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At least 937 records · Page 52

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DOE OSTI2025

When Pore Met Semi: Charting the Rise of Porous Metal Halide Semiconductors

Metal halide semiconductors (MHS) are a versatile class of materials with fully customizable mechanical and optoelectronic properties that have proven to be prominent candidates in numerous impactful applications. Finding a way to generate porosity in MHS would bestow upon them an additional node in property engineering, thus allowing them to be utilized in uncharted technologies. Motivated by this promise, we developed a general strategy to render the MHS porous. We employed molecular cages as structure-directing agents and countercations, which fostered a new family of materials: porous metal halide semiconductors (PMHS). The presence of molecular cages gave rise to ultramicroporous structures imposed by the organic part cavities and a record water stability performance of 27 months so far. In this Perspective, we discuss the principles and promises of PMHS, which combine the merits of porous and electronic compounds.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2025

Structural Design and Modeling of MARVEL Primary Coolant System Using the ASME Section III, Division 5, Code

This paper presents the structural design and supporting analysis for the Microreactor Applications Research Validation and Evaluation (MARVEL) primary coolant system (PCS) using the American Society of Mechanical Engineers (ASME) Boiler and Pressure Vessel Code Section III, Division 5, rules. MARVEL is a liquid metal–cooled microreactor intended to provide experimental capabilities for the rapid testing and development of microreactor technologies. The PCS utilizes high-temperature sodium-potassium liquid metal as the primary coolant and operates at a design temperature of 570°C, necessitating the consideration of creep-related failure mechanisms. The base metal for the PCS is 316H stainless steel, and the weldments are made with a 16-8-2 filler. The design approach incorporates the current base code rules along with ASME code cases N-924, N-861, and N-862 to address primary load, ratcheting, and creep-fatigue evaluations, respectively. The reactor’s operation involves complex thermal and mechanical interactions due to natural convective flow and differential thermal expansion between components. In conclusion, this paper discusses the structural engineering challenges encountered, such as managing thermal stresses in the distribution plenum and guard vessel, and outlines the strategies implemented to meet the code requirements, including design modifications and operational constraints.

21 - SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLAN↗

DOE OSTI2026

Status Update of Permanent Magnet Radiation Resiliency Studies at CEBAF

The proposed energy upgrade of the Continuous Electron Beam Accelerator Facility (CEBAF) incorporates Fixed-Field Alternating-gradient (FFA) arcs utilizing permanent magnet technology. Given the radiation environment within the CEBAF tunnel enclosure, validating the long-term magnetic stability of these materials is a critical step for the project's technical feasibility. This contribution presents an overview of the ongoing permanent magnet radiation resiliency program at Jefferson Lab. We briefly review the experimental methodology used to monitor demagnetization in situ and summarize the operational experience from the initial data-taking campaign. Furthermore, we discuss the upgrades implemented for the second exposure campaign, currently underway, which aims to refine dose correlation and reduce systematic uncertainties. We report on the general status of the program and the roadmap for certifying permanent magnet optics for the proposed upgrade energies.

Bodenstein, R. [Thomas Jefferson National Accelera↗

DOE OSTI2024

Advanced Reactor Safeguards & Security 2024 Program Roadmap

The Advanced Reactor Safeguards and Security (ARSS) program was established to provide research support addressing near term challenges that advanced nuclear reactor vendors face in meeting domestic Material Control and Accounting (MC&A), Physical Protection System (PPS), and Cybersecurity requirements for U.S. construction. The technical work in the program is meant to (1) support nuclear reactor vendors with advanced MC&A, PPS, and Cybersecurity designs for next generation reactors, (2) provide technical bases for the regulator, and (3) promote the integration of Safeguards and Security by Design early in the design process. Existing domestic regulations for safeguards and security, as outlined in the Code of Federal Regulations, were written for large light water reactors, and rule-making efforts are underway to develop regulations more suited to different reactor designs. The ARSS program seeks to remove roadblocks in the deployment of new and advanced reactors by solving regulatory challenges, reducing safeguards and security costs, and utilizing the latest technologies and approaches for robust plant monitoring and protection. This roadmap discusses the goals of the ARSS program, current research, and program plan for the next five years.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

DOE OSTI2024

Laboratory Directed Research & Development: FY23 Annual Report

Sandia is a federally funded research and development center (FFRDC) focused on developing and applying advanced science and engineering capabilities to mitigate national security threats. This is accomplished through the exceptional staff leading research at the Labs and partnering with universities and companies. Sandia’s LDRD program aims to maintain the scientific and technical vitality of the Labs and to enhance the Labs’ ability to address future national security needs. The program funds foundational, leading-edge discretionary research projects that cultivate and utilize core science, technology, and engineering (ST&E) capabilities. Per Congressional intent (P.L. 101-510) and Department of Energy (DOE) guidance (DOE Order 413.2C, Chg 1), Sandia’s LDRD program is crucial to maintaining the nation’s scientific and technical vitality

96 KNOWLEDGE MANAGEMENT AND PRESERVATION↗

DOE OSTI2024

MAPSTER: Automated Geospatial Data Sharing – Version 1.4.0

The US Department of Energy’s (DOE) Oak Ridge National Laboratory (ORNL) developed MAPSTER which is a geospatial data management tool that aggregates, organizes, and shares data from dispersed sources such as unmanned aerial systems (UAS). Built specifically for use in environments where communications may be limited, MAPSTER utilizes two key technologies to effectively manage data in the field and enable easy data sharing with authorized partners: Observer and Checkpoint. Observer is a lightweight software package on an edge device, such as a laptop, that automatically detects newly processed UAS data and sends to a central server called Checkpoint. Checkpoint is a centralized server at ORNL that receives and manages data from all Observer instances. Even in a very low bandwidth environment, Observer can still send information about the UAS data product almost instantly as it generates its own metadata package on the size of KB (kilobytes). MAPSTER is not only for UAS data but for any geospatial data collected at the austere edge and dispersed sources.

97 MATHEMATICS AND COMPUTING↗

DOE OSTI2024

Optimal Design and Operation of a Solvent-Sorbent Hybrid Capture Process for Minimizing the Cost of High Capture

High capture can cause a significant increase in energy penalty if the appropriate technology/technologies are not utilized. The optimal technology for bulk capture is not necessarily the optimal technology for polishing capture (i.e., high extent of capture from the flue gas with very low partial pressure of CO2). This work investigates the use of MEA for bulk capture with the polishing capture being accomplished by a functionalized metal organic framework (MOF).

Kasturi, Pooja↗

DOE OSTI2024

Sustainable Solar Energy for Hughes Village (Hudotl’eekkaakk’e Tribe) (Final Technical Report)

Hughes Village Council is the local Tribal government for Hughes, Alaska. With the funding from this project, the Village Council designed and installed a 120kW solar Photo Voltaic (PV) array with a 250 kW/335kWh lithium-ion battery bank that has offset diesel consumption in the community by an estimated 10% per year. This translates to approximately 6,000 gallons of fuel per year. The goal is to reduce diesel consumption and turn the diesel generators off for certain periods of the Alaskan summer when solar PV is abundant and electrical loads in the community are low. Daily generator logs from the community show an average load of approximately 50kW-60kW with peaks ranging from 100kW-160kW. This project aligns with the tribe’s mission to work towards tribal energy sovereignty, utilizing sustainable energy technologies, and their overall goal of 25% clean energy by 2025.

14 SOLAR ENERGY↗

DOE OSTI2025

RESEARCH Laboratory Directed Research & Development FY24 Annual Report

99 GENERAL AND MISCELLANEOUS↗

DOE OSTI2025

UNIFI's Grid-Forming (GFM) Inverter Reference Design: A Tutorial on Modeling, Control, and Experimental Implementation of GFM Inverters

The UNIFI Consortium's tutorial on grid-forming (GFM) inverters provides a comprehensive guide to the modeling, control, and experimental implementation of GFM inverters. As the integration of renewable energy accelerates, the transition from traditional grid following (GFL) to GFM inverters is crucial to ensure stable and sustainable power systems. This document outlines a reference design for three-phase and single-phase GFM inverters developed at the University of Texas at Austin. The tutorial also provides step-by-step guidance for accessing and using UNIFI’s GitHub repository, enabling users to design, build, and test GFM inverters efficiently. By fostering collaboration and equipping users with accessible resources, this initiative aims to drive widespread adoption of GFM technology across academia, utilities, and industries.

24 POWER TRANSMISSION AND DISTRIBUTION↗

DOE OSTI2025

Material Control & Accounting Modeling Developments for a Generic TRISO Fuel Fabrication Facility

The Material Protection, Accounting, and Control Technologies (MPACT) program utilizes modeling and simulation to assess Material Control and Accountability (MC&A) concerns for a variety of nuclear facilities. The Sandia National Laboratories (SNL)-developed Fissile Facility Flow Modeler (F3M) and the Material Accountancy Performance Indicator Toolkit (MAPIT) have historically provided MPACT with the capability to analyze MC&A approaches for nuclear facilities to determine that these facilities meet regulatory requirements. In FY25, improvements on the application of the F3M and MAPIT tools to simulate a generic TRi-structural ISOtropic (TRISO) fuel fabrication facility were successfully completed. The generic TRISO fuel fabrication F3M model captures the entire TRISO fuel fabrication process and is adaptable to any final TRISO fuel form, including spherical pebbles and cylindrical compacts loaded into graphite prismatic blocks. Comprehensive F3M/MAPIT functionality for the generic TRISO fuel fabrication model has been demonstrated. This modeling framework can be applied to support the U.S. Department of Energy and domestic nuclear industry stakeholders in developing MC&A approaches for advanced fuel fabrication facilities via statistical tests that demonstrate compliance to regulatory requirements.

97 MATHEMATICS AND COMPUTING↗

DOE OSTI2026

Dynamic Evaluation of the Upper Tyler Formation and Well Stimulation Fluid Interactions Using Micro-CT Imaging

Abundant concentrations of swelling clays in the oil-bearing upper Tyler Formation inhibit unconventional well stimulation techniques and associated long-term oil and gas production success. Laboratory evaluation of the geochemical interactions between the formation material and various stimulation fluids may help identify innovative approaches that provide a solution to successful well stimulation and subsequent oil production. The objective of this research was to understand the complexities of well stimulation fluid and clay mineral interactions within the Tyler Formation and identify potential fracturing fluid formulations that mitigate swelling properties of the clays in the reservoir to enhance stimulation success and promote long-term oil and gas production. Collaboration with the National Energy Technology Laboratory (NETL), utilizing their Tescan DynaTOM micro-CT analysis instrumentation, provided an innovative approach to understand real-time, dynamic interactions of the formation material and various potential stimulation fluids. Results are anticipated to identify key mechanisms occurring at the micro-scale level and provide insight into modified stimulation techniques uniquely suited for successful production applications.

enhanced oil recovery↗

DOE OSTI2025

A Novel Approach for Microencapsulating Salt Hydrate-Based Phase Change Materials

Energy storage technologies, particularly those utilizing phase change materials (PCMs), have gained attention for their high energy density and efficient thermal management. PCMs, which store energy through solid-liquid phase transitions, can efficiently capture and release thermal energy, but face the challenge of leakage during the phase change process. Inorganic PCMs, such as salt hydrates, offer high energy storage capacity, but are difficult to encapsulate due to their corrosive nature. Conventional encapsulation techniques for inorganic PCMs are limited, particularly for scalable applications. In this work, we present an innovative method for the encapsulation of salt hydrate-based inorganic PCMs (CaCl 2 ·6H 2 O) using co-axial electrospinning. The process involves the creation of co-axial fibers, with salt hydrate as the core and polymer (e.g., PVP) as the outer shell, effectively preventing leakage and improving the stability of the PCM. This approach demonstrates the potential for scalable microencapsulation of inorganic PCMs, marking the first report of using co-axial electrospinning for this purpose. This novel technique could contribute to enhancing the performance and applicability of PCMs in thermal energy storage systems and other energy efficiency applications.

36 MATERIALS SCIENCE↗

DOE OSTI2026

Wind Turbine Materials Recycling Prize Phase 2 (Commercialization of Wind Turbine Blade Waste (WTBW)-Based, Lightweight, Cementitious Composite Materials): Cooperative Research and Development Final Report, CRADA Number CRD-24-31305

The National Laboratory of the Rockies (NLR) and AltiSora, LLC., will develop new lightweight cementitious composite material technologies that will utilize wind turbine blade waste as a raw material to; (1) allow a high value addition (2) at low cost, enabling (3) a significant waste consumption volume; while (4) consuming the entire wind turbine blade, without (5) creating any waste or emissions and to also (6) offer specific benefits to communities involved.

17 WIND ENERGY↗

NASA NTRS1968