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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,027 records · Page 57
All sourcesNASA NTRSDOE OSTI
DOE OSTI2019

Front-end electronic readout system for the Belle II imaging Time-Of-Propagation detector

The Time-Of-Propagation detector is a Cherenkov particle identification detector based on quartz radiator bars for the Belle II experiment at the SuperKEKB ee collider. The purpose of the detector is to identify the type of charged hadrons produced in ee collisions, and requires a single photon timing resolution below 100 picoseconds. A novel front-end electronic system was designed, built, and integrated to acquire data from the 8192 microchannel plate photomultiplier tube channels in the detector. Waveform sampling of these analog signals is done by switched-capacitor array application-specific integrated circuits. The processes of triggering, digitization of windows of interest, readout, and data transfer to the Belle II data acquisition system are managed by Xilinx Zynq-7000 programmable system on a chip devices.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2020

The Catalytic Reduction of Dinitrogen Under Mild Conditions (Final Report)

In order to use molecular hydrogen as an alternative to fossil fuels, large quantities of hydrogen (or protons and electrons) would have to be generated from water using a method based on solar energy and stored as a molecule in which hydrogen is a high weight percentage. The hydrogen must then be generated as needed from the form in which it is stored. An attractive molecule for this purpose is ammonia (~17% hydrogen by weight). Among the many problems that must be addressed for a successful implementation of this approach in the long term is the reduction of nitrogen catalytically to ammonia with protons and electrons under mild conditions, a goal that is addressed in this proposal. The first abiological catalytic reduction of N 2 to NH 3 by protons and electrons under mild conditions (22 °C and 1 atm) employed molybdenum catalysts, [(HIPTNCH 2 CH 2 ) 3 N]Mo (HIPTN 3 N 3- ), where HIPT (hexaisopropylterphenyl) is 3,5- (2,4,6-i-Pr 3 C 6 H 2 ) 2 C 6 H 3 . A total of approximately four turnovers (to give a maximum of eight equivalents of ammonia) along with approximately one equivalent of hydrogen per N 2 reduced, were found. A limitation of this catalytic approach is loss of the ligand from the metal. This project is aimed at developing a complex that contains a ligand that will not be removed from the metal. A macrocyclic TREN-based ligand of this type has been synthesized recently. The project is aimed at making similar ligands and molybdenum complexes that contain them and testing the new catalysts for catalytic reduction of dinitrogen. The results of these investigations will help guide further design of ligands for more efficient reduction of nitrogen to ammonia and ultimately an integrated device in which protons and electrons are generated using solar energy and employed to reduce nitrogen to ammonia using molybdenum catalysts.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2013

Plasma relaxation mechanics of pulsed high power microwave surface flashover

Microwave transmission and reflection characteristics of pulsed radio frequency field generated plasmas are elucidated for air, N{sub 2}, and He environments under pressure conditions ranging from 10 to 600 torr. The pulsed, low temperature plasma is generated along the atmospheric side of the dielectric boundary between the source (under vacuum) and the radiating environment with a thickness on the order of 5 mm and a cross sectional area just smaller than that of the waveguide. Utilizing custom multi-standard waveguide couplers and a continuous low power probing source, the scattering parameters were measured before, during, and after the high power microwave pulse with emphasis on the latter. From these scattering parameters, temporal electron density estimations (specifically the longitudinal integral of the density) were calculated using a 1D plane wave-excited model for analysis of the relaxation processes associated. These relaxation characteristics ultimately determine the maximum repetition rate for many pulsed electric field applications and thus are applicable to a much larger scope in the plasma community than just those related to high power microwaves. This manuscript discusses the diagnostic setup for acquiring the power measurements along with a detailed description of the kinematic and chemical behavior of the plasma as it decays down to its undisturbed state under various gas type and pressure conditions.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2024

Arbitrary Low-Dimensional Film Transfer Enabled by GeO 2 Release Layer

Low-dimensional materials show great promise for enhanced computing and sensing performance in mission-relevant environments. However, integrating low-dimensional materials into conventional electronics remains a challenge. Here, we demonstrate a novel transfer method by which low-dimensional materials and their heterostructures can be transferred onto any arbitrary substrate. Our method relies on a water soluble GeO 2 substrate from which lowdimensional materials are transferred without significant perturbation. We apply the method to transfer a working electronic device based on a low-dimensional material. Process developments are achieved to enable the fabrication and transfer of a working electronic device, including the growth of high-k dielectric on GeO 2 by atomic layer deposition and inserting an indium diffusion barrier into the device gate stack. This work supports Sandia’s heterogeneous integration strategy to broaden the implementation of low-dimensional films and their devices.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Technoeconomic Analysis of Novel PV Plant Designs for Extreme Cost Reductions

This project sought to gain a deeper understanding of the cost and performance of future solar photovoltaic (PV) plant components, including bifacial PV modules, tandem PV modules, increased plant voltage architectures, and module-level power electronics, and how they may be integrated into new PV plant designs to significantly reduce the levelized cost of electricity (LCOE) of PV. This was done through extensive modeling of current PV plants and future technologies in three different locations, informed by a comprehensive literature review and informational interviews to develop performance and cost assumptions for these technologies. Sensitivities were conducted to understand tradeoffs between different design options, such as the added energy from increasing row spacing versus additional land costs. An optimization tool was then created utilizing an evolutionary algorithm to determine an optimal PV plant configuration for a given set of technologies that resulted in minimized plant LCOE based upon typical performance and cost inputs.

14 SOLAR ENERGY↗
DOE OSTI2015

Design Fabrication and Characterization of High Density Silicon Photonic Components

Our burgeoning appetite for data relentlessly demands exponential scaling of computing and communications resources leading to an overbearing and ever-present drive to improve e ciency while reducing on-chip area even as photonic components expand to ll application spaces no longer satis ed by their electronic counterparts. With a high index contrast, low optical loss, and compatibility with the CMOS fabrication infrastructure, silicon-on-insulator technology delivers a mechanism by which e cient, sub-micron waveguides can be fabricated while enabling monolithic integration of photonic components and their associated electronic infrastructure. The result is a solution leveraging the superior bandwidth of optical signaling on a platform capable of delivering the optical analogue to Moore's Law scaling of transistor density. Device size is expected to end Moore's Law scaling in photonics as Maxwell's equations limit the extent to which this parameter may be reduced. The focus of the work presented here surrounds photonic device miniaturization and the development of 3D optical interconnects as approaches to optimize performance in densely integrated optical interconnects. In this dissertation, several technological barriers inhibiting widespread adoption of photonics in data communications and telecommunications are explored. First, examination of loss and crosstalk performance in silicon nitride over SOI waveguide crossings yields insight into the feasibility of 3D optical interconnects with the rst experimental analysis of such a structure presented herein. A novel measurement platform utilizing a modi ed racetrack resonator is then presented enabling extraction of insertion loss data for highly e cient structures while requiring minimal on-chip area. Finally, pioneering work in understanding the statistical nature of doublet formation in microphotonic resonators is delivered with the resulting impact on resonant device design detailed.

36 MATERIALS SCIENCE↗
DOE OSTI2025

Bioelectrochemical crossbar architecture screening platform for extracellular electron transfer

Electroactive microbes can serve as living components in bioelectronic devices, where their unique ability to transfer electrons enables applications in sensing, energy conversion, and synthesis, but they remain challenging to engineer because the bioelectrochemical systems (BESs) used for characterization are low throughput. Here, we present a bioelectrochemical crossbar architecture screening platform (BiCASP) that uses stacked and orthogonally arrayed electrodes to enable individual sample selection for characterization in arrayed formats. This device reports on the current generated by electroactive bacteria on the minute timescale, decreasing the time for data acquisition by several orders of magnitude compared to conventional BESs. This device increases the throughput of screening engineered biological components in cells, identifying mutants of the membrane protein wire MtrA in Shewanella oneidensis that retain the ability to support extracellular electron transfer (EET). BiCASP may be integrated with bioelectronics that need directed evolution of electroactive proteins.

Shewanella↗
DOE OSTI2019

Nanocavity-Enhanced Giant Stimulated Raman Scattering in Si Nanowires in the Visible Light Region

Silicon photonics has been a very active area of research especially in the past two decades in order to meet the ever-increasing demand for more computational power and faster device speeds and their natural compatibility with complementary metal-oxide semiconductor. In order to develop Si as a useful photonics material, essential photonic components such as light sources, waveguides, wavelength convertors, modulators, and detectors need to be developed and integrated. However, due to the indirect electronic bandgap of Si, conventional light emission devices such as light-emitting diodes and lasers cannot be built. Therefore, there has been considerable interest in developing Si-based Raman lasers, which are nonlinear devices and require large stimulated Raman scattering (SRS) in an optical cavity. However, due to the low quantum yield of SRS in Si, Raman lasers have very large device footprints and high lasing threshold, making them unsuitable for faster, smaller, and energy-efficient devices. Here in this paper, we report strong SRS and extremely high Raman gain in Si nanowire optical cavities in the visible region with measured SRS threshold as low as 30 kW/cm 2 . At cavity mode resonance, light is confined into a low mode volume and high intensity electromagnetic mode inside the Si nanowire due to its high refractive index, which leads to strong SRS at low pump intensities. Electromagnetic calculations reveal greater than 6 orders of magnitude increase in Raman gain coefficient at 532 nm pump wavelength, compared to the gain value at 1.55 μm wavelength reported in literature, despite the 10 8 higher losses at 532 nm. Because of the high gain in such small structures, we believe that this is a significant first step in realizing a monolithically integrable nanoscale low-powered Si Raman laser.

36 MATERIALS SCIENCE↗
DOE OSTI2014

Organic integrated circuits for information storage based on ambipolar polymers and charge injection engineering

Ambipolar semiconducting polymers, characterized by both high electron (μ{sub e}) and hole (μ{sub h}) mobility, offer the advantage of realizing complex complementary electronic circuits with a single semiconducting layer, deposited by simple coating techniques. However, to achieve complementarity, one of the two conduction paths in transistors has to be suppressed, resulting in unipolar devices. Here, we adopt charge injection engineering through a specific interlayer in order to tune injection into frontier energy orbitals of a high mobility donor-acceptor co-polymer. Starting from field-effect transistors with Au contacts, showing a p-type unbalanced behaviour with μ{sub h} = 0.29 cm{sup 2}/V s and μ{sub e} = 0.001 cm{sup 2}/V s, through the insertion of a caesium salt interlayer with optimized thickness, we obtain an n-type unbalanced transistor with μ{sub e} = 0.12 cm{sup 2}/V s and μ{sub h} = 8 × 10{sup −4} cm{sup 2}/V s. We applied this result to the development of the basic pass-transistor logic building blocks such as inverters, with high gain and good noise margin, and transmission-gates. In addition, we developed and characterized information storage circuits like D-Latches and D-Flip-Flops consisting of 16 transistors, demonstrating both their static and dynamic performances and thus the suitability of this technology for more complex circuits such as display addressing logic.

36 MATERIALS SCIENCE↗
DOE OSTI2023

Introduction of a Variable Inductance Transformer for the Design of Resonant Power Converters

Magnetic integration is a hot topic in power electronics that concerns the use of a transformer’s leakage and magnetizing inductances purposefully in isolated power electronic converters, thereby giving the opportunity to save the cost and footprint of any additional inductor. This is of prime interest, especially in CLLLC resonant converters which require up to three inductors. For a complete integration of these inductances, the concept of a variable inductance transformer (VIT) is introduced in this thesis. A VIT is an adaptive magnetic structure that facilitates an easy adjustment of both magnetizing and leakage inductances to meet their desired values. However, for a more promising design, an accurate estimation of these inductances is necessary. While the evaluation of magnetizing inductance is quite straightforward, the calculation of leakage inductance is rather convoluted, because the leakage inductance is influenced by both the winding layout and the operating frequency. In this thesis, three new semi-analytical methods for calculating the frequency-independent leakage inductance, and a novel semi-analytical method for evaluating the frequency-dependent leakage inductance are proposed. These methods can calculate the respective leakage inductances of a VIT within an outstanding ±5% uncertainty. Finally, a bidirectional CLLLC resonant dc-dc converter is investigated for the constant current constant voltage (CCCV) charging of the next-generation 900 V traction battery of an electric vehicle. A new voltage gain equation is derived for designing the CLLLC resonant tank, and a small-signal model is presented for designing the variable-frequency feedback controller. Furthermore, a new methodology to design a VIT is developed to overcome the challenges associated with small coupling coefficients and guarantee a complete magnetic integration of the tank inductances. All theoretical results presented herein are verified through simulations and experiments performed on hardware prototypes designed in the lab.

24 POWER TRANSMISSION AND DISTRIBUTION↗
DOE OSTI2024

Longitudinal Solid P Longitudinal Solid Polarized Target for CL get for CLAS12 and Study of Spin AS12 and Study of Spin Structure of Nucleons

A suite of experiments measuring target-spin observables in electron-nucleon scattering (dubbed Run Group C) was conducted at Jefferson Lab's Hall B in Newport News, VA with a new polarized nuclear target known as 'APOLLO' (Ammonia POLarized LOngitudinally). This innovative target is engineered to seamlessly integrate with the advanced 12GeV CEBAF (Continuous Electron Beam Accelerator Facility) accelerator and the Hall B CLAS12 (12 GeV CEBAF Large Acceptance Spectrometer) detector array. The 'APOLLO' target harnesses the power of Dynamic Nuclear Polarization (DNP) to achieve longitudinal polarization of solid ammonia, thereby creating a net polarization in both protons (NH3) and deuterons (ND3). These samples are subjected to a 5 Tesla magnetic field produced by the CLAS12 spectrometer central solenoid, cooled to 1 K using helium evaporation, and subsequently exposed to microwave radiation at a frequency of 140 GHz. This project was made possible through a collaborative partnership between the Jefferson Lab Target Group, Old Dominion University, University of Virginia, Christopher Newport University, and the CLAS Collaboration. Integrating the APOLLO target into CLAS12 presented unique challenges because of its specific spatial and dimensional constraints. This dissertation will highlight the innovative solutions developed to address these challenges, including the creation of a new target material transport system, the incorporation of superconducting magnetic correction coils, and the development of a customized Nuclear Magnetic Resonance (NMR) system. In addition to a detailed description of the development and operation of APOLLO, and an overview of RGC, this document also describes the global data fitting of proton asymmetries in the Deep Inelastic scattering (DIS) and the Resonance regions, and it offers insights into the comprehensive analysis of target polarization data.

Pandey, Pushpa↗
DOE OSTI2016

Meso-scale anisotropic hydrogen segregation near grain-boundaries in polycrystalline nickel characterized by EBSD/SIMS

To study anisotropic hydrogen segregation and diffusion in nickel polycrystalline, Secondary Ion Mass Spectrometry (SIMS) and Electron Back Scattered Diffraction (EBSD) are integrated to investigate hydrogen distribution around grain boundaries. Hydrogen distribution in pre-charged samples were correlated with grain boundary character by integrating high-resolution grain microstructure from EBSD inverse pole figure map and low-resolution hydrogen concentration profile map from SIMS. This multimodal imaging instrumentation shows that grain boundaries in nickel can be categorized into two families based on behavior of hydrogen distribution crossing grain boundary: the first one includes random grain boundaries with fast hydrogen diffusivity, showing a sharp gap for hydrogen concentration profile cross the grain boundaries. The second family are special Σ3n grain boundaries with low hydrogen diffusivity, showing a smooth gradient of hydrogen concentration cross the grain boundary. Heterogeneous hydrogen distributions due to grain boundary family revealed by SIMS/EBSD on mesoscale further validate the recent hydrogen permeation data and anisotropic ab-initio calculations in nanoscale. The results highlight the fact that grain boundaries character impacts hydrogen distribution significantly.

Electron Back Scattered Diffraction↗
DOE OSTI2015

Plasma Physics Approximations in Ares

Lee & More derived analytic forms for the transport properties of a plasma. Many hydro-codes use their formulae for electrical and thermal conductivity. The coefficients are complex functions of Fermi-Dirac integrals, F n ( μ/θ ), the chemical potential, μ or ζ = ln(1+e μ/θ ), and the temperature, θ = kT. Since these formulae are expensive to compute, rational function approximations were fit to them. Approximations are also used to find the chemical potential, either μ or ζ . The fits use ζ as the independent variable instead of μ/θ . New fits are provided for A α (ζ ),A β (ζ ), ζ, f(ζ ) = (1 + e -μ/θ )F 1/2 (μ/θ), F 1/2 '/F 1/2 , F c α , and F c β . In each case the relative error of the fit is minimized since the functions can vary by many orders of magnitude. The new fits are designed to exactly preserve the limiting values in the non-degenerate and highly degenerate limits or as ζ→ 0 or ∞. The original fits due to Lee & More and George Zimmerman are presented for comparison.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2016

Effect of five-membered ring and heteroatom substitution on charge transport properties of perylene discotic derivatives: A theoretical approach

Density functional theory calculations were carried out to investigate the evolvement of charge transport properties of a set of new discotic systems as a function of ring and heteroatom (B, Si, S, and Se) substitution on the basic structure of perylene. The replacement of six-membered rings by five-membered rings in the reference compound has shown a prominent effect on the electron reorganization energy that decreases ∼0.2 eV from perylene to the new carbon five-membered ring derivative. Heteroatom substitution with boron also revealed to lower the LUMO energy level and increase the electron affinity, therefore lowering the electron injection barrier compared to perylene. Since the rate of the charge transfer between two molecules in columnar discotic systems is strongly dependent on the orientation of the stacked cores, the total energy and transfer integral of a dimer as a disc is rotated with respect to the other along the stacking axis have been predicted. Aimed at obtaining a more realistic approach to the bulk structure, the molecular geometry of clusters made up of five discs was fully optimized, and charge transfer rate and mobilities were estimated for charge transport along a one dimensional pathway. Heteroatom substitution with selenium yields electron transfer integral values ∼0.3 eV with a relative disc orientation of 25°, which is the preferred angle according to the dimer energy profile. All the results indicate that the tetraselenium-substituted derivative, not synthetized so far, could be a promising candidate among those studied in this work for the fabrication of n-type semiconductors based on columnar discotic liquid crystals materials.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2022

Design and Challenges of Edge Computing ASICs on Front-End Electronics

In situ or hardware-embedded data processing of raw signals, close to their source, in radiation detectors is expected to provide dramatic improvements in data quality and volumes. However, the implementation of artificial neural networks (ANNs) in the front-end electronics, and the design of custom integrated circuits (ASICs), comes with challenges. In addition, detectors have to operate with limited power budget and implement complex functionalities in a very dense space. They often are exposed to extreme conditions as they work in high-radiation environments and/or cryogenic temperatures. This paper presents examples of applications and design methodologies for in-situ ANNs, along with the challenges of retaining the fidelity of the trained networks. For illustration, we use the problem of estimating the energy deposited by the radiation from digitized waveforms. The proposed implementation starts with an ML algorithm trained in Qkeras and eventually leads to an equivalent ASIC implementation. The associated design challenges in realizing energy and area efficient implementations in CMOS processes are reviewed. Novel approaches that employ hybrid technologies (combination of CMOS with memristors), in-memory computing models, and bio-inspired spiking neural networks are also highlighted

47 OTHER INSTRUMENTATION↗
DOE OSTI2024

Grid Integration of Renewable Energy and Energy Storage

Grid integration of renewable energy and energy storage requires forward-looking planning process, and increased emphasizes on reliability, resilience, and equity. Power-electronics based energy generation including solar, wind, distributed energy resources (DERs), and various types of grid-tied energy storage and emerging loads, are reshaping grid operator's understanding on interconnection level performance and responses. This paper will present the ongoing work at PNNL related to power electronics R&D, energy modeling and analysis, and a wide spectrum of grid stability studies and technologies in support of grid integration of renewable energy and energy storage.

Power Electronics, grid integration of renewable e↗
DOE OSTI2019

Experimental Demonstration of the Henon-Heiles Quasi-Integrable System at IOTA

The Integrable Optics Test Accelerator is a research electron and proton storage ring recently commissioned at the Fermilab Accelerator Science and Technology facility. Its research program is focused on testing novel techniques for improving beam stability and quality, notably the concept of non-linear integrable optics. In this paper, we report the first results of experimental investigation of a quasi-integrable transverse focusing system with one invariant of motion, a Henon-Heiles type system implemented with octupole magnets. Good agreement with simulations is demonstrated on key parameters of achievable tune spread and dynamic aperture preservation. Resilience to perturbations and imperfections in the lattice is explored. We conclude by outlining future research plans and discussing applicability to future high intensity accelerators.

43 PARTICLE ACCELERATORS↗
DOE OSTI2020

Experimental Studies of Single Invariant Quasi-Integrable Nonlinear Optics at IOTA

The Integrable Optics Test Accelerator is a research electron and proton storage ring recently commissioned at the Fermilab Accelerator Science and Technology facility. Its research program is focused on testing novel techniques for improving beam stability and quality, notably the concept of non-linear integrable optics. In this paper, we report on run 1 results of experimental studies of a quasi-integrable transverse focusing system with one invariant of motion, a Henon-Heiles type system implemented with octupole magnets. Good agreement with simulations is demonstrated on key parameters of achievable tune spread, dynamic aperture, and invariant conservation. We also outline current simulation and hardware improvement efforts for run 2, planned for fall of 2019.

43 PARTICLE ACCELERATORS↗