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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 991 records · Page 55
All sourcesNASA NTRSDOE OSTI
NASA NTRS1981

Calibration of a gamma-ray telescope using tagged position annihilation photons

Measurements of detection efficiency, angular resolution, and energy resolution properties of a gamma ray telescope used to study celestial gamma rays from balloon flight altitudes are described. Nearly monochromatic photons produced at the National Bureau of Standards tagged photon facility were used for the calibration. Details of the photon beam configuration and properties and results of the measurements made at photon energies of 15.1 and 31.1 MeV are presented. Finally, the data are compared with a Monte Carlo analysis of the instrument properties.

Bertsch, D. L.↗
DOE OSTI2020

Application of Generalized Standard Addition Method and Ultraviolet Spectroscopy to Quantify Electrolytic Depolymerization of Lignin

Industrial lignin waste is an important byproduct of bio-refineries and the paper industry. Depolymerization of this industrial lignin could generate useful aromatic compounds. This group has focused on electrolytic decomposition of biorefinery lignin. To quantify electrolytic decomposition of the lignin in a highly caustic solution, ultraviolet (UV) spectroscopy provides a useful probe. The conversion of the neat lignin to the oxidized products achieved by the electrolytic reactor may be measured by quantifying the amount of unreacted neat lignin that remains in the effluent. Because the properties of electrolytic decomposition products are largely unknown, a useful approach to quantify decomposition of the neat lignin is to use a multivariate calibration method referred to as the generalized standard addition method (GSAM). In this approach, the electrolytic decomposition products represent a background interference and the neat lignin that remains can be quantified. Furthermore, this approach allows the conversion of the neat lignin to be calculated in a solution that is a complex mixture.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2024

Improving gas adsorption modeling for MOFs by local calibration of Hubbard U parameters

While computational screening with density functional theory (DFT) is frequently employed for the screening of metal–organic frameworks (MOFs) for gas separation and storage, commonly applied generalized gradient approximations (GGAs) exhibit self-interaction errors, which hinder the predictions of adsorption energies. We investigate the Hubbard U parameter to augment DFT calculations for full periodic MOFs, targeting a more precise modeling of gas molecule–MOF interactions, specifically for N2, CO2, and O2. We introduce a calibration scheme for the U parameter, which is tailored for each MOF, by leveraging higher-level calculations on the secondary building unit (SBU) of the MOF. When applied to the full periodic MOF, the U parameter calibrated against hybrid HSE06 calculations of SBUs successfully reproduces hybrid-quality calculations of the adsorption energy of the periodic MOF. The mean absolute deviation of adsorption energies reduces from 0.13 eV for a standard GGA treatment to 0.06 eV with the calibrated U, demonstrating the utility of the calibration procedure when applied to the full MOF structure. Furthermore, attempting to use coupled cluster singles and doubles with perturbative triples calculations of isolated SBUs for this calibration procedure shows varying degrees of success in predicting the experimental heat of adsorption. It improves accuracy for N2 adsorption for cases of overbinding, whereas its impact on CO2 is minimal, and ambiguities in spin state assignment hinder consistent improvements of O2 adsorption. Our findings emphasize the limitations of cluster models and advocate the use of full periodic MOF systems with a calibrated U parameter, providing a more comprehensive understanding of gas adsorption in MOFs.

Chemistry↗
NASA NTRS1975

Strain-gage bridge calibration and flight loads measurements on a low-aspect-ratio thin wing

Strain-gage bridges were used to make in-flight measurements of bending moment, shear, and torque loads on a low-aspect-ratio, thin, swept wing having a full depth honeycomb sandwich type structure. Standard regression analysis techniques were employed in the calibration of the strain bridges. Comparison of the measured loads with theoretical loads are included.

Peele, E. L.↗
DOE OSTI2024

Reduced-dimension Bayesian optimization for model calibration of transient vapor compression cycles

Development and calibration of first-principles dynamic models of vapor compression cycles (VCCs) is of critical importance for applications that include control design and fault detection and diagnostics. Nevertheless, the inherent complexity of models that are represented by large systems of differential–algebraic equations leads to significant challenges for model calibration processes that utilize classical gradient-based methods. Bayesian optimization (BO) is a sample-efficient and gradient-free approach using a probabilistic surrogate model and optimal search over a feasible parameter space. Despite the benefits of BO in reducing computational costs, challenges remain in dealing with a high-dimensional calibration task resulting from a large set of parameters that have significant impacts on system behavior and need to be calibrated simultaneously. This paper presents a reduced-dimension BO framework for calibrating transient VCCs models where the calibration space is projected to a low-dimensional subspace for accelerating convergence of the solution algorithm and consequently reducing the number of transient simulations. The proposed approach was demonstrated via two case studies associated with different VCC applications where 10 parameters were calibrated in each case using laboratory measurements. The reduced-dimension BO framework only required 1 / 8 th of the iterations associated with a standard BO method that deals with high-dimensional calibration parameters for converged solutions and yielded comparable accuracy. Furthermore, both calibrated models revealed significant accuracy improvements compared to uncalibrated models.

Ma, Jiacheng↗
NASA NTRS1978

Results of the 1974 through 1977 NASA/JPL balloon flight solar cell calibration program

From 1974 through 1977, seven solar cell calibration flights and two R&D flights with a spectroradiometer as a payload were attempted. There were two R&D flights, and one calibration flight that failed. Each calibration flight balloon was designed to carry its payload to an altitude of 36.6 km (120 kft). The R&D flight balloons were designed for a payload altitude of 47.5 km (150 kft). At the end of the flight period, the upper (solar cell calibration system) and lower (consolidated instrument package (DIP) payloads were separated from the balloon and descend via parachutes. The calibrated solar cells recovered in this manner were used as primary intensity reference standards during solar simulator testing of solar cells and solar arrays with similar spectral response characteristics. This method of calibration has become the most widely accepted technique for developing space standard solar cells.

Sidwell, L. B.↗
DOE OSTI2015

A calibration of NICMOS Camera 2 for low count rates

NICMOS 2 observations are crucial for constraining distances to most of the existing sample of z>1 SNe Ia. Unlike conventional calibration programs, these observations involve long exposure times and low count rates. Reciprocity failure is known to exist in HgCdTe devices and a correction for this effect has already been implemented for high and medium count rates. However, observations at faint count rates rely on extrapolations. Here instead, we provide a new zero-point calibration directly applicable to faint sources. This is obtained via inter-calibration of NIC2 F110W/F160W with the Wide Field Camera 3 (WFC3) in the low count-rate regime using z∼1 elliptical galaxies as tertiary calibrators. These objects have relatively simple near-IR spectral energy distributions, uniform colors, and their extended nature gives a superior signal-to-noise ratio at the same count rate than would stars. The use of extended objects also allows greater tolerances on point-spread function profiles. We find space telescope magnitude zero points (after the installation of the NICMOS cooling system, NCS) of 25.296 ±0.022 for F110W and 25.803 ±0.023 for F160W, both in agreement with the calibration extrapolated from count rates ≳1000 times larger (25.262 and 25.799). Before the installation of the NCS, we find 24.843 ±0.025 for F110W and 25.498 ±0.021 for F160W, also in agreement with the high-count-rate calibration (24.815 and 25.470). We also check the standard bandpasses of WFC3 and NICMOS 2 using a range of stars and galaxies at different colors and find mild tension for WFC3, limiting the accuracy of the zero points. To avoid human bias, our cross-calibration was “blinded” in that the fitted zero-point differences were hidden until the analysis was finalized.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2017

Radiochemical Methodology Applied To Determination of gamma-Emitting Radionuclides In Waste Samples From IEA-R1 Reactor - 17265

The Brazilian reactor IEA-R1 has been in operation since 1957. It is an open pool-type nuclear research reactor, operating at 2 to 5 MW that uses water as coolant, moderator and biological shield. Polypropylene filter cartridges are part of the water treatment system of the reactor and become radioactive as they remove suspended solid material from the cooling water during the operation of the reactor. Annually, the replacement of the filters from the reactor's water treatment system generates about 36 units. The development of a method for the characterization of the radionuclides present in the filters is required for routine operation in the Radioactive Waste Management Facility (RWMF) in order to determine the radioisotopic inventory of the waste packages. Wastes from nuclear reactors contain transuranic elements, activation and fission products, only few of them emitting gamma radiation measurable by simple gamma scanning methods. The method of the Scaling Factors (SF) uses empirically determined proportions between the concentrations of Difficult to Measure (DTM) radionuclides and that of easily measurable gamma emitters called Key Nuclide (KN), to calculate DTM concentrations. The objective of this study is to describe a method of the dissolution of the filter cartridges for determination of gamma emitting radionuclides. To determine the activity of a sample by means of of gamma spectrometry, it is necessary previous knowledge of the efficiency curve for a given geometry, which can be obtained by calibrating the efficiency and energy of the detector. The need to dissolve the filter cartridges has arisen given the difficulty in obtaining a standard source with the same filter geometry. Therefore, for this work, the calibration curve was constructed using a mixed gamma-ray standard with known activities, same geometry, density, physical state and chemical composition of the source to be analyzed. A sample with background count (BG) was prepared and analyzed under the same conditions as the samples and the result was subtracted from the results obtained for each filter sample. After many tests, it was possible to establish a method for the dissolution of filter cartridges for the determination of gamma-emitting radionuclides. A mixed gamma-ray standard was produced in liquid form, containing the following radionuclides: {sup 241}Am, {sup 137}Cs and {sup 60}Co, which have photo-peaks at the following energies: 59.54, 661.66 and 1332.49 keV, respectively. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
NASA NTRSDate not supplied

TPSAS-NF1676L-19788-DND

The calibration of the historical AVHRR visible channels has always been hindered by the degrading NOAA satellite orbits. The complete AVHRR record spans over three decades making it useful for cloud, aerosol, and land use climate studies. Studies that monitor long-term changes in these properties require climate quality calibration. The AVHRR sensors do not have any onboard visible calibration, unlike the IR channels. Many AVHRR post-launch calibration methods have been published. Some of these are based on the pseudo invariant targets such as desert and polar ice and others employ direct calibration transfer from a well-calibrated sensor such as MODIS. Most historical studies only employed only one method and reconciling calibration differences from multiple studies was difficult. This study employs multiple calibration approaches, which are then merged according to their individual uncertainty. Since the visible spectral response functions are similar across AVHRR sensor and that the morning and afternoon orbits usually degrade in the same manner, an afternoon and morning orbiter during the MODIS era is chosen as the reference AVHRR sensor. The reference AVHRR sensor is inter-calibrated with the Aqua-MODIS Collection 6 standard using simultaneous nadir overpass (SNO) radiance pairs. Three pseudo invariant target approaches are utilized, deserts, polar ice and deep convective clouds. These sites are characterized using reference AVHRR reflectances as a function of solar zenith angle. The multiple calibration approach is then validated with non-reference AVHRR sensor during the MODIS era, using AVHRR and MODIS SNO measurements. For historical AVHRR satellite having consistent calibration across invariant targets then validates the approach. This calibration effort is in sponsored by the NOAA CDR program to provide climate quality visible calibration coefficients to the remote sensing community. Each of the calibration approaches are unique and when utilized in tandem can accurately calibrate the AVHRR record. AVHRR calibration methods cannot rely on repeatable annual orbits for calibration model development. Inconsistent results prompt code and invariant target examinations that cannot be determined using only single method approaches. Results from this study will be presented at the meeting.

David Doelling↗
NASA NTRS2007

A Comprehensive Plan for the Long-Term Calibration and Validation of Oceanic Biogeochemical Satellite Data

The primary objective of this planning document is to establish a long-term capability and validating oceanic biogeochemical satellite data. It is a pragmatic solution to a practical problem based primarily o the lessons learned from prior satellite missions. All of the plan's elements are seen to be interdependent, so a horizontal organizational scheme is anticipated wherein the overall leadership comes from the NASA Ocean Biology and Biogeochemistry (OBB) Program Manager and the entire enterprise is split into two components of equal sature: calibration and validation plus satellite data processing. The detailed elements of the activity are based on the basic tasks of the two main components plus the current objectives of the Carbon Cycle and Ecosystems Roadmap. The former is distinguished by an internal core set of responsibilities and the latter is facilitated through an external connecting-core ring of competed or contracted activities. The core elements for the calibration and validation component include a) publish protocols and performance metrics; b) verify uncertainty budgets; c) manage the development and evaluation of instrumentation; and d) coordinate international partnerships. The core elements for the satellite data processing component are e) process and reprocess multisensor data; f) acquire, distribute, and archive data products; and g) implement new data products. Both components have shared responsibilities for initializing and temporally monitoring satellite calibration. Connecting-core elements include (but are not restricted to) atmospheric correction and characterization, standards and traceability, instrument and analysis round robins, field campaigns and vicarious calibration sites, in situ database, bio-optical algorithm (and product) validation, satellite characterization and vicarious calibration, and image processing software. The plan also includes an accountability process, creating a Calibration and Validation Team (to help manage the activity), and a discussion of issues associated with the plan's scientific focus.

Hooker, Stanford B.↗
NASA NTRS2011

The Physical Conditions of a Lensed Star-Forming Galaxy at Z=1.7

We report rest-frame optical Keck/NIRSPEC spectroscopy of the brightest lensed galaxy yet discovered, RCSGA 032727-132609 at z=1.7037. From precise measurements of the nebular lines, we infer a number of physical properties: redshift ' extinction, star formation rate ' ionization parameter, electron density, electron temperature, oxygen abundance, and N/O, Ne/O, and Ar/O abundance ratios, The limit on [O III] 4363 A tightly constrains the oxygen abundance via the "direct" or Te method, for the first time in an average-metallicity galaxy at z approx.2. We compare this result to several standard "bright-line" O abundance diagnostics, thereby testing these empirically-calibrated diagnostics in situ. Finally, we explore the positions of lensed and unlensed galaxies in standard diagnostic diagrams, to explore the diversity of ionization conditions and mass-metallicity ratios at z=2.

Rigby, Jane↗
DOE OSTI2025

Sparge Sampling of Molten Salts for Online Monitoring via Laser-Induced Breakdown Spectroscopy

A method was developed to sample molten salts by sparging to generate and transport aerosols to an isolated instrument for compositional analysis by laser-induced breakdown spectroscopy (LIBS). Real-time monitoring of molten salt composition is critical to developing molten salt nuclear reactors, which offer enhanced safety and efficiency. In this article, the sparge sampling method is described and compared with sampling using a Collison nebulizer. The size distribution and transport of aerosols produced from molten eutectic NaNO 3 –KNO 3 salt were compared for multiple gas flow rates (75–1200 mL min –1 ) and transport distances (0.68–2.61 m). Both methods produced aerosols ranging from 0.5 to 5.0 μm determined using a cascade impactor. Aerosols were effectively transported without pre- or trace-heating of gas lines, but transport efficiency was reduced by the formation of agglomerates. Sparge sampling was found to use less sample and less gas than a Collison nebulizer while producing a more concentrated aerosol stream (up to 5 μg L –1 ). The effects of laser energy and delay time on the signal quality of LIBS measurements of these aerosols were also studied. High energy and short delay times were found to enhance signal and repeatability, whereas signal-to-background and signal-to-noise ratios were highest at low energy and longer delay times. The capabilities of this system for online monitoring of molten salts were demonstrated with calibrations for Sr and Li with relative standard deviations of 2.6% and 1.5% and limits of detection of 380 and 180 μg g –1 , respectively.

Aerosols↗
NASA NTRS1996

On the Accurate Calibration of the SeaWinds Radar Antenna: A Cylindrical Near-Field Measurement Approach

This paper demonstrates the utility of a cylindrical near-field measurement approach for the SeaWinds radar antenna calibration. Both generalized measurement error models and measured tests on a standard gain horn and NASA Scatterometer instrument antenna have been performed to achieve and verify the desired calibration accuracy. A comparison between far-field measured data and those obtained from cylindrical near-field measurements was found in excellent agreement.

spaceborne↗
DOE OSTI2015

Experimental approaches for the development of gamma spectroscopy well logging system

This article discusses experimental approaches for the development of gamma spectroscopy well logging system. Considering the size of borehole sonde, we customize 2 x 2 inches inorganic scintillators and the system including high voltage, preamplifier, amplifier and multichannel analyzer (MCA). The calibration chart is made by test using standard radioactive sources so that the measured count rates are expressed by energy spectrum. Optimum high-voltage supplies and the measurement parameters of each detector are set up by experimental investigation. Also, the responses of scintillation detectors have been examined by analysis according to the distance between source and detector. Because gamma spectroscopy well logging needs broad spectrum, high sensitivity and resolution, the energy resolution and sensitivity as a function of gamma ray energy are investigated by analyzing the gamma ray activities of the radioactive sources.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
DOE OSTI2014

MO-G-17A-09: Quantitative Autoradiography of Biopsy Specimens Extracted Under PET/CT Guidance

Purpose: To develop a procedure for accurate determination of PET tracer concentration with high spatial accuracy in situ by performing Quantitative Autoradiography of Biopsy Specimens (QABS) extracted under PET/CT guidance. Methods: Autoradiography (ARG) standards were produced from a gel loaded with a known concentration of FDG biopsied with 18G and 20G biopsy needles. Specimens obtained with these needles are generally cylindrical: up to 18 mm in length and about 0.8 and 0.6 mm in diameter respectively. These standards, with similar shape and density as biopsy specimens were used to generate ARG calibration curves.Quantitative ARG was performed to measure the activity concentration in biopsy specimens extracted from ten patients. The biopsy sites were determined according to PET/CT's obtained in the operating room. Additional CT scans were acquired with the needles in place to confirm correct needle placements. The ARG images were aligned with the needle tip in the PET/CT images using the open source CERR software. The mean SUV calculated from the specimen activities (SUVarg) were compared to that from PET (SUVpet) at the needle locations. Results: Calibration curves show that the relation between ARG signal and activity concentration in those standards is linear for the investigated range (up to 150 kBq/ml). The correlation coefficient of SUVarg with SUVpet is 0.74. Discrepancies between SUVarg and SUVpet can be attributed to the small size of the biopsy specimens compared to PET resolution. Conclusion: The calibration procedure using surrogate biopsy specimens provided a method for quantifying the activity within the biopsy cores obtained under FDG-PET guidance. QABS allows mapping the activity concentration in such biopsy specimens with a resolution of about 1mm. QABS is a promising tool for verification of biopsy adequacy by comparing specimen activity to that expected from the PET image. A portion of this research was funded by a research grant from Biospace Lab, 13 rue Georges Auric 75019 Paris, FRANCE.

62 RADIOLOGY AND NUCLEAR MEDICINE↗
NASA NTRS1991

Cryogenic radiometers and intensity-stabilized lasers for Eos radiometric calibrations

Liquid helium-cooled electrical substitution radiometers (ESRs) provide irradiance standards with demonstrated absolute accuracy at the 0.01 percent level, spectrally flat response between the UV and IR, and sensitivity down to 0.1 nW/sq cm. We describe an automated system developed for NASA - Goddard Space Flight Center, consisting of a cryogenic ESR illuminated by servocontrolled laser beams. This system is designed to provide calibration of single-element and array detectors over the spectral range between 257nm in the UV to 10.6 microns in the IR. We also describe a cryogenic ESR optimized for black body calibrations that has been installed at NIST, and another that is under construction for calibrations of the CERES scanners planned for Eos.

Foukal, P.↗