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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,063 records · Page 59

Effect of specimen geometry on the energy absorption capability of composite materials

Static crushing tests were conducted on graphite and Kevlar reinforced epoxy tubes to examine the influence of specimen geometry on the energy absorption capability of composite materials. Tube inside diameter to wall thickness (D/t) ratio was determined to significantly affect the energy absorption capability of composite materials. As D/t ratio decreases, the energy absorption capability increases nonlinearly. The energy absorption capability of K/E tubes was found to be geometrically scalable but energy absorption of Gr/E tubes was not geometrically scalable.

Farley, G. L.↗

Process Optimization of Bismaleimide (BMI) Resin Infused Carbon Fiber Composite

Engineers today are presented with the opportunity to design and build the next generation of space vehicles out of the lightest, strongest, and most durable materials available. Composites offer excellent structural characteristics and outstanding reliability in many forms that will be utilized in future aerospace applications including the Commercial Crew and Cargo Program and the Orion space capsule. NASA's Composites for Exploration (CoEx) project researches the various methods of manufacturing composite materials of different fiber characteristics while using proven infusion methods of different resin compositions. Development and testing on these different material combinations will provide engineers the opportunity to produce optimal material compounds for multidisciplinary applications. Through the CoEx project, engineers pursue the opportunity to research and develop repair patch procedures for damaged spacecraft. Working in conjunction with Raptor Resins Inc., NASA engineers are utilizing high flow liquid infusion molding practices to manufacture high-temperature composite parts comprised of intermediate modulus 7 (IM7) carbon fiber material. IM7 is a continuous, high-tensile strength composite with outstanding structural qualities such as high shear strength, tensile strength and modulus as well as excellent corrosion, creep, and fatigue resistance. IM7 carbon fiber, combined with existing thermoset and thermoplastic resin systems, can provide improvements in material strength reinforcement and deformation-resistant properties for high-temperature applications. Void analysis of the different layups of the IM7 material discovered the largest total void composition within the [ +45 , 90 , 90 , -45 ] composite panel. Tensile and compressional testing proved the highest mechanical strength was found in the [0 4] layup. This paper further investigates the infusion procedure of a low-cost/high-performance BMI resin into an IM7 carbon fiber material and the optical, chemical, and mechanical analyses performed.

Ehrlich, Joshua W.↗

Analysis and Testing of a Metallic Repair Applicable to Pressurized Composite Aircraft Structure

Development of repair technology is vital to the long-term application of new structural concepts on aircraft structure. The design, analysis, and testing of a repair concept applicable to a stiffened composite panel based on the Pultruded Rod Stitched Efficient Unitized Structure was recently completed. The damage scenario considered was a mid-bay to mid-bay saw-cut with a severed stiffener, flange, and skin. A bolted metallic repair was selected so that it could be easily applied in the operational environment. The present work describes results obtained from tension and pressure panel tests conducted to validate both the repair concept and finite element analysis techniques used in the design effort. Simulation and experimental strain and displacement results show good correlation, indicating that the finite element modeling techniques applied in the effort are an appropriate compromise between required fidelity and computational effort. Static tests under tension and pressure loadings proved that the proposed repair concept is capable of sustaining load levels that are higher than those resulting from the current working stress allowables. Furthermore, the pressure repair panel was subjected to 55,000 pressure load cycles to verify that the design can withstand a life cycle representative for a transport category aircraft. These findings enable upward revision of the stress allowables that had been kept at an overly-conservative level due to concerns associated with repairability of the panels. This conclusion enables more weight efficient structural designs utilizing the composite concept under investigation.

Przekop, Adam↗

Hydrogen sensing in different hydrogen-carrying gases using composites of PdSnO 2 and halloysite nanotubes

Here, in this work, we developed composites of palladium-decorated tin dioxide (PdSnO 2 ) and halloysite nanotubes (HNTs) by adding different amounts of HNTs as additives into PdSnO 2 , and investigated how the different amounts of HNTs in the composites and the different hydrogen (H 2 ) carrying gases (air and helium (He)) could affect the H 2 sensing performance of such composites (PdSnO 2 -HNT). Through the sensing-performance characterization using H 2 carried by air, it was found that PdSnO 2 with an appropriate small amount of HNTs (i.e., 2 % of PdSnO 2 mass) can improve the sensing performance with respect to limit of detection (LOD) and response/recovery time. Further, the optimal PdSnO2-HNT composite as a sensor was tested to detect H 2 in He. The testing results indicated that the composite can detect H 2 in He, but its performance parameters (i.e., the profile of calibration curve, LOD, and response time) are different from those of such a sensor in detecting H 2 in air. Moreover, the composite still presented better sensing performance than PdSnO 2 without HNTs in detecting H 2 in He. Possible reasons for the effects of HNT and H 2 -carrying gas on the sensing performance of PdSnO 2 -HNT-based sensors were discussed. We believe that this study provides valuable insights into the functionality and the adaptability of PdSnO 2 -HNT-based H 2 sensors in diverse operational conditions.

36 MATERIALS SCIENCE↗

Computer aided derivation of equations for composite mechanics problems and finite element analyses

Explicit equations are derived for analysis of multilayered fiber composites and for finite element analyses. The equations are obtained using a symbolic program and tested for various composite properties as well as for different fiber orientations. In order to analyze multilayered fiber composite structures, a variable thickness finite element is formulated. Examples of an airfoil geometry, simulated in a form of a cantilevered beam with various fiber orientations are studied.

Sarigul, N.↗

Erosive burning of solid propellants

Presented here is a review of the experimental and modeling work concerning erosive burning of solid propellants (augmentation of burning rate by flow of product gases across a burning surface). A brief introduction describes the motor design problems caused by this phenomenon, particularly for low port/throat area ratio motors and nozzleless motors. Various experimental techniques for measuring crossflow sensitivity of solid propellant burning rates are described, with the conclusion that accurate simulation of the flow, including upstream flow development, in actual motors is important since the degree of erosive burning depends not only on local mean crossflow velocity and propellant nature, but also upon this upstream development. In the modeling area, a brief review of simplified models and correlating equations is presented, followed by a description of more complex numerical analysis models. Both composite and double-base propellant models are reviewed. A second generation composite model is shown to give good agreement with data obtained in a series of tests in which composite propellant composition and heterogeneity (particle size distribution) were systematically varied. Finally, the use of numerical models for the development of erosive burning correlations is described, and a brief discussion of scaling is presented.

King, Merrill K.↗

Mechanical Behavior and Analytical Modeling of Melt-Infiltrated SiC/SiC Woven Composite

The desirable properties in ceramic matrix composites (CMCs), such as high temperature strength, corrosion resistance, high toughness, low density, or good creep resistance have led to increased use of CMCs in high-speed engine structural components and structures that operate in extreme temperature and hostile aero-thermo-chemical environments. Ceramic matrix composites have been chosen for turbine material in the design of 21st century civil propulsion systems to achieve high fuel economy, improved reliability, extended life, and reduced cost. Most commercial CMCs are manufactured using a chemical vapor infiltration (CVI) process. However, a lower cost fabrication known as melt-infiltration process is also providing CMCs marked for use in hot sections of high-speed civil transports. Limited samples of a SiC/SiC melt-infiltrated woven composites are being investigated at room and elevated temperature below and above matrix cracking. These samples show graceful failure and toughness at room temperature with a reduction in strength and modulus at elevated temperatures. A generic finite element model is also being developed to predict monotonic and cyclic loading behavior of the woven composite. Use of the initial test data from the woven composite is being used for the development of the analytical model. This model is the first of a iterative process leading towards the development the model's capability to predict behavior at room and elevated temperature for monotonic and cyclic loading. The purpose of this paper is to report on the material and mechanical findings of the SiC/SiC melt-infiltrated woven composite and progress on the development of the finite element model.

Lang, J.↗

Status of High-Strength Nanotube Composites at Johnson Space Center

Single-wall carbon nanotubes offer extraordinary mechanical properties that could start a revolution in materials science. The combination of very high strength and modulus with high strain to failure makes nanotubes an ideal fiber for strengthening in composites. Because of the scale of these fibers, new challenges exist for processing of composite materials and materials characterization. Our project includes aspects of nanotube materials from production and characterization to purification and incorporation into composites for mechanical testing. Early results show that some new techniques will be necessary for the strength of single wall nanotubes to be fully utilized. Current research at JSC focuses on structural polymeric materials to attempt to lower the weight of spacecraft necessary for interplanetary missions. Studies show good nanotube dispersion and wetting by the epoxy materials. Results of tensile strength tests will also be reported. This presentation will focus on current research into polymer nanotube composites and the next steps toward this revolution in aerospace materials.

Files, Bradley S.↗

Using the Climbing Drum Peel (CDP) Test to Obtain a G(sub IC) value for Core/Facesheet Bonds

A method of measuring the Mode I fracture toughness of core/facesheet bonds in sandwich Structures is desired, particularly with the widespread use of models that need this data as input. This study examined if a critical strain energy release rate, G(sub IC), can be obtained from the climbing drum peel (CDP) test. The CDP test is relatively simple to perform and does not rely on measuring small crack lengths such as required by the double cantilever beam (DCB) test. Simple energy methods were used to calculate G(sub IC) from CDP test data on composite facesheets bonded to a honeycomb core. Facesheet thicknesses from 2 to 5 plies were tested to examine the upper and lower bounds on facesheet thickness requirements. Results from the study suggest that the CDP test, with certain provisions, can be used to find the GIG value of a core/facesheet bond.

Nettles, A. T.↗

In-Plane Tensile Properties, Creep Behavior and Failure Mechanisms of CVI and PIP SiC/SiC Composites at Temperatures to 1,650⁰C in Air

The in-plane tensile and creep properties of 2D woven CVI and PIP SiC/SiC composites with SylramicTM-iBN SiC fibers were measured at temperatures to 16500C in air and the data compared with the literature. Batch-to-batch variations in the tensile and creep properties, influence of thermal treatment on creep, creep parameters, damage mechanisms and failure modes for these composites were studied. Under the tested conditions, the CVI SiC/SiC composites exhibited both matrix and fiber dominated creep depending on stress, whereas the PIP SiC/SiC composites displayed only fiber dominated creep. Creep durability in both composite systems is controlled by the most creep resistant phase as well as oxidation of the fibers via cracked matrix. The Larson-Miller parameter and Monkman-Grant relationship were used wherever applicable for analyzing and predicting creep durability.

SiC-SiC Composites, CVI, PIP, Creep, In-plane tens↗

Materials Testing on the DC-X and DC-XA

Flight testing of thermal protection materials has been carried out over a two year period on the base heat shield of the Delta Clipper (DC-X and DC-XA), as well on a body flap. The purpose was to use the vehicle as a test bed for materials and more efficient repair or maintenance processes which would be potentially useful for application on new entry vehicles (i.e., X-33, RLV, planetary probes), as well as on the existing space shuttle orbiters. Panels containing Thermal Protection Systems (TPS) and/or structural materials were constructed either at NASA Ames Research Center or at McDonnell Douglas Aerospace (MDA) and attached between two of the four thrusters in the base heat shield of the DC-X or DC-XA. Three different panels were flown on DC-X flights 6, 7, and 8. A total of 7 panels were flown on DC-XA flights 1, 2, and 3. The panels constructed at Ames contained a variety of ceramic TPS including flexible blankets, tiles with high emissivity coatings, lightweight ceramic ablators and other ceramic composites. The MDS test panels consisted primarily of a variety of metallic composites. This report focuses on the ceramic TPS test results.

Smith, Dane↗

Autohesive strength development in polysulfone resin and graphite-polysulfone composites

The effects of bonding temperature and contact time on autohesive strength development in thermoplastic polysulfone resin and graphite-polysulfone composites were investigated. Two test methods were examined to measure autohesion in the neat resin samples. These included an interfacial tension test and a compact tension fracture toughness test. Autohesive strength development in fiber-reinforced composites was measured using a double cantilever beam interlaminar fracture toughness test. The results of the tests were compared with current diffusion theories explaining crack healing and welding of glassy polymers. Discrepancies between the results of the present investigation and the diffusion theories are discussed.

Howes, Jeremy C.↗

Development and thermal performance verification of composite insulation boards containing foam-encapsulated vacuum insulation panels

High-performance thermal insulation is a critical need for buildings. This article presents the development and thermal characterization of composite foam insulation boards containing low-cost vacuum insulation cores. The composite foam-vacuum insulation boards were created in a semi-automatic operation in a foam insulation manufacturing plant. The low-cost vacuum insulation is a new technology called modified atmosphere insulation. The production process of modified atmosphere insulation is much simpler than traditional vacuum insulation manufacturing, and it has the potential for significant cost reduction at the same thermal performance. Prototypes of small- and full-scale composite insulation boards were created for testing and evaluation under laboratory and natural weatherization conditions. The laboratory tests showed that the overall thermal resistance of the composite insulation board is at least twice that of current rigid foam insulation used in building envelope. Lastly, ongoing test of the composite insulation in a natural exposure test facility indicates that the high thermal performance was retained through handling and installation as well as natural aging over a period of one and a half years.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

Development of design allowable data for Celion 6000/LARC-160, graphite/polyimide composite laminates

A design allowables test program was conducted on Celion 6000/LARC-160 graphite polyimide composite to establish material performance over a 116 K (-250 F) to 589 K (600 F) temperature range. Tension, compression, in-plane shear and short beam shear properties were determined for uniaxial, quasi-isotropic and + or - 45 deg laminates. Effects of thermal aging and moisture saturation on mechanical properties were also evaluated. Celion 6000/LARC-160 graphite/polyimide can be considered an acceptable material system for structural applications to 589 K (600 F).

Ehret, R. M.↗

Experimental results on plasma interactions with large surfaces at high voltages

Multikilowatt power levels for future payloads can be more efficiently generated using solar arrays operating in the kilovolt range. This implies that large areas of the array at high operating voltages will be exposed to the space plasma environment. The resulting interactions of these high voltage surfaces with space plasma environments can seriously impact the performance of the satellite system. The plasma-surface interaction phenomena were studied in tests performed in two separate vacuum chambers, a 4.6 m diameter by 19.2 long chamber and a 20 m diameter by 27.4 m long chamber. The generated plasma density was approximately 1x10 to the 4th power/cu cm. Ten solar array panels, each with areas of 1400 sq cm were used in the tests. Nine of the solar panels were tested as a composite unit in the form of a 3x3 solar panel matrix. The results from all the tests confirmed small sample tests results: insulators were found to enhance the plasma coupling current for high positive bias and arcing was found to occur at high negative bias.

Grier, N. T.↗

Program for establishing long-time flight service performance of composite materials in the center wing structure of C-130 aircraft. Phase 4: Ground/flight acceptance tests

The advantageous structural uses of advanced filamentary composites are demonstrated by design, fabrication, and test of three boron-epoxy reinforced C-130 center wing boxes. The advanced development work necessary to support detailed design of a composite reinforced C-130 center wing box was conducted. Activities included the development of a basis for structural design, selection and verification of materials and processes, manufacturing and tooling development, and fabrication and test of full-scale portions of the center wing box. Detailed design drawings, and necessary analytical structural substantiation including static strength, fatigue endurance, flutter, and weight analyses are considered. Some additional component testing was conducted to verify the design for panel buckling, and to evaluate specific local design areas. Development of the cool tool restraint concept was completed, and bonding capabilities were evaluated using full-length skin panel and stringer specimens.

Harvill, W. E.↗

An evaluation of the +/-45 deg tensile test for the determination of the in-plane shear strength of composite materials

The applicability of the +/-45 deg tensile test for the determination of the in-plane shear strength of advanced composite laminates is studied. The assumptions used for the development of the shear strength formulas were examined, and factors such as the specimen geometry and stacking sequence were assessed experimentally. It was found that the strength of symmetric and balanced +/-45 deg laminates depends primarily upon the specimen thickness rather than the specimen width. These findings have important implications for the +/-45 deg tensile test which is recommended by several organizations for the determination of the in-plane shear stress/strain response and the shear strength of continuous fiber reinforced composites. Modifications to the recommended practices for specimen selection and shear strength determination are suggested.

Kellas, S.↗

Resistance heating releases structural adhesive

Composite adhesive package bonds components together for testing and enables separation when testing is completed. The composite of adhesives, insulation and a heating element separate easily when an electrical current is applied.

Glemser, N. N.↗