. H.↗

The Australian National Airborne Field Experiment 2005: Soil Moisture Remote Sensing at 60 Meter Resolution and Up

Spatially-distributed soil moisture observations have applications spanning a wide range of spatial resolutions from the very local needs of individual farmers to the progressively larger areas of interest to weather forecasters, water resource managers, and global climate modelers. To date, the most promising approach for space-based remote sensing of soil moisture makes use of passive microwave emission radiometers at L-band frequencies (1-2 GHz). Several soil moisture-sensing satellites have been proposed in recent years, with the European Space Agency's Soil Moisture Ocean Salinity (SMOS) mission scheduled to be launched first in a couple years. While such a microwave-based approach has the advantage of essentially allweather operation, satellite size limits spatial resolution to 10's of km. Whether used at this native resolution or in conjunction with some type of downscaling technique to generate soil moisture estimates on a finer-scale grid, the effects of subpixel spatial variability play a critical role. The soil moisture variability is typically affected by factors such as vegetation, topography, surface roughness, and soil texture. Understanding and these factors is the key to achieving accurate soil moisture retrievals at any scale. Indeed, the ability to compensate for these factors ultimately limits the achievable spatial resolution and/or accuracy of the retrieval. Over the last 20 years, a series of airborne campaigns in the USA have supported the development of algorithms for spaceborne soil moisture retrieval. The most important observations involved imagery from passive microwave radiometers. The early campaigns proved that the retrieval worked for larger and larger footprints, up to satellite-scale footprints. These provided the solid basis for proposing the satellite missions. More recent campaigns have explored other aspects such as retrieval performance through greater amounts of vegetation. All of these campaigns featured extensive ground truth collection over a range of grid spacings, to provide a basis for examining the effects of subpixel variability. However, the native footprint size of the airborne L-band radiometers was always a few hundred meters. During the recently completed (November, 2005) National Airborne Field Experiment (NAFE) campaign in Australia, a compact L-band radiometer was deployed on a small aircraft. This new combination permitted routine observations at native resolutions as high as 60 meters, substantially finer than in previous airborne soil moisture campaigns, as well as satellite footprint areal coverage. The radiometer, the Polarimetric L-band Microwave Radiometer (PLMR) performed extremely well and operations included extensive calibration-related observations. Thus, along with the extensive fine-scale ground truth, the NAFE dataset includes all the ingredients for the first scaling studies involving very-high-native resolution soil moisture observations and the effects of vegetation, roughness, etc. A brief overview of the NAFE will be presented, then examples of the airborne observations with resolutions from 60 m to 1 km will be shown, and early results from scaling studies will be discussed.

Kim, E. J.↗

Numerical study of the chemo-mechanical behavior of FEBEX bentonite in nuclear waste disposal based on the Barcelona expansive model

Experimental studies show that compacted bentonite used as a backfill material for nuclear waste repository experiences strong coupling between chemical and mechanical processes. Here, we use a dual-structure expansive soil model, referred to as the Barcelona Expansive Model (BExM), to predict the behavior of bentonite buffer in subsurface emplacement tunnels for high-level radioactive waste. After emplacement, the bentonite is subjected to complex and coupled Thermal-Hydraulic-Mechanical-Chemical (THMC) processes. The BExM constitutive model is implemented in a multi-phase reactive transport and geomechanics simulator, TOUGHREACT-FLAC3D, and the model is verified with one benchmark test on FEBEX bentonite. We utilize a one-way Chemo-Mechanical (C-M) coupling approach, in which chemical changes affect the mechanical behavior of bentonite through the BExM linked with the evolution of mass fraction of smectite, exchangeable cation concentration, and ionic strength via osmotic suction. The parameters of the new coupled model for FEBEX bentonite are calibrated against a series of laboratory experiments with various salinity solutions. Finally, coupled THMC modeling is conducted for a generic argillite repository with bentonite buffer under high temperature, focusing on the long-term chemical change and its effect on the mechanical process.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Grating-Based Imaging-Scattering with Portable Neutron Generator

Company: Adelphi Technology, Inc. Title: Grating-Based Imaging-Scattering with Portable Neutron Generator PI: Dr. Jay Theodore Cremer, Jr. Topic: 26a Statement of the problem or situation that is being addressed. Successful plant growth depends upon an efficient and robust root system. The plant root is part of a larger system of water and microbial flows in the soil system. While much effort has been exerted to develop an imaging system for water, microbes, and roots, the problem is challenging, and no widely accepted imaging method currently exists. The optical solutions use a highly modified soil system. X-ray imaging methods are insensitive to the soft tissues in the presence of sand. Thermal neutron imaging has been often tested, but found inadequate, due to limited access and low image resolution. This project will develop a new strategy for neutron imaging of plant/soil systems. The project will allow long duration experiments in greenhouse environments and increase the image information content to the micron scale. General statement of how this problem is being addressed. Portable, rugged thermal and fast neutron sources are being developed where portable means a two-soldier team can carry the source and power unit to survey rough terrain for explosives. In the past decade, microfabrication of X-ray and thermal/cold neutron optics has opened a new imaging strategy. The standard transmission image is now supplemented with simultaneous acquisition of a phase contrast image and an image revealing scattering features. In materials science, the interferometric neutron scattering image has been used to detect early crack formation in stressed additive manufacturing test samples. The detection requires sensitivity to scattering features at the 1-micron scale. By addition of our proposed grating-optic to Adelphi Technology’s radiographic/tomographic imaging system, which is based on portable thermal neutron source, the resulting thermal neutron scatter image of the plant/soil system, will reveal details at 1-micron. Commercial Applications and Other Benefits Neutron interferometry imaging has greater penetration through large metal components compared to industrial X-ray imaging. The low-cost, large area optics developed for greenhouse applications, combined with the robust, portable neutron generator, can then be marketed as a system for inspection of additive manufactured components. In the aerospace industry, all freshly printed components are validated with X-ray CT. Scheduled maintenance again requires X-ray CT as the ability to predict aerospace component lifetime does not yet exist. Large aerospace components are only partially observed with X-ray imaging. Key Words Neutron radiography/tomography, grating interferometry, thermal neutron generator imaging, plant root and soil imaging, rhizosphere imaging, deployable neutron imaging systems Summary for Members of Congress A rugged, portable source of thermal neutrons is adapted for neutron interferometry imaging with the addition of low-cost, 3D printed optics. The first application of our proposed deployable, compact thermal neutron generator imaging system, using a grating optic, is plant root/soil science in greenhouse settings and agricultural laboratories.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Self-supervised and multi-fidelity learning for extended predictive soil spectroscopy

Infrared spectroscopy is a cost-effective, non-destructive, and environmentally benign technology that is increasingly recognized as an important solution for meeting the global demand for soil data. While both near-infrared (NIR) and mid-infrared (MIR) diffuse reflectance spectroscopy enable rapid estimation of soil properties, they present a significant trade-off: NIR offers superior scalability and lower operational costs, whereas MIR provides higher analytical fidelity by capturing fundamental molecular vibrations. In this study, we propose a self-supervised, multi-fidelity learning framework designed to bridge this gap. Our approach leverages large-scale MIR spectral libraries to learn a compact, transferable latent representation, into which NIR spectra are subsequently aligned for downstream prediction. The workflow consists of pretraining a latent model on a large MIR library, adapting the representation using a smaller paired NIR–MIR dataset, and evaluating generalization on an independent external test set. Across a range of chemical and physical soil properties, we found that MIR-derived embeddings improved prediction accuracy relative to baseline models that used raw MIR inputs. Predictions derived from the spectrum conversion (NIR to MIR) task did not match the performance of the original MIR spectra but were similar or superior to predictive performance of NIR-only models, suggesting the unified spectral latent space can effectively leverage the larger and more diverse MIR dataset for prediction of soil properties not well represented in current NIR libraries.

54 ENVIRONMENTAL SCIENCES↗

Conjectures about the evolution of the moon.

The principal questions about the derivation of the lunar surface have not yet been settled: is it the surface left over from the process of accumulation of the moon, or is it a surface generated by magmatic processes on the moon and subsequently altered by further infall from outside. The evidence derived from many sources now favors the former. Seismic data suggest an absence of bedrock down to a depth of several kilometers, and instead a compacted powder only. The 'mascon' evidence can be understood as a consequence of major impacts in a deep porous layer. The great abundance of cosmic ray tracks in most soil samples demands a much greater cosmic ray dosage than present rates would cause in the age of the moon, unless the dust represented infallen material previously irradiated.

Gold, T.↗

Developing Soil Models for Dynamic Impact Simulations

This paper describes fundamental soils characterization work performed at NASA Langley Research Center in support of the Subsonic Rotary Wing (SRW) Aeronautics Program and the Orion Landing System (LS) Advanced Development Program (ADP). LS-DYNA(Registered TradeMark)1 soil impact model development and test-analysis correlation results are presented for: (1) a 38-ft/s vertical drop test of a composite fuselage section, outfitted with four blocks of deployable energy absorbers (DEA), onto sand, and (2) a series of impact tests of a 1/2-scale geometric boilerplate Orion capsule onto soil. In addition, the paper will discuss LS-DYNA contact analysis at the soil/structure interface, methods used to estimate frictional forces, and the sensitivity of the model to density, moisture, and compaction.

Fasanella, Edwin L.↗

Long-Life, Lightweight, Multi-Roller Traction Drives for Planetary Vehicle Surface Exploration

NASA s initiative for Lunar and Martian exploration will require long lived, robust drive systems for manned vehicles that must operate in hostile environments. The operation of these mechanical drives will pose a problem because of the existing extreme operating conditions. Some of these extreme conditions include operating at a very high or very cold temperature, operating over a wide range of temperatures, operating in very dusty environments, operating in a very high radiation environment, and operating in possibly corrosive environments. Current drive systems use gears with various configurations of teeth. These gears must be lubricated with oil (or grease) and must have some sort of a lubricant resupply system. For drive systems, oil poses problems such as evaporation, becoming too viscous and eventually freezing at cold temperatures, being too thin to lubricate at high temperatures, being degraded by the radiation environment, being contaminated by the regolith (soil), and if vaporized (and not sealed), it will contaminate the regolith. Thus, it may not be advisable or even possible to use oil because of these limitations. An oil-less, compact traction vehicle drive is a drive designed for use in hostile environments like those that will be encountered on planetary surfaces. Initially, traction roller tests in vacuum were conducted to obtain traction and endurance data needed for designing the drives. From that data, a traction drive was designed that would fit into a prototype lunar rover vehicle, and this design data was used to construct several traction drives. These drives were then tested in air to determine their performance characteristics, and if any final corrections to the designs were necessary. A limitation with current speed reducer systems such as planetary gears and harmonic drives is the high-contact stresses that occur at tooth engagement and in the harmonic drive wave generator interface. These high stresses induce high wear of solid lubricant coatings, thus necessitating the use of liquid lubricants for long life.

Klein, Richard C.↗

Spectral Analysis of Regular Material Point Method and its Application to Study High Pressure Reverse Osmosis Membrane Compaction and Embossing

Material Point Method (MPM) is gaining widespread interest in applied continuum mechanics. The fact that all the continuum properties are stored on the particles (or material points) and the governing equations are solved on these material points makes MPM extremely suited to problems involving severe material deformations, such as crack propagation, soil movement, and fluid flows. Despite its popularity, only a few studies have focused on the numerical properties of MPM. This presentation introduces a global spectral analysis of the regular material point method. Contrary to previous studies, the analysis focuses on the numerical properties of the method in the spectral space. The amplification factor is derived as a function of the non- dimensional wave numbers. It provides insights into the stability and dissipative properties of the method for various CFL and Fourier numbers. The effect of the grid shape functions, number of particles per cell and their locations inside the grid cell are also analyzed. The EXAGOOP MPM solver (https://github.com/NREL/Exagoop.git) is developed at the National Renewable Energy Laboratory as a part of the NAWI UHPRO project and is based on the AMReX framework. A single-level, uniform cartesian grid is used as the background mesh, while the particle class in AMReX is used to manage the material point operations. Linear hat and B-splines are used as grid shape functions, while the time integration is performed using explicit Euler time integration. EXAGOOP is both CPU and GPU compatible and has been demonstrated to work well on multiple compute architectures. The performance of EXAGOOP on various computing architectures is presented along with its application to study compaction and embossing of high-pressure reverse osmosis membranes. The MPM solution accurately reproduces the membrane deformation. The deformed pore size and structure simulated using MPM also agree well with experimental SEM images.

material point method↗

RadSTAR L-Band Imaging Scatterometer: Performance Assessment

RadSTAR is an instrument development program aimed at combining a radiometer and a scatterometer system into a highly compact configuration that uses a single, electronically scanned antenna to provide co-located and simultaneous measurements of emission and backscatter for airborne and spaceborne applications [I]. The program was designed to map soil moisture and ocean salinity, both important components of the water cycle, and to map sea ice density and thickness, an important factor in ocean-atmosphere heat exchange in Polar Regions. The accuracy in estimation of these and a number of other Earth science parameters can be greatly enhanced by providing the co-aligned radar/radiometer microwave measurements. For instance, radiometer estimates of soil moisture from soil emission are affected by emission from vegetation, and from the roughness of the surface. Complementary measurements using the scatterometer can be used to evaluate the vegetation and surface roughness effects. Hence, the combined observations can provide an improved estimate. As with soil moisture, the ocean salinity is a function of the microwave emission from the sea surface temperature (SST) and sea roughness. There, the addition of radar backscatter measurements of sea roughness enables the correction of the emissivity and provide more accurate estimates of ocean salinity. Similar arguments can be made for other important Earth science parameters. This paper discusses the RadSTAR program, the radar system design, calibration, and digital beamforming techniques, and presents preliminary analysis of the data collected during the test flights. The data sets obtained during the flights and during the radar calibration in the anechoic chamber are also employed to asses the performance of the radar. The paper also discusses the Digital Beamforming Synthetic Aperture Radar (DBSAR) processor, a real-time processor recently developed for the LIS instrument which enables beam synthesis, fine resolutions, and large swaths.

Rincon, Rafael↗

Nanofluidic Size-Exclusion Chromatograph

Efforts are under way to develop a nanofluidic size-exclusion chromatograph (SEC), which would be a compact, robust, lightweight instrument for separating molecules of interest according to their sizes and measuring their relative abundances in small samples. About as large as a deck of playing cards, the nanofluidic SEC would serve, in effect, as a laboratory on a chip that would perform the functions of a much larger, conventional, bench-top SEC and ancillary equipment, while consuming much less power and much smaller quantities of reagent and sample materials. Its compactness and low power demand would render it attractive for field applications in which, typically, it would be used to identify and quantitate a broad range of polar and nonpolar organic compounds in soil, ice, and water samples. Size-exclusion chromatography is a special case of high-performance liquid chromatography. In a conventional SEC, a sample plug is driven by pressure along a column packed with silica or polymer beads that contain uniform nanopores. The interstices between, and the pores in, the beads collectively constitute a size-exclusion network. Molecules follow different paths through the size-exclusion network, such that characteristic elution times can be related to sizes of molecules: basically, smaller molecules reach the downstream end of the column after the larger ones do because the smaller ones enter minor pores and stay there for a while, whereas the larger ones do not enter the pores. The volume accessible to molecules gradually diminishes as their size increases. All molecules bigger than a pore size elute together. For most substances, the elution times and sizes of molecules can be correlated directly with molecular weights. Hence, by measuring the flux of molecules arriving at the downstream end as a function of time, one can obtain a liquid mass spectrum for the molecules present in a sample over a broad range of molecular weights.

Feldman, Sabrina↗