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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 955 records · Page 53
All sourcesNASA NTRSDOE OSTI
NASA NTRS2003

Superior Ballistic Impact Resistance Achieved by the Co-Base Alloy Haynes 25

The fan case in a jet engine is required to contain a fan blade in the rare event of a blade loss during operation. Because of its function, the fan case is the largest structural component in high-bypass-ratio turbofan engines used in commercial aircraft. Therefore, the use of lighter and stronger materials would be advantageous in most engines and is practically a necessity in the latest generation of high-bypass engines. Small panels, 7 in. wide by 7 in. long, of a number of metallic alloys were impact tested at room temperature with a 0.50-caliber blunt-nose titanium alloy projectile at the NASA Glenn Research Center (ref. 1). These metallic systems included several high-strength aluminum (Al) alloys, Al-based laminates, aluminum metal matrix composites (Al-MMCs), nickel-base superalloys (Inconel 718 and 625), several titanium (Ti) alloys in different heat treated conditions, 304L stainless steel, a stainless-steel-based laminate, and a high strength steel (Nitronic 60). It was determined that a simple Co-base alloy (Haynes 25) had the best impact resistance on an areal weight basis. Haynes 25 was at least 10 percent better than IMI 550, the best titanium alloy tested to date, and it was far superior to other metals, especially at higher impact velocities (greater than 1100 ft/sec). Because this material could be ideal for fan containment applications in supersonic aircraft as a replacement for titanium, impact tests were also conducted at 371 oC and compared with results from alloys tested at elevated temperature under previous programs (i.e., Inconel 718, Ti-6242, M-152, Timetal 21S, and Aeromet 100). Although cobalt-base alloys are used in some high-temperature engine applications, to our knowledge they are not used in any containment systems. Advantages of cobalt over titanium include lower cost, easier processing, better high-temperature strength, and no fire hazard if tip rub occurs. Future plans include testing of lightweight sandwich panels with Haynes 25 as a core material in the form of a foam or lattice block structure and scaling up the current tests by using blade-simulating projectiles impacting large plates and half rings.

Hebsur, Mohan G.↗
DOE OSTI2020

Impact Response of Cold Spray Deposited Materials

Solid-state cold spraying (CS) of metals and respective blends is becoming increasingly attractive compared to conventional high temperature processes due to the unique properties such as increased yield strength, low ductility, and differences in tensile and compressive strengths that result from microstructural features due to the CS process. Here we report the results of plate impact experiments applied to CS deposits of tantalum (Ta), niobium (Nb), and a tantalum- niobium blend (TaNb). These methods allowed for definition of the Hugoniot for each material type and allowed for assessment of the Hugoniot Elastic Limit (HEL). Scanning electron microscopy was used on recovered samples to characterize the fracture mechanism during spallation.

36 MATERIALS SCIENCE↗
DOE OSTI2019

Influence of Rolling Temperature on the Mechanical Properties and Microstructure of Variable-Plane-Rolled Mg-3Al-1Zn Alloy

AZ31 magnesium alloy was produced via variable-plane rolling (VPR) under different temperatures. The effects of rolling temperature on the microstructure, texture and mechanical properties were investigated. A double-peak basal texture was formed during VPR treatment. Dynamic recrystallization (DRX) was observed during the VPR treatment, and it can reduce the texture intensity owing to the coalescence of sub-grains. Four types of twins were observed in the VPR treatment: {10-12} extension twins, {10-13}, {10-11} contraction twins and {10-11}-{10-12} double twins. The suitable temperature of AZ31 magnesium alloy for VPR treatment is determined as 623 K through experiments with tensile yield strength of 240 MPa, compressive yield strength of 162 MPa and elongation of 13%. Owing to the important impact of temperature on mechanical properties, the alloy was further VPRed with a decrease in temperature pass-by-pass. The high temperature of 623 K at the initial passes randomized the texture, which led to notably high ductility.

36 MATERIALS SCIENCE↗
DOE OSTI2017

Rapid assessment of crystal orientation in semi-crystalline polymer films using rotational zone annealing and impact of orientation on mechanical properties

Crystal orientation in semi-crystalline polymers tends to enhance their performance, such as increased yield strength and modulus, along the orientation direction. Zone annealing (ZA) orients the crystal lamellae through a sharp temperature gradient that effectively directs the crystal growth, but the sweep rate (V ZA ) of this gradient significantly impacts the extent of crystal orientation. Here in this work, we demonstrate rotational zone annealing (RZA) as an efficient method to elucidate the influence of V ZA on the crystal morphology of thin films in a single experiment using isotactic poly(1-butene), PB-1, as a model semi-crystalline polymer. These RZA results are confirmed using standard, serial linear ZA to tune the structure from an almost unidirectional oriented morphology to weakly oriented spherulites. The overall crystallinity is only modestly changed in comparison to isothermal crystallization (maximum of 55% from ZA vs. 48% for isothermal crystallization). However, the average grain size increases and the spherulites become anisotropic from ZA. Due to these structural changes, the Young's modulus of the oriented films, both parallel and perpendicular to the spherulite orientation direction, is significantly increased by ZA. The modulus does become anisotropic after ZA due to the directionality in the crystal structure, with more than a threefold increase in the modulus parallel to the orientation direction for the highest oriented film in comparison to the modulus from isothermal crystallization. Lastly, RZA enables rapid identification of conditions to maximize orientation of crystals in thin polymer films, which could find utility in determining conditions to improve crystallinity and performance in organic electronics.

36 MATERIALS SCIENCE↗
DOE OSTI2017

Spall damage of a Ta particle-reinforced metallic glass matrix composite under high strain rate loading

We investigate deformation and damage of a Zr-based bulk metallic glass (BMG) and its Ta particle-reinforced composite (MGMC) under impact loading, as well as quasi-static tension for comparison. Yield strength, spall strength, and damage accumulation rate are obtained from free-surface velocity histories, and MGMC appears to be more damage-resistant. Scanning electron microscopy, electron back scattering diffraction and x-ray computed tomography, are utilized for characterizing microstructures, which show features consistent with macroscopic measurements. Different damage and fracture modes are observed for BMG and MGMC. Multiple well-defined spall planes are observed in BMG, while isolated and scattered cracking around reinforced particles dominates fracture of MGMC. Particle–matrix interface serves as the source and barrier to crack nucleation and propagation under both quasi-static and impact loading. Finally, deformation twinning and grain refinement play a key role in plastic deformation during shock loading but not in quasi-static loading. In addition, 3D cup-cone structures are resolved in BMG, but not in MGMC due to its heterogeneous stress field.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Alternative PWHT to Improve High-Temperature Mechanical Properties of Advanced 9Cr Steel Welds

Creep-resistant 9Cr steels are extremely important in thermal power generation industry due to their marked resistance to creep and corrosion. The weldability of these alloys is critical since they are used in welded construction equipment. The required mechanical properties are achieved after post-weld heat treatment. This study examined the effect of different post-weld heat treatments on microstructure and mechanical properties of creep strength-enhanced 9Cr steel welding deposits. It was obtained with an experimental flux-cored arc welding wire used under protective gas (Ar-20% CO{sub 2}). The heat treatments used were: (1) tempering (760 °C × 2 h), (2) solubilizing (1050 °C × 1 h) + tempering (760 °C × 2 h) and (3) solubilizing (1150 °C × 1 h) + first tempering (660 °C × 3 h) + second tempering (660 °C × 3 h). All-weld metal chemical composition was analyzed, and hot tensile tests were carried out at different temperatures. Charpy-V impact tests and Vickers microhardness measurements were also performed. Microstructures were studied using x-ray diffraction and optical and scanning electron microscopy. In all cases, a martensitic matrix with intergranular and intra-granular precipitates was detected. In the as-welded condition, δ-ferrite was also found. Microhardness dropped, and the impact energy increased with post-weld heat treatments. The highest hot tensile strength result was achieved with samples submitted to austenization at 1150 °C and double tempering at 660 °C.

36 MATERIALS SCIENCE↗
NASA NTRS1975

Improving the toughness of refractory compounds

Composition and processing studies were conducted on silicon nitride and silicon carbide materials. Charpy mode impact testing to 2415 F established the effectiveness of higher purity silicon nitride powder sources in reducing the scatter of measurements and in improving short time bend strengths as well as bend stress rupture properties. Stabilized zirconia additions in particular were observed to dramatically enhance low and high temperature bend strengths and stress rupture properties for all grades of silicon nitride powder. Silicon carbide samples showed relatively poor impact resistance, although the maxima in stress rupture behavior was exhibited by this material.

Vasilos, T.↗
DOE OSTI2021

Dynamic Strength of Copper at High Pressures Using Pressure Shear Plate Experiments

Measurement of strength at high pressures is critical to understanding the behavior of materials subjected to extreme loading conditions. Recent developments have extended the pressure shear plate impact (PSPI) technique to the high-pressure regime. Such experiments provide a unique opportunity to extract the complete stress-strain behavior of materials at relatively high pressures. The modified technique includes a new fiber-optic heterodyne transverse velocity interferometer system and new analysis methods to account for the inelastic response of the anvil plates. In this study, PSPI experiments are conducted on oxygen-free high conductivity (OFHC) copper at pressures ranging from 10 to 43 GPa and at strain rates of ~10 5 s -1 . Complete stress-strain curves of copper are obtained using a hybrid methodology that relies on numerical simulations and particle velocity records gathered in these experiments. Experiments are conducted at similar pressures and strain rates using two types of anvils that undergo different levels of plastic strains: tool steel and tungsten carbide, to check the robustness of the hybrid method. The behavior of copper at these high pressures and strain rates is compared with previous literature data, and the effect of pressure and strain rate on the strength behavior of copper are discussed. Here, it was observed that the rate of change in yield strength change in pressure was 2.5 times the rate of change of shear modulus with pressure. The strength models that predict the response of copper at these extreme conditions are also examined and validated.

36 MATERIALS SCIENCE↗
NASA NTRS2018

Extratropical Cyclone Precipitation Life Cycles: A Satellite-Based Analysis

Although extratropical cyclones are the most common midlatitude storms, the relationship between their precipitation life cycle and dynamical strength life cycle has not been thoroughly analyzed. Given that thermodynamic heat exchanges associated with precipitation impact cyclone circulation, there is a need to understand the precipitation/dynamics relationship. Based on Integrated MultisatellitE Retrievals for Global Precipitation MeasurementGPM precipitation and Lagrangian cyclone tracks, the precipitation maximum occurs prior to the dynamical strength maximum 70% of the time. The lag in timing is consistent with the difference in cyclone precipitable water vapor at the two peaks. Conditional subsetting of the cyclone composites shows that if the precipitable water vapor distribution is constrained to be equal throughout the composite life cycle, the precipitation peak occurs very near the time of the peak in cyclone dynamical strength. Thus, the boost in dynamical strength caused by latent heat associated with precipitation manifest itself with little to no time lag.

Extratropical cyclone↗
DOE OSTI2018

Development of castable nanostructured alloys as a new generation RAFM steels

Castable nanostructured alloys (CNAs) are being developed as a new generation of reduced-activation ferritic-martensitic (RAFM) steels to overcome certain limitations of the current RAFM steels, such as their narrow operating temperature range and associated low strength at high temperatures. Six CNAs were developed and examined, exhibiting noticeably increased yield strength, tensile strength and creep resistance as compared to the current RAFM steels, which are comparable to ODS-Eurofer (0.3% Y 2 O 3 ) at 650 °C. The enhanced strength of CNAs is also associated with a beneficial increase in Charpy impact upper-shelf energies, up to ~2.5 times that of the current RAFM steels, with comparable ductile-brittle transition temperatures. Furthermore, a broad analysis of microstructure, alloy chemistry and grain size analyses clearly support the mechanisms that explain the mechanical property improvements of these CNAs, providing essential insight for further development of advanced RAFM steels to meet the challenges of future fusion reactors.

36 MATERIALS SCIENCE↗
NASA NTRS1980

Recent developments in the design, testing and impact-damage tolerance of stiffened composite panels

The structural technology of laminated filamentary-composite stiffened-panel structures under combined in-plane and lateral loadings is discussed. Emphasis is on analyzing the behavior of the structures under load, determining appropriate structural proportions for weight efficient configurations, and effects of impact damage and geometric imperfections on structural performance. Experimental data on buckling of panels under in-plane compression validate the analysis and sizing methods, and illustrate structural performance and efficiency obtained from representative structures. It is shown that the strength of panels under in-plane compression can be degraded by low-velocity impact damage, and data are presented which indicate that the matrix is a significant factor influencing tolerance to impact damage.

Williams, J. G.↗
NASA NTRS2013

Experimental and Analytical Characterization of the Macromechanical Response for Triaxial Braided Composite Materials

Increasingly, carbon composite structures are being used in aerospace applications. Their highstrength, high-stiffness, and low-weight properties make them good candidates for replacing many aerospace structures currently made of aluminum or steel. Recently, many of the aircraft engine manufacturers have developed new commercial jet engines that will use composite fan cases. Instead of using traditional composite layup techniques, these new fan cases will use a triaxially braided pattern, which improves case performance. The impact characteristics of composite materials for jet engine fan case applications have been an important research topic because Federal regulations require that an engine case be able to contain a blade and blade fragments during an engine blade-out event. Once the impact characteristics of these triaxial braided materials become known, computer models can be developed to simulate a jet engine blade-out event, thus reducing cost and time in the development of these composite jet engine cases. The two main problems that have arisen in this area of research are that the properties for these materials have not been fully determined and computationally efficient computer models, which incorporate much of the microscale deformation and failure mechanisms, are not available. The research reported herein addresses some of the deficiencies present in previous research regarding these triaxial braided composite materials. The current research develops new techniques to accurately quantify the material properties of the triaxial braided composite materials. New test methods are developed for the polymer resin composite constituent and representative composite coupons. These methods expand previous research by using novel specimen designs along with using a noncontact measuring system that is also capable of identifying and quantifying many of the microscale failure mechanisms present in the materials. Finally, using the data gathered, a new hybrid micromacromechanical computer model is created to simulate the behavior of these composite material systems under static and ballistic impact loading using the test data acquired. The model also quantifies the way in which the fiber/matrix interface affects material response under static and impact loading. The results show that the test methods are capable of accurately quantifying the polymer resin under a variety of strain rates and temperature for three loading conditions. The resin strength and stiffness data show a clear rate and temperature dependence. The data also show the hydrostatic stress effects and hysteresis, all of which can be used by researchers developing composite constitutive models for the resins. The results for the composite data reveal noticeable differences in strength, failure strain, and stiffness in the different material systems presented. The investigations into the microscale failure mechanisms provide information about the nature of the different material system behaviors. Finally, the developed computer model predicts composite static strength and stiffness to within 10 percent of the gathered test data and also agrees with composite impact data, where available.

Littell, Justin D.↗
NASA NTRS1982

Effects of fiber/matrix interactions on the properties of graphite/epoxy composites

A state-of-the-art literature review of the interactions between fibers and resin within graphite epoxy composite materials was performed. Emphasis centered on: adhesion theory; wetting characteristics of carbon fiber; load transfer mechanisms; methods to evaluate and measure interfacial bond strengths; environmental influence at the interface; and the effect of the interface/interphase on composite performance, with particular attention to impact toughness. In conjunction with the literature review, efforts were made to design experiments to study the wetting behavior of carbon fibers with various finish variants and their effect on adhesion joint strength. The properties of composites with various fiber finishes were measured and compared to the base-line properties of a control. It was shown that by tailoring the interphase properties, a 30% increase in impact toughness was achieved without loss of mechanical properties at both room and elevated temperatures.

Mcmahon, P. E.↗
DOE OSTI2022

Powder Metallurgy HIP Process Study and Mechanical Property Evaluations for IN740H

The effects of hot isostatic pressing (HIP) parameters and powder size distribution (PSD) on the resulting microstructure and properties of powder metallurgy (P/M) IN740H have been investigated. Properties can be substantially tailored through the appropriate management of these parameters. Applying a thermal presoak to the input powder prior to the sintering stage of HIP can significantly increase average grain size and coarse grain fraction, enabling a trade for improved creep resistance at the expense of tensile strength. Here, powder thermal presoak was found to have a larger impact on microstructure and properties than the use of a coarser PSD alone. Additionally, substantial grain growth and grain boundary migration is observed in P/M IN740H at HIP temperatures above 1260°C. Given its inherently finer grain size, P/M HIP IN740H typically outperforms its cast and wrought counterparts in tensile response. Creep life at 700–800°C was inferior to wrought due to PPBs coincident with grain boundaries which served as cavity nucleation sites, leading to lower creep ductility. The ability to adjust the microstructure toward a more balanced creep and tensile behavior allows P/M HIP IN740H to be considered for high-temperature applications in advanced ultra-supercritical steam and supercritical carbon dioxide power cycles.

36 MATERIALS SCIENCE↗
DOE OSTI2022

The role of information structures in game-theoretic multi-agent learning

Multi-agent learning (MAL) studies how agents learn to behave optimally and adaptively from their experience when interacting with other agents in dynamic environments. The outcome of a MAL process is jointly determined by all agents’ decision-making. Hence, each agent needs to think strategically about others’ sequential moves, when planning future actions. The strategic interactions among agents makes MAL go beyond the direct extension of single-agent learning to multiple agents. With the strategic thinking, each agent aims to build a subjective model of others decision-making using its observations. Such modeling is directly influenced by agents’ perception during the learning process, which is called the information structure of the agent’s learning. As it determines the input to MAL processes, information structures play a significant role in the learning mechanisms of the agents. This review creates a taxonomy of MAL and establishes a unified and systematic way to understand MAL from the perspective of information structures. Here we define three fundamental components of MAL: the information structure (i.e., what the agent can observe), the belief generation (i.e., how the agent forms a belief about others based on the observations), as well as the policy generation (i.e., how the agent generates its policy based on its belief). In addition, this taxonomy enables the classification of a wide range of state-of-the-art algorithms into four categories based on the belief-generation mechanisms of the opponents, including stationary, conjectured, calibrated, and sophisticated opponents. We introduce Value of Information (VoI) as a metric to quantify the impact of different information structures on MAL. Finally, we discuss the strengths and limitations of algorithms from different categories and point to promising avenues of future research.

97 MATHEMATICS AND COMPUTING↗
DOE OSTI2019

Coal-Filler-Based Thermoplastic Composites as Construction Materials: A New Sustainable End-Use Application

This paper investigates coal’s viability as an alternative filler to wood flour in Wood Plastic Composites (WPCs) – a class of materials used in building applications in lieu of pressure-treated wood. Coal Plastic Composites (CPCs) were fabricat-ed with 15 – 60 wt.% coal combined with high density polyethylene and their physical (mechanical, water absorption and metal leaching) and chemical (oxidative degradation and flammability) properties were compared with commercial WPCs. In addition, mass and energy balances (10 tonne/hr basis) and life cycle analyses (60 wt.% filler and 1 tonne ba-sis) were conducted on CPCs and WPCs to assess environmental impact during manufacturing. At 60 wt.%, CPCs had a higher flexural strength, slower oxidative degradation and burn rate, and lower water absorption in comparison to com-mercial WPCs, suggesting better performance and stability in building applications. Furthermore, CPC manufacturing showed 44% lower greenhouse gas emissions and 62% less energy usage in comparison with WPC. These results indi-cate that direct utilization of coal as a filler in construction composite applications may yield lower cost products with lower associated emissions and energy demand compared to existing WPC materials, potentially yielding a more sustain-able end-use for coal than current uses such as power production.

Coal Plastic Composites, Wood Plastic Composites, ↗
DOE OSTI2015

Tensile behavior of laser treated Fe-Si-B metallic glass

Fe-Si-B metallic glass foils were treated with a linear laser track using a continuous wave Nd-YAG laser and its effect on the overall tensile behavior was investigated. Microstructure and phase evolutions were evaluated using X-ray diffraction, resistivity measurements, and transmission electron microscopy. Crystallization fraction was estimated via the differential scanning calorimetry technique. Metallic glass foils treated with the lower laser fluences (<0.49 J/mm{sup 2}) experienced structural relaxation, whereas higher laser fluences led to crystallization within the laser treated region. The overall tensile behavior was least impacted by structural relaxation, whereas crystallization severely reduced the ultimate tensile strength of the laser treated metallic glass foils.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Predicting metal–metal interactions. I. The influence of strain on nanoparticle and metal adlayer stabilities

Strain-engineering of bimetallic nanomaterials is an important design strategy for developing new catalysts. In this paper, we introduce an approach for including strain effects into a recently introduced, density functional theory (DFT)-based alloy stability model. The model predicts adsorption site stabilities in nanoparticles and connects these site stabilities with catalytic reactivity and selectivity. Strain-based dependencies will increase the model’s accuracy for nanoparticles affected by finite-size effects. In addition to the stability of small nanoparticles, strain also influences the heat of adsorption of epitaxially grown metal-on-metal adlayers. In this respect, we successfully benchmark the strain-including alloy stability model with previous experimentally determined trends in the heats of adsorption of Au and Cu adlayers on Pt (111). For these systems, our model predicts stronger bimetallic interactions in the first monolayer than monometallic interactions in the second monolayer. We explicitly quantify the interplay between destabilizing strain effects and the energy gained by forming new metal–metal bonds. While tensile strain in the first Cu monolayer significantly destabilizes the adsorption strength, compressive strain in the first Au monolayer has a minimal impact on the heat of adsorption. Hence, this study introduces and, by comparison with previous experiments, validates an efficient DFT-based approach for strain-engineering the stability, and, in turn, the catalytic performance, of active sites in bimetallic alloys with atomic level resolution.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗