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At least 937 records · Page 52

Chromium-Based Mitigation Coatings on SiC Materials for Fuel Cladding

SiC composites are undergoing assessment under the Advanced Fuels Campaign for Light Water Reactors (LWR) as an Accident Tolerant Fuel (ATF) cladding. As noted, the main concern has been the hydrothermal corrosion of SiC under all LWR chemistries, resulting in cladding oxidation and recession unacceptable for the duration of burn-up. Improvements in future fuel burn-up further increase recession mitigation requirements. Hermeticity of ceramic cladding may also be a concern in terms of quality control. Coatings are being investigated as a practical solution to address concerns regarding SiC cladding for both accident conditions and normal operations. SiC materials were coated by various technologies to produce Cr-based mitigation coatings as a corrosion barrier in LWR water chemistry. In all cases, deposition of Cr compounds requires that SiC behave as a cathode during processing, which requires surface electrical conductivity. Morphology and phase analysis of the coatings are still undergoing investigation, mainly for predicting differential swelling, thermal expansion and microcracking. Autoclave corrosion and in-pile irradiation in a PWR water loop will follow in mid-2016. (authors)

36 MATERIALS SCIENCE↗

The PROMETRA program: plane strain tests on fresh and highly irradiated zircaloy-4, ZIRLO and M5 fuel claddings

In the framework of the PROMETRA program, clad hardening constitutive laws (stress-strain curves) have been already implemented in the SCANAIR code. These laws were derived from uniaxial hoop tensile tests performed on narrow machined ring samples. However, they do not reproduce the conditions of strain multi-axiality acting on cladding during a RIA (Reactivity-Initiated Accident) in a PWR. As a consequence, a new specimen called Plane Strain Tensile (PST) similar to the annular sample developed by Pennsylvania State University has been developed at CEA on a wider notched ring. It aims to accurately predict the cladding failure in more prototypical conditions, close to plane strain hoop tension in the middle of the gage section. This paper details the PST tests implementation and results in the framework of the PROMETRA program on fresh and irradiated claddings. The development of this test has led also to the development of a technique to measure local deformations in the gage section of the PST specimen using 2-D Digital Image Correlation (DIC). Tests performed on fresh Zircaloy-4 and on irradiated Zircaloy-4, M5 and ZIRLO specimens are analyzed relying of post-test examinations and finite element simulations. In the case of tests performed on irradiated Zry-4 and ZIRLO at 280 and 350 Celsius degrees, the presence of a hydride rim favors the crack nucleation on the outer surface. In this case, rupture nucleation occurs preferentially in the vicinity of notches. Such tests are not representative of the rupture of a cladding subjected to plane strain loading. Nevertheless, they give a good representation of the initiation of rupture observed during RIA on irradiated cladding, resulting in a hydride damage. Zry-4 specimens tested at 480 Celsius degrees and M5TM at 280 and 350 C. degrees result in a ductile fracture nucleation in the center of the specimen. This rupture is prototypical of a ductile rupture of an irradiated specimen subjected to a plane strain loading. However, the nucleation on inner surface by shear at the mandrel contact is not prototypical of a clad rupture during the PCMI (Pellet Clad Mechanical Interaction) phase of a RIA (membrane stresses in the clad thickness in RIA). An important lesson learned from this experimental approach is that the PST test is a particularly complex test, both in its implementation and interpretation.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Multiscale Modeling of Accident Tolerant Fuels under the NEAMS ATF Program

The U.S. Department of Energy's Nuclear Energy Advanced Modeling and Simulation (NEAMS) program has been developing computational analysis tools for nuclear fuel simulation. These codes include BISON and Marmot for investigation of fuel behavior at the continuum and microstructural scales, respectively. In 2014, NEAMS introduced what it calls High Impact Problems (HIPs) into its development plan. These HIPs are intended to make significant advancements in a particular area of nuclear power research in a short period of time (3 years or less). NEAMS has chosen an accident tolerant fuel (ATF) project, which emphasizes utilizing BISON and Marmot to model proposed materials, as its first HIP. Since the events that occurred at the Fukushima-Daiichi nuclear power plant in 2011, the U.S. Department of Energy's Office of Nuclear Energy accelerated research in nuclear fuel concepts with enhanced accident tolerance as part of its Fuel Cycle Research and Development (FCRD) Advanced Fuels Campaign (AFC). Accident tolerant fuels are expected to perform at least as well as conventional fuel during normal conditions and provide significantly increased response time in the event of an accident. Given the many unknowns associated with proposed ATF concepts, the research and development being undertaken by AFC in this area is a challenge, particularly considering the desire to have a lead test rod or assembly in a commercial plant by 2022. With the AFC as its primary stakeholder, the NEAMS ATF HIP is developing material models (using a multi-scale approach) for multiple candidate materials. Through a variety of analyses employing these models, the ATF HIP is providing insight and support to the AFC as it strives to understand these materials and prioritize further development. Use of computational tools such as BISON and Marmot are a vital component of the AFC's strategy since experimental data will not be available broadly and quickly enough to understand the proposed materials fully by the time the AFC must make further development decisions. This summary reviews the overall approach of the NEAMS ATF HIP. First, we give an overview of the current materials chosen for investigation. We also review the overall multi-scale approach to model development. We briefly review the work underway at multiple national laboratories to develop mechanistic engineering scale models based on lower length scale insight. Note that coordinated work is also underway at multiple universities, but those efforts are not detailed here. The NEAMS ATF HIP is assisting the AFC in assessing two accident tolerant materials, uranium silicide fuel and FeCrAl cladding. A multi-scale material model development approach is being undertaken to formulate the models necessary to investigate the materials over a range of normal and off-normal scenarios. This approach includes molecular dynamics, density functional theory, mesoscale modeling, and engineering scale modeling. Sensitivity studies are underway to understand the most critical scenarios and material model input parameters. The information generated is being given to the AFC for their use in selecting promising ATF concepts. (authors)

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Characterization of modeling and experimental data inconsistencies from burst testing for high-burnup commercial fuel rod applications

Fuel fragmentation, relocation, and dispersal are some of the largest issues remaining in the nuclear industry before rod-average burnup can be increased beyond 62 GWd/tU. The issue is primarily related to the potential for fuel to be dispersed into the reactor primary system, which may increase public risk. One way to prevent dispersal is to avoid cladding burst. The objective of this work is to support the high burnup safety case by evaluating cladding burst under high-burnup, full-length fuel rods and to identify uncertainties that could improve model predictions. The results of this analysis will evaluate realistic, prototypic loss-of-coolant accident (LOCA) conditions; support future cladding burst test designs; and inform the development of mechanistic material models. Realistic high-burnup operating conditions were implemented in the BISON fuel performance code to simulate steady-state and LOCA transient fuel rod evolution to the point at which cladding burst occurred. Parametric studies are performed to assess code response to changes in rod internal pressures and heating rates. Results were compared with simulated LOCA experiments to identify inconsistencies between commercial fuel rod analysis and experimental validation. The representative full-length fuel rod LOCA simulation results did not agree with cladding burst tests. Cladding burst tests indicated burst occurring well below (100–150 °C) those calculated in the full-length fuel rod LOCA analysis. Further investigation indicated that the cladding burst tests do not appear to be representative for full-length fuel rods. The inconsistency investigated in this work showed that the differences between the BISON simulation and the experiment's cladding burst conditions arise from an incomplete characterization of the cladding surface temperature, detailed rodlet characterization, lack of cladding strain measurements, and uncertainty in the cladding creep and failure models.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Out-of-pile performance of High Temperature Irradiation Resistant and Cladding Thermocouples

The High Temperature Irradiation Resistant thermocouple (HTIR-TCs) has proven to be the nuclear temperature sensor. It outlast and outperforms all other commercially available thermocouples above 1100 °C inside reactor pressure vessels; also, recent calibration methods have pushed the HTIR-TC to accurately read temperatures through thermal transients during reactor shutdowns and restarts. The new temperature range of HTIR-TCs is from 0 °C to 1650 °C. The main objective of this study is to address manufacturing a more robust TC for handling and inserting into reactor experiments; to also apply the TC to a wider application. The TC has shown to be mainly susceptible to oxygen levels inside the heat treatment and calibration process and it is recommended that O2 levels be brought to as low as possible. However, through modeling efforts the O2 has been found to intercalate only within the first few layers of niobium on the outer sheath. Lastly, multiple materials were used for the sheath and insulators; all with similar outcomes when testing occurred over a long period of time.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Reduced Diameter and Lined Cladding Production Status

A contract has been placed with Century Tube Inc. to produce cladding for the FAST experiment. Excess EBR II cladding tubes will be cold drawn down to 0.115 in. diameter × 0.009 in. wall and 0.077 in. × 0.006 in. wall. Lined cladding will also be tested in the FAST experiment. Century Tube will produce several samples, varying assembly the assembly process, with solid zirconium or vanadium rods inside of the HT9. Cladding/liner bonding of each will be evaluated using microscopy. The best one will be further processed to form a liner tube within the cladding. A shrink fit approach is also being developed, where a solid zirconium or vanadium bar is shrunk fit into a cladding piece. This process has shown favorable results and will be compared against the co drawn samples when available.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Investigation of Tank 241-AN-101 Floating Solids

Tank 241-AN-101 is the receiver tank for retrieval of several C-Farms waste tanks, including Tanks 241-C-102 and 241-C-111. Tank 241 C 111 received first-cycle decontamination waste from the bismuth phosphate process and Plutonium and Uranium Extraction cladding waste, as well as hydraulic fluid. Three grab samples, 1AN-16-01, 1AN-16-01A, and 1AN-16-01B, were collected at the surface of Tank 241-AN-101 on April 25, 2016, after Tank 241-C-111 retrieval was completed. Floating solids were observed in the three grab samples in the 11A hot cell after the samples were received at the 222-S Laboratory. Routine chemical analyses, solid phase characterization on the floating and settled solids, semivolatile organic analysis mainly on the aqueous phase for identification of degradation products of hydraulic fluids were performed. Investigation of the floating solids is reported.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Thermal mechanical assessment of a SiC-SiC-composite clad fuel pin concept in a light water reactor environment

Accident Tolerant Fuels (ATFs) are designed to increase coping time following an accident scenario while preserving or improving current steady state reactor operational performance. A potential ATF concept is SiC-SiC composite claddings. Fuel performance simulations were conducted on a SiC-SiC based cladding concept utilizing a multilayered approach for improved performance. This cladding concept referred to as the Duplex concept is a duplex structure composed of a monolithic SiC layer placed on the outside of a SiC-SiC composite. A liquid metal is added to fuel-cladding gap for improved heat dissipation from the fuel. The monolithic SiC layer is used to improve the coolant corrosion characteristics and protect the SiC-SiC composite layer from exposure to the coolant. The fuel performance code BISON was used to conduct fuel performance simulations on the cladding concepts. Comparisons are made with a current prototypic fuel rod design (UO 2 fuel enclosed in Zircaloy-4 cladding). Representative steady-state cases were considered for normal power and two cycle power histories. Additionally, a PCI ramp case was simulated to analyze potential anticipated operational occurrences. Transient response during a Loss of Coolant Accident and a Reactivity Initiated Accident were also simulated. This computational study demonstrated that for normal operating conditions, the SiC concept cladding performed as well as the baseline for the standard power cases evaluated. The ramping evaluations indicate potential fracturing of the SiC-SiC composite of the composite cladding compared to the Zircaloy-4 cladding due to the temperature gradient and the subsequent differential thermal conductivity degradation and swelling across the composite thickness. In conclusion, the rod fails early at low enthalpy for RIA but survives a LOCA with minimal material loss due to high temperature steam corrosion.

11 - NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Investigation of constituent redistribution in U-Pu-Zr fuels and its dependence on varying Zr content

This contribution investigates fuel constituent segregation and fuel-cladding chemical interactions (FCCI) in three U-Pu-Zr fuel pins irradiated to ~11% burnup in Experimental Breeder Reactor-II as part of the X441 DP-1 experiment. In examined pins, Zr content ranged from 6 to 10 and 14 wt.%, while Pu concentration was constant at 19 wt.% Pu. The primary goal of the investigation was to determine the role Zr content plays in fuel performance and this manuscript provides assessment of both constituent redistribution and FCCI as a function of axial position. FCCI was observed in all pins, though no cladding failure was noted. Optical and scanning electron microscopy (SEM) results show that variation in Zr content alters the number and relative size of constituent redistribution zones in the fuel. For example, larger Zr-rich central regions and smaller U-rich intermediate regions were observed in 14 wt.% Zr fuels. More importantly, all examined fuels have four or more discrete constituent redistribution regions, where each region has dissimilar morphological features. The existence of four to six distinctive regions deviates from traditionally accepted three region redistribution model, highlights complexity of constituent redistribution in this metal fuel, and identifies the need to conduct additional studies using state-of-the-art instrumentation.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Potential Effect of Interfacial Bonding on Used Nuclear Fuel Vibration Reliability

This summary abstract describes the methodology used to evaluate the effect of pellet pellet and pellet clad interactions with consideration of the interfacial bonding efficiency on UNF vibration integrity. This methodology provides a solid roadmap for further protocol development with respect to effective lifetime prediction of a UNF system under normal transportation vibration. The proposed methodology that couples FEA simulations and experimental exploration efforts is also under development. The current methodology is focused on assessing the influence of interfacial bonding at the pellet pellet and the pellet clad interfaces on UNF vibration integrity. The FEA simulation results were also calibrated and benchmarked with the fatigue aging data obtained from reversible bending fatigue testing.

fuel-pellet interface↗

PWR cores with silicon carbide cladding

The feasibility of using silicon carbide rather than Zircaloy cladding, to reach higher power levels and higher discharge burnups in PWRs has been evaluated. A preliminary fuel design using fuel rods with the same dimensions as in the Westinghouse Robust Fuel Assembly but with fuel pellets having 10 vol% central void has been adopted to mitigate the higher fuel temperatures that occur due to the lower thermal conductivity of the silicon carbide and to the persistence of the open clad-pellet gap over most of the fuel life. With this modified fuel design, it is possible to achieve 18 month cycles that meet present-day operating constraints on peaking factor, boron concentration, reactivity coefficients and shutdown margin, while allowing batch average discharge burnups up to 80 MWD/kgU and peak rod burnups up to 100 MWD/kgU. Power uprates of 10% and possibly 20% also appear feasible. For non-uprated cores, the silicon carbide-clad fuel has a clear advantage that increases with increasing discharge burnup. Even for comparable discharge burnups, there is a savings in enriched uranium. Control rod configuration modifications may be required to meet the shutdown margin criterion for the 20% up-rate. Silicon carbide's ability to sustain higher burnups than Zircaloy also allows the design of a licensable two year cycle with only 96 fresh assemblies, avoiding the enriched uranium penalty incurred with use of larger batch sizes due to their excessive leakage. (authors)

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

Multidimensional modeling of fuel-cladding friction in an LWR fuel rod

Solving finite element problems with friction often increases the level of difficulty to obtain properly converged solutions. This type of challenge becomes more salient when advanced, possibly multiscale, material models are employed to capture the thermomechanical behavior of fuel and cladding materials. Here the present work details our recent developments in a nuclear fuel performance finite element code for the systematic consideration of friction in nuclear reactor finite element simulations. We show the application of friction and its effects on the mechanics of light-water reactor rods accounting for various fuel constitutive modeling techniques, model dimensionalities, pellet assumed geometries, and power conditions. In particular, we focus on the fuel rod mechanical behavior as it relates to fuel constitutive models, sensitivity to the coefficient of friction, pellet states of stress, and rod elongation. We discuss the trade-offs between the various multidimensional modeling options and highlight the relevance of frictional effects in the prediction of the fuel rod deformation and interfacial stresses. To relate our modeling results with actual reactor operation, simulations including frictional effects are compared with fuel rod elongation experimental data and some challenges for carrying out a full validation of the axial mechanics are discussed.

42 ENGINEERING↗

Preliminary Content Evaluation of the North Anna High Burn-Up Sister Fuel Rod Segments for Transportation in the 10-160B and NAC-LWT

The U.S. Department of Energy’s (DOE’s) Used Fuel Disposition Campaign (UFDC) Program has transported high-burnup nuclear sister fuel rods from a commercial nuclear power plant for purposes of evaluation and testing. The evaluation and testing of high-burnup used nuclear fuel is integral to DOE initiatives to collect information useful in determining the integrity of fuel cladding for future safe transportation of the fuel, and for determining the effects of aging, on the integrity of UNF subjected to extended storage and subsequent transportation. The UFDC Program, in collaboration with the U.S. Nuclear Regulatory Commission and the commercial nuclear industry, has obtained individual used nuclear fuel rods for testing. The rods have been received at Oak Ridge National Laboratory (ORNL) for both separate effects testing (SET) and small-scale testing (SST). To meet the research objectives, testing on multiple 6 inch fuel rod pins cut from the rods at ORNL will be performed at Pacific Northwest National Laboratory (PNNL). Up to 10 rod equivalents will be shipped. Options were evaluated for multiple shipments using the 10-160B (based on 4.5 rod equivalents) and a single shipment using the NAC-LWT. Based on the original INL/Virginia Power transfer agreement, the rods are assumed to 152 inches in length with a 0.374-inch diameter. This report provides a preliminary content evaluation for use of the 10-160B and NAC-LWT for transporting those fuel rod pins from ORNL to PNNL. This report documents the acceptability of using these packagings to transport the fuel segments from ORNL to PNNL based on the following evaluations: enrichment, A2 evaluation, Pu-239 FGE evaluation, heat load, shielding (both gamma and neutron), and content weight/structural evaluation.

10-160B↗

Investigations on the Thermal-hydraulic Behavior of Accident Tolerant Fuel Cladding Materials

Since the 2011 Fukushima accident, significant research has been devoted to developing accident-tolerant fuel (ATF) cladding materials. These investigations have mostly focused on the ability to resist runaway steam oxidation and retain mechanical strength and structural integrity under thermal shocks. However, much remains unknown about the materials’ thermal-hydraulic behavior, particularly under light-water reactor (LWR) operating conditions. Two phenomena that determine safety margins in both normal and off-normal operating conditions - i.e., the critical heat flux (CHF) and Leidenfrost point (LFP) temperature - have not been investigated thoroughly for ATF materials. Surface properties, such as wettability and roughness, are known to influence pool and flow boiling CHF, as well as the LFP temperature. However, little is known about the surface wettability of ATF materials, particularly at LWR pressure and temperature. Little has been done on flow-boiling CHF and quenching heat transfer, especially for droplet quenching. Nonetheless, it is known that CHF in transient conditions, e.g., an exponentially escalating power transient, can be significantly different from that expected in steady-state operation. Very few studies have investigated transient CHF, either on ATF materials or under LWR pressure and temperature. The thorough understanding of transient CHF under prototypical reactor conditions will benefit not only the deployment of ATF but also the upcoming national efforts to study transient ATF behavior in the Transient Reactor Test Facility (TREAT) at Idaho National Laboratory. In summary, as a part of ATF development efforts, there is an urgent need to understand how and how much these materials may affect two-phase heat transfer phenomena in nuclear reactor conditions.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

Advanced synthesis for enhanced accident tolerant of LWR cladding materials

Advanced materials synthesis is utilized at Argonne National Laboratory (ANL) with the intended goal of improving performance of light water reactor (LWR) claddings under normal operation and accident conditions. The advanced synthesis utilizes atomic layer deposition (ALD) techniques to infiltrate SiC wires wrapped around ZIRLO tubes with SiC deposits, to form a SiC-SiC composite on the ZIRLO tubes. This paper reports on the effort to deposit SiC using ALD. The deposition was successful in infiltrating deep into the wires structure, reaching the surface of the ZIRLO tubes, as indicated through different characterization techniques. Because of the slow deposition rate of SiC, only a limited amount of SiC was deposited (a few hundreds of nm of SiC thick layers). This was followed by a few micrometers of ALD deposition of zircon (ZrSiO{sub 4}.) on top of the SiC deposition. The additional deposition was adequate to hold the wires together around the tube. Work is ongoing to increase the SiC ALD deposition rate, and infiltrate the larger pores within the wires with other SiC deposition methods such as low temperature chemical vapor deposition (CVD). (authors)

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

Fuel performance analysis of Cr-coated Zircaloy-4 cladding during a prototypical LOCA event using BISON

Here, deformation and failure of chromium (Cr) coated Zircaloy-4 (Zry-4) were studied in loss-of-coolant accident (LOCA) conditions using the BISON fuel performance code. The BISON validation model simulating Halden research reactor experiments was extended to include Cr coatings and higher rod internal pressures to simulate high-burnup fuel. The transient simulations show Cr coatings help relieve stress in the Zry-4 substrate during the transient, delaying the onset of high-temperature creep, which leads to ballooning and bursting of the cladding. A nominal Cr coating thickness of 30 µm delays clad failure by 26 seconds and increases the clad burst temperature by 40 K. A parametric study showed that time to failure and burst temperature both increase with coating thickness, and Cr-coated cladding offers burst resistance under a wide range of rod internal pressures simulating high-burnup fuel. Results indicate that a thin Cr coating provides resistance against ballooning and bursting of cladding during LOCA events.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

SiC MODIFICATIONS TO MELCOR FOR SEVERE ACCIDENT ANALYSIS APPLICATIONS

The Department of Energy (DOE) Office of Nuclear Energy (NE) Light Water Reactor (LWR) Sustainability Program encompasses strategic research focused on improving reactor core economics and safety margins through the development of an advanced fuel cladding system. The Fuels Pathway within this program focuses on fuel system components outside of the fuel pellet, allowing for alteration of the existing zirconium-based clad system through coatings, addition of ceramic sleeves, or complete replacement (e.g. fully ceramic cladding). The DOE-NE Fuel Cycle Research & Development (FCRD) Advanced Fuels Campaign (AFC) is also conducting research on materials for advanced, accident tolerant fuels and cladding for application in operating LWRs. To aide in this assessment, a silicon carbide (SiC) version of the MELCOR code was developed by substituting SiC in place of Zircaloy in MELCOR’s reactor core oxidation and material property routines. The purpose of this development effort is to provide a numerical capability for estimating the safety advantages of replacing Zr-alloy components in LWRs with SiC components. This modified version of the MELCOR code was applied to the Three Mile Island (TMI-2) plant accident. While the results are considered preliminary, SiC cladding showed a dramatic safety advantage over Zircaloy cladding during this accident.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Preliminary Simulations of Commercial Drying Cycles Using the Advanced Drying Cycle Simulator

The purpose of this report is to document updates on the apparatus to simulate commercial vacuum drying procedures at the Nuclear Energy Work Complex at Sandia National Laboratories. Validation of the extent of water removal in a dry spent nuclear fuel storage system based on drying procedures used at nuclear power plants is needed to close existing technical gaps. Operational conditions leading to incomplete drying may have potential impacts on the fuel, cladding, and other components in the system during subsequent storage and disposal. A general lack of data suitable for model validation of commercial nuclear canister drying processes necessitates well-designed investigations of drying process efficacy and water retention. Scaled tests that incorporate relevant physics and well-controlled boundary conditions are essential to provide insight and guidance to the simulation of prototypic systems undergoing drying processes. This report documents fiscal year 2023 (FY23) updates on the Advanced Drying Cycle Simulator (ADCS). This apparatus was built to simulate commercial drying procedures and quantify the amount of residual water remaining in a pressurized water reactor (PWR) fuel assembly after drying. The ADCS was constructed with a prototypic 17×17 PWR fuel skeleton and waterproof heater rods to simulate decay heat. These waterproof heaters are the next generation design to heater rods developed and tested at Sandia National Laboratories in FY20. In FY23, a series of four simulated commercial drying tests was completed. This report presents the temperature and pressure histories of the drying tests as well as axial temperature profiles that can be compared to data from the Electric Power Research Institute (EPRI) High Burnup Demonstration TN-32B cask. Water content measurements and dew point calculations from a Hiden Analytical HPR-30 mass spectrometer are also presented in this report. Due to familiarization with this first-of-a-kind system, refinements to equipment calibration and test procedures have been identified to better match commercial drying cycles for future simulated tests. However, the presented data demonstrate the successful construction and operation of a viable research platform for quantifying residual water content closely approaching that expected in dry storage canisters during commercial drying procedures.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗