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NASA NTRS1986

Analytical ultrasonics for evaluation of composite materials response. Part 2: Generation and detection

To evaluate the response of composite materials, it is imperative that the input excitation as well as the observed output be well characterized. This characterization ideally should be in terms of displacements as a function of time with high spatial resolution. Additionally, the ability to prescribe these features for the excitation is highly desirable. Various methods for generating and detecting ultrasound in advanced composite materials are examined. Characterization and tailoring of input excitation is considered for contact and noncontact, mechanical, and electromechanical devices. Type of response as well as temporal and spatial resolution of detection methods are discussed as well. Results of investigations at Virginia Tech in application of these techniques to characterizing the response of advanced composites are presented.

Duke, J. C., Jr.↗

DOE OSTI2016

Engineered magnetic domain textures in exchange bias bilayer systems

A magnetic domain texture has been deterministically engineered in a topographically flat exchange-biased (EB) thin film system. The texture consists of long-range periodically arranged unit cells of four individual domains, characterized by individual anisotropies, individual geometry, and with non-collinear remanent magnetizations. The texture has been engineered by a sequence of light-ion bombardment induced magnetic patterning of the EB layer system. The magnetic texture's in-plane spatial magnetization distribution and the corresponding domain walls have been characterized by scanning electron microscopy with polarization analysis (SEMPA). The influence of magnetic stray fields emerging from neighboring domain walls and the influence of the different anisotropies of the adjacent domains on the Néel type domain wall core's magnetization rotation sense and widths were investigated. It is shown that the usual energy degeneracy of clockwise and counterclockwise rotating magnetization through the walls is revoked, suppressing Bloch lines along the domain wall. Estimates of the domain wall widths for different domain configurations based on material parameters determined by vibrating sample magnetometry were quantitatively compared to the SEMPA data.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2024

Characterization of Crystal Properties and Defects in CdZnTe Radiation Detectors

CdZnTe-based detectors are highly valued because of their high spectral resolution, which is an essential feature for nuclear medical imaging. However, this resolution is compromised when there are substantial defects in the CdZnTe crystals. In this study, we present a learning-based approach to determine the spatially dependent bulk properties and defects in semiconductor detectors. This characterization allows us to mitigate and compensate for the undesired effects caused by crystal impurities. We tested our model with computer-generated noise-free input data, where it showed excellent accuracy, achieving an average RMSE of 0.43% between the predicted and the ground truth crystal properties. In addition, a sensitivity analysis was performed to determine the effect of noisy data on the accuracy of the model.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2017

Increased Throughput and Sensitivity of Synchrotron-Based Characterization for Photovoltaic Materials

Optimizing photovoltaic (PV) devices requires characterization and optimization across several length scales, from centimeters to nanometers. Synchrotron-based micro-X-ray fluorescence spectromicroscopy (μ-XRF) is a valuable link in the PV-related material and device characterization suite. μ-XRF maps of elemental distributions in PV materials have high spatial resolution and excellent sensitivity and can be measured on absorber materials and full devices. Recently, we implemented on-the-fly data collection (flyscan) at Beamline 2-ID-D at the Advanced Photon Source at Argonne National Laboratory, eliminating a 300 ms per-pixel overhead time. This faster scanning enables high-sensitivity (~10 14 atoms/cm 2 ), large-area (10 000s of μm 2 ), high-spatial resolution (<;200 nm scale) maps to be completed within a practical scanning time. We specifically show that when characterizing detrimental trace metal precipitate distributions in multicrystalline silicon wafers for PV, flyscans can increase the productivity of μ-XRF by an order of magnitude. Additionally, flyscan μ-XRF mapping enables relatively large-area correlative microscopy. As an example, we map the transition metal distribution in a 50 μm-diameter laser-fired contact of a silicon solar cell before and after lasing. As a result, while we focus on μ-XRF of mc-Si wafers for PV, our results apply broadly to synchrotron-based mapping of PV absorbers and devices.

14 SOLAR ENERGY↗

DOE OSTI2016

Spatially-Resolved Proteomics: Rapid Quantitative Analysis of Laser Capture Microdissected Alveolar Tissue Samples

Global proteomics approaches allow characterization of whole tissue lysates to an impressive depth. However, it is now increasingly recognized that to better understand the complexity of multicellular organisms, global protein profiling of specific spatially defined regions/substructures of tissues (i.e. spatially-resolved proteomics) is essential. Laser capture microdissection (LCM) enables microscopic isolation of defined regions of tissues preserving crucial spatial information. However, current proteomics workflows entail several manual sample preparation steps and are challenged by the microscopic mass-limited samples generated by LCM, and that impact measurement robustness, quantification, and throughput. Here, we coupled LCM with a fully automated sample preparation workflow that with a single manual step allows: protein extraction, tryptic digestion, peptide cleanup and LC-MS/MS analysis of proteomes from microdissected tissues. Benchmarking against the current state of the art in ultrasensitive global proteomic analysis, our approach demonstrated significant improvements in quantification and throughput. Using our LCM-SNaPP proteomics approach, we characterized to a depth of more than 3,400 proteins, the ontogeny of protein changes during normal lung development in laser capture microdissected alveolar tissue containing ~4,000 cells per sample. Importantly, the data revealed quantitative changes for 350 low abundance transcription factors and signaling molecules, confirming earlier transcript-level observations and defining seven modules of coordinated transcription factor/signaling molecule expression patterns, suggesting that a complex network of temporal regulatory control directs normal lung development with epigenetic regulation fine-tuning pre-natal developmental processes. Furthermore, our LCM-proteomics approach facilitates efficient, spatially-resolved, ultrasensitive global proteomics analyses in high-throughput that will be enabling for several clinical and biological applications.

60 APPLIED LIFE SCIENCES↗

NASA NTRS2004

A Comparison of Local Variance, Fractal Dimension, and Moran's I as Aids to Multispectral Image Classification

The accuracy of traditional multispectral maximum-likelihood image classification is limited by the skewed statistical distributions of reflectances from the complex heterogenous mixture of land cover types in urban areas. This work examines the utility of local variance, fractal dimension and Moran's I index of spatial autocorrelation in segmenting multispectral satellite imagery. Tools available in the Image Characterization and Modeling System (ICAMS) were used to analyze Landsat 7 imagery of Atlanta, Georgia. Although segmentation of panchromatic images is possible using indicators of spatial complexity, different land covers often yield similar values of these indices. Better results are obtained when a surface of local fractal dimension or spatial autocorrelation is combined as an additional layer in a supervised maximum-likelihood multispectral classification. The addition of fractal dimension measures is particularly effective at resolving land cover classes within urbanized areas, as compared to per-pixel spectral classification techniques.

Emerson, Charles W.↗

NASA NTRS2010

Application of a Near Infrared Imaging System for Thermographic Imaging of the Space Shuttle during Hypersonic Re-Entry

High resolution calibrated near infrared (NIR) imagery was obtained of the Space Shuttle s reentry during STS-119, STS-125, and STS-128 missions. The infrared imagery was collected using a US Navy NP-3D Orion aircraft using a long-range infrared optical package referred to as Cast Glance. The slant ranges between the Space Shuttle and Cast Glance were approximately 26-41 nautical miles at point of closest approach. The Hypersonic Thermodynamic Infrared Measurements (HYTHIRM) project was a NASA Langley led endeavor sponsored by the NASA Engineering Safety Center, the Space Shuttle Program Office and the NASA Aeronautics Research Mission Directorate to demonstrate a quantitative thermal imaging capability. HYTHIRM required several mission tools to acquire the imagery. These tools include pre-mission acquisition simulations of the Shuttle trajectory in relationship to the Cast Glance aircraft flight path, radiance modeling to predict the infrared response of the Shuttle, and post mission analysis tools to process the infrared imagery to quantitative temperature maps. The spatially resolved global thermal measurements made during the Shuttle s hypersonic reentry provides valuable flight data for reducing the uncertainty associated with present day ground-to-flight extrapolation techniques and current state-of-the-art empirical boundary-layer transition or turbulent heating prediction methods. Laminar and turbulent flight data is considered critical for the development of turbulence models supporting NASA s next-generation spacecraft. This paper will provide the motivation and details behind the use of an upgraded NIR imaging system used onboard a Navy Cast Glance aircraft and describe the characterizations and procedures performed to obtain quantitative temperature maps. A brief description and assessment will be provided of the previously used analog NIR camera along with image examples from Shuttle missions STS-121, STS-115, and solar tower test. These thermal observations confirmed the challenge of a long-range acquisition during re-entry. These challenges are due to unknown atmospheric conditions, image saturation, vibration etc. This provides the motivation for the use of a digital NIR sensor. The characterizations performed on the digital NIR sensor included radiometric, spatial, and spectral measurements using blackbody radiation sources and known targets. An assessment of the collected data for three Space Shuttle atmospheric re-entries, STS-119, STS-125, and STS-128, are provided along with a description of various events of interest captured using the digital NIR imaging system such as RCS firings and boundary layer transitions. Lastly the process used to convert the raw image counts to quantitative temperatures is presented along with comparisons to the Space Shuttle's onboard thermocouples.

Zalameda, Joseph N.↗

NASA NTRSDate not supplied

Flow Characterization of the NASA Langley Unitary Plan WindTunnel, Test Section 2: Computational Results

Flow in the empty Unitary Planform Wind Tunnel at the NASA Langley Research Center issimulated with computational fluid dynamics methods. The objectives are to assess CFD’s truepredictive capability and to generate flow-field maps upstream of the tunnel’s test section foruse in associated vehicle tests. Multiple CFD solvers, grid adaption methods, and turbulencemodels are used by five teams doing the simulations. The simulation domain is as large aspractical: from the start of the settling chamber, just downstream of the last set of turningvanes, to well downstream of the test section. Simulations are done at three Mach numbers andseveral Reynolds numbers that cover most of the tunnel’s operating range. The sensitivity ofthe CFD solutions to simulation process details, including turbulence model, spatial resolutionand settling-chamber inflow velocity profile, is characterized. Significant sensitivities in somedetails of the predicted test section flow are described. CFD predicts that details of flow inthe settling chamber can affect the flow in the test section. Turning of the flow through thetunnel contraction and past nozzle-block hardware generates streamwise vortices, some ofwhich survive into the core of the test section, principally at low Mach number. Preliminarycomparisons to experimental measurements are given. The major flow characteristics andthe dynamical vortices predicted by CFD exist in the experiment. Several details in CFD andexperiment are observed to differ, including the effects of the vortices and features that appearto be Mach waves in the test section. Sensitivity to grid resolution and turbulence modelingis noted in the vortices; no potential cause for the differences in Mach waves has yet beenidentified in the CFD sensitivity studies.

wind tunnel↗

DOE OSTI2018

Wavelet multiresolution analysis of particle-laden turbulence

Direct numerical simulations of incompressible homogeneous-isotropic turbulence laden with a dilute suspension of inertial point particles are performed in conjunction with a wavelet multiresolution analysis of the results. The use of spatially localized wavelet basis functions enables the simultaneous consideration of physical and scale spaces in the spectral characterization of the flow field of the carrier phase and the concentration field of the dispersed phase. The multiresolution analysis of the dispersed phase provides statistical information about the spatial variabilities of a scale-dependent coarse-grained number density field and the local energy spectra of its fluctuations, characterizing the sensitivities of those quantities to variations in scale and Stokes number. In particular, the spatial variabilities of the wavelet energy spectrum of the particle concentration fluctuations are observed to be maximum in regimes where the particles preferentially concentrate. The results highlight the scale-dependent inhomogeneities of the structures in the concentration field generated by preferential concentration, and the existence of characteristic scales of interaction between the dispersed and carrier phases. Additionally, an interphase multiresolution analysis is performed that indicates the occurrence of a spatial anticorrelation between the enstrophy and kinetic-energy spectra of the carrier phase and the particle concentration at small scales in regimes where preferential concentration is important. In conclusion, this anticorrelation vanishes as the scale is increased and is largely suppressed when the preferential-concentration effect is negligible.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

NASA NTRS2003

Characterization of Aeromechanics Response and Instability in Fans, Compressors, and Turbine Blades

This study investigated the effect of interaction between tip clearance flow, steady and unsteady upstream wakes in rotor and stator blade rows in terms of blade forced response. In a stator blade row, the interaction of steady wakes in the upstream rotor frame with the stator imply a blade forced response whose spectrum contains the Blade passing frequency (BPF) and its harmonics, with a decaying amplitude as the frequency increases. When the incoming wakes are unsteady, however, the spectrum of blade excitation exhibits unexpectedly amplified high frequencies due to the modulation of BPF with the fluctuation frequency. In a rotor blade row, a tip flow instability has been demonstrated with a frequency (TVF) equal to 0.45 times the Blade Passing frequency corresponding to a reduced frequency (F(sub c) (sup +)) of 0.7. Under uniform inlet flow conditions, the frequency and spatial content of the tip flow region have been characterized. The disturbance TVF was the dominant disturbance in the flow field and was found to imply variations of the pressure coefficient of more than 30% on the blade tip (between 35% to 90% chord) and in the rotor-generated wake (from 75% to 100% hub-to-tip position). In an attempt to better understand the origin of the instability, the structure of the tip flow has also been analyzed. The interface between the tip flow region and the core flow has been found to have periodical wave-like flow patterns which proceed downstream at a speed of approximately 0.42 times the core flow speed at a frequency corresponding to TVF. A list of conclusions derived from these interactions is presented.

Tan, Choon S.↗

NASA NTRS2001

On-Orbit Performance of MODIS On-Board Calibrators

The Terra MODIS (Moderate Resolution Imaging Spectroradiometer) was launched on December 18, 1999 and acquired the first scene data on February 24, 2000. It has 36 spectral bands covering spectral range from 0.41 to 14.2 microns and provides spatial resolutions of 250 (2 bands), 500 (5 bands), and 1000 m at Nadir. The instrument on-orbit calibration and characterization are determined and monitored through the use of a number of on-board calibrators (OBC). Radiometric calibration for the reflective solar bands (B1-B19, B26), from VIS (visible) to SWIR (short wavelength infrared) (0.41 to 2.1 microns), uses a Spectralon (tm) solar diffuser (SD) and a solar diffuser stability monitor (SDSM). For the thermal emissive bands (B20-B25, B27-B36), from MWIR (medium wavelength infrared) to LWIR (long wavelength infrared) (3.75 to 14.2 micron), a V-grooved flat panel blackbody is used. The instrument spectral for the VIS to SWIR bands and spatial co-registration characterizations for all bands are monitored on-orbit by the spectral radiometric calibration assembly (SRCA). In this report, we discuss the application and performance of the key MODIS on-board calibrators and their impacts on the instrument system calibration and characterization.

Xiong, X.↗

NASA NTRS2016

Overview of LBTI: A Multipurpose Facility for High Spatial Resolution Observations

The Large Binocular Telescope Interferometer (LBTI) is a high spatial resolution instrument developed for coherent imaging and nulling interferometry using the 14.4 m baseline of the 2x8.4 m LBT. The unique telescope design, comprising of the dual apertures on a common elevation-azimuth mount, enables a broad use of observing modes. The full system is comprised of dual adaptive optics systems, a near-infrared phasing camera, a 1-5 micrometer camera (called LMIRCam), and an 8-13 micrometer camera (called NOMIC). The key program for LBTI is the Hunt for Observable Signatures of Terrestrial planetary Systems (HOSTS), a survey using nulling interferometry to constrain the typical brightness from exozodiacal dust around nearby stars. Additional observations focus on the detection and characterization of giant planets in the thermal infrared, high spatial resolution imaging of complex scenes such as Jupiter's moon, Io, planets forming in transition disks, and the structure of active Galactic Nuclei (AGN). Several instrumental upgrades are currently underway to improve and expand the capabilities of LBTI. These include: Improving the performance and limiting magnitude of the parallel adaptive optics systems; quadrupling the field of view of LMIRcam (increasing to 20"x20"); adding an integral field spectrometry mode; and implementing a new algorithm for path length correction that accounts for dispersion due to atmospheric water vapor. We present the current architecture and performance of LBTI, as well as an overview of the upgrades.

The Large Binocular Telescope Interferometer (LBTI↗

NASA NTRS2013

Suomi NPP VIIRS Prelaunch and On-orbit Geometric Calibration and Characterization

The Visible Infrared Imager Radiometer Suite (VIIRS) sensor was launched 28 October 2011 on the Suomi National Polarorbiting Partnership (SNPP) satellite. VIIRS has 22 spectral bands covering the spectrum between 0.412 m and 12.01 m, including 16 moderate resolution bands (M-bands) with a spatial resolution of 750 m at nadir, 5 imaging resolution bands (I-bands) with a spatial resolution of 375 m at nadir, and 1 day-night band (DNB) with a near-constant 750 m spatial resolution throughout the scan. These bands are located in a visible and near infrared (VisNIR) focal plane assembly (FPA), a short- and mid-wave infrared (SWMWIR) FPA and a long-wave infrared (LWIR) FPA. All bands, except the DNB, are co-registered for proper environmental data records (EDRs) retrievals. Observations from VIIRS instrument provide long-term measurements of biogeophysical variables for climate research and polar satellite data stream for the operational communitys use in weather forecasting and disaster relief and other applications. Well Earth-located (geolocated) instrument data is important to retrieving accurate biogeophysical variables. This paper describes prelaunch pointing and alignment measurements, and the two sets of on-orbit correction of geolocation errors, the first of which corrected error from 1,300 m to within 75 m (20 I-band pixel size), and the second of which fine tuned scan angle dependent errors, bringing VIIRS geolocation products to high maturity in one and a half years of the SNPP VIIRS on-orbit operations. Prelaunch calibration and the on-orbit characterization of sensor spatial impulse responses and band-to-band co-registration (BBR) are also described.

Geolocation↗

NASA NTRS1997

Application of High-Resolution Thermal Infrared Remote Sensing and GIS to Assess the Urban Heat Island Effect

Day and night airborne thermal infrared image data at 5 m spatial resolution acquired with the 15-channel (0.45 micron - 12.2 micron) Advanced Thermal and Land Applications Sensor (ATLAS) over Alabama, Huntsville on 7 September, 1994 were used to study changes in the thermal signatures of urban land cover types between day and night. Thermal channel number 13 (9.6 micron - 10.2 micron) data with the best noise-equivalent temperature change (NEAT) of 0.25 C after atmospheric corrections and temperature calibration were selected for use in this analysis. This research also examined the relation between land cover irradiance and vegetation amount, using the Normalized Difference Vegetation Index (NDVI), obtained by ratioing the difference and the sum of the red (channel number 3: 0.60-0.63 micron) and reflected infrared (channel number 6: 0.76-0.90 micron) ATLAS data. Based on the mean radiance values, standard deviations, and NDVI extracted from 351 pairs of polygons of day and night channel number 13 images for the city of Huntsville, a spatial model of warming and cooling characteristics of commercial, residential, agricultural, vegetation, and water features was developed using a GIS approach. There is a strong negative correlation between NDVI and irradiance of residential, agricultural, and vacant/transitional land cover types, indicating that the irradiance of a land cover type is greatly influenced by the amount of vegetation present. The predominance of forests, agricultural, and residential uses associated with varying degrees of tree cover showed great contrasts with commercial and services land cover types in the center of the city, and favors the development of urban heat islands. The high-resolution thermal infrared images match the complexity of the urban environment, and are capable of characterizing accurately the urban land cover types for the spatial modeling of the urban heat island effect using a GIS approach.

Lo, C. P.↗

DOE OSTI2018

Sum-Frequency Generation from a Thin Cylindrical Layer

In the Rayleigh–Gans–Debye approximation, we have solved the problem of the sum-frequency generation by two plane elliptically polarized electromagnetic waves from the surface of a dielectric particle of a cylindrical shape that is coated by a thin layer possessing nonlinear optical properties. The formulas that describe the sum-frequency field have been presented in the tensor and vector forms for the second-order nonlinear dielectric susceptibility tensor, which was chosen in the general form, containing chiral components. Expressions describing the sum-frequency field from the cylindrical particle ends have been obtained for the case of a nonlinear layer possessing chiral properties. Three-dimensional directivity patterns of the sum-frequency radiation have been analyzed for different combinations of parameters (angles of incidence, degrees of ellipticity, orientations of polarization ellipses, cylindrical particle dimensions). The mathematical properties of the spatial distribution functions of the sum-frequency field, which characterize the symmetry of directivity patterns, have been revealed.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2017

X-ray micro computed tomography characterization of cellular SiC foams for their applications in chemical engineering

Open-cell SiC foams clearly are promising materials for continuous-flow chemical applications such as heterogeneous catalysis and distillation. X-ray micro computed tomography characterization of cellular β-SiC foams at a spatial voxel size of 13.6{sup 3} μm{sup 3} and the interpretation of morphological properties of SiC open-cell foams with implications to their transport properties are presented. Static liquid hold-up in SiC foams was investigated through in-situ draining experiments for the first time using the μ-CT technique providing thorough 3D information about the amount and distribution of liquid hold-up inside the foam. This will enable better modeling and design of structured reactors based on SiC foams in the future. In order to see more practical uses, μ-CT data of cellular foams must be exploited to optimize the design of the morphology of foams for a specific application. - Highlights: •Characterization of SiC foams using novel X-ray micro computed tomography. •Interpretation of structural properties of SiC foams regarding to their transport properties. •Static liquid hold-up analysis of SiC foams through in-situ draining experiments.

36 MATERIALS SCIENCE↗

DOE OSTI2016

Coupling among Microbial Communities, Biogeochemistry, and Mineralogy across Biogeochemical Facies

Physical properties of sediments are commonly used to define subsurface lithofacies and these same physical properties influence subsurface microbial communities. This suggests an (unexploited) opportunity to use the spatial distribution of facies to predict spatial variation in biogeochemically relevant microbial attributes. Here, we characterize three biogeochemical facies—oxidized, reduced, and transition—within one lithofacies and elucidate relationships among facies features and microbial community biomass, diversity, and community composition. Consistent with previous observations of biogeochemical hotspots at environmental transition zones, we find elevated biomass within a biogeochemical facies that occurred at the transition between oxidized and reduced biogeochemical facies. Microbial diversity—the number of microbial taxa—was lower within the reduced facies and was well-explained by a combination of pH and mineralogy. Null modeling revealed that microbial community composition was influenced by ecological selection imposed by redox state and mineralogy, possibly due to effects on nutrient availability or transport. As an illustrative case, we predict microbial biomass concentration across a three-dimensional spatial domain by coupling the spatial distribution of subsurface biogeochemical facies with biomass-facies relationships revealed here. We expect that merging such an approach with hydro-biogeochemical models will provide important constraints on simulated dynamics, thereby reducing uncertainty in model predictions.

Stegen, James C.↗

DOE OSTI2025

Real-time neutron multiplicity and source localization for criticality safety during fuel debris removal

Advancing neutron detection and analysis techniques for complex radiation environments is an ongoing focus in nuclear instrumentation and monitoring. This proposal presents research and development of a generalized real-time neutron monitoring and analysis system, applicable to any detector capable of producing time-tagged neutron count data. While the work is demonstrated using the Neutron Multiplication Analysis Detector (NoMAD), a modular 15-tube helium-3 (He-3) array, due to its availability, spatial resolution, and flexible deployment, the methods developed are extensible to other systems, including organic scintillators and fast digital detectors. This research investigates two complementary analytical techniques for real-time characterization of neutron emitting sources: neutron multiplicity estimation based on the Hage-Cifarelli formalism and spatial localization using supervised machine learning applied to spatial count rate patterns. These methods are designed to operate under dynamic, evolving conditions such as fuel debris retrieval or reactor startup, where neutron-emitting material geometries may be partially unknown or changing over time. By integrating statistical neutron emission data with spatial localization, this research aims to develop and evaluate methods for real time neutron monitoring, source characterization, and material verification. Key contributions include implementation of a low-latency data pipeline for continuous neutron multiplicity analysis, development and validation of machine learning models for spatial inference, and experimental evaluation of system performance under variable measurement conditions. The outcomes are intended to support applications in nuclear safeguards, verification, emergency response, and reactor startup.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗