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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 109 records · Page 6
All sourcesNASA NTRSDOE OSTI
DOE OSTI2026

Structural and spectroscopic characterization of a Tb(IV) polyoxometalate

There has been a renaissance in high valent lanthanide chemistry, which has resulted in the first examples of tetravalent praseodymium (Pr) and terbium (Tb) in molecular systems. These feats have been achieved with tailored ligands that facilitate tetravalent lanthanide stability in non-aqueous conditions. The next step in realizing the potential of high valent lanthanide chemistry is moving towards complexes that are stable in ambient and aqueous conditions. In this investigation, we advance this paradigm by obtaining definitive evidence of Tb(IV) in a molecular system under aqueous conditions utilizing the lacunary Wells-Dawson polyoxometalate, K 10 P 2 W 17 O 61 •20H 2 O. Herein we present the single crystal structure of K 16 Tb(IV)(P 2 W 17 O 61 ) 2 •39.85H 2 O (Tb(IV)W 34 ) as well as extensive spectroscopic evidence obtained via UV–Vis-NIR, X-ray absorption near edge spectroscopy, continuous wave X-band electron paramagnetic resonance spectroscopy and SQUID magnetometry measurements to confirm the oxidation state of Tb in W 34 complexes as +4.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2024

A neutron fluence map of the Los Alamos National Laboratory Godiva IV critical assembly

A neutron fluence map and a total ionizing dose map of the Los Alamos National Laboratory Godiva IV fast burst critical assembly was generated using passive reactor dosimetry, comprised of sulfur pellets and thermoluminescent dosimeters. Godiva IV is an unmoderated, fast burst, critical assembly constructed of approximately 65 kg of highly enriched uranium fuel alloyed with 1.5 % molybdenum for strength. The mapping was performed during a single 75.6 ºC temperature rise burst operation, with the top and sides of the cylindrical Godiva-IV Top Hat covered in passive dosimetry. Dosimetry was placed in a symmetric pattern around the Top Hat, with higher concentrations near the control rods and burst rod. A specific portion of the lower quadrant of the burst rod was mapped to confirm a testing region where the neutron fluence varied by no more than ± 5%. The results will be used to assess the neutron, gamma, and total ionizing dose environment in three-dimensional space around the assembly for higher fidelity experiment placement, active dosimetry positioning, and radiation field characterization.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2024

The 1.3 Å resolution structure of the truncated group Ia type IV pilin from Pseudomonas aeruginosa strain P1

The type IV pilus is a diverse molecular machine capable of conferring a variety of functions and is produced by a wide range of bacterial species. The ability of the pilus to perform host-cell adherence makes it a viable target for the development of vaccines against infection by human pathogens such as Pseudomonas aeruginosa . Here, the 1.3 Å resolution crystal structure of the N-terminally truncated type IV pilin from P. aeruginosa strain P1 (ΔP1) is reported, the first structure of its phylogenetically linked group (group I) to be discussed in the literature. The structure was solved from X-ray diffraction data that were collected 20 years ago with a molecular-replacement search model generated using AlphaFold ; the effectiveness of other search models was analyzed. Examination of the high-resolution ΔP1 structure revealed a solvent network that aids in maintaining the fold of the protein. On comparing the sequence and structure of P1 with a variety of type IV pilins, it was observed that there are cases of higher structural similarities between the phylogenetic groups of P. aeruginosa than there are between the same phylogenetic group, indicating that a structural grouping of pilins may be necessary in developing antivirulence drugs and vaccines. These analyses also identified the α–β loop as the most structurally diverse domain of the pilins, which could allow it to serve a role in pilus recognition. Studies of ΔP1 in vitro polymerization demonstrate that the optimal hydrophobic catalyst for the oligomerization of the pilus from strain K122 is not conducive for pilus formation of ΔP1; a model of a three-start helical assembly using the ΔP1 structure indicates that the α–β loop and the D-loop prevent in vitro polymerization.

Bragagnolo, Nicholas↗
DOE OSTI2025

Investigation of a U(IV)/U(III) Thermodynamic Reference Electrode for High-Temperature Molten Fluoride Salts

While thermodynamic reference electrodes with known and stable potentials are common in traditional aqueous systems, the high temperature and corrosive environment of a molten fluoride salt makes achieving long term stability with a thermodynamic reference electrode challenging, especially at temperatures of 600°C or higher. In this work, a thermodynamic reference electrode consisting of U(IV)/U(III) in a boron nitride compartment was evaluated for use in FLiBe at temperatures ≥ 600°C. FLiBe used in the study was purified by AlphaTech's proprietary process and characterized by ICP-MS and square wave voltammetry. The free oxide concentration was <2 ppm. Using the purified FLiBe, the U(IV)/U(III) thermodynamic reference electrode was shown to provide a stable, well-defined, and reproducible potential for more than 600+ hours of use in different tests. Moreover, the thermodynamic reference electrode showed a consistent potential with no signs of failure, even after being cooled between tests and then reheated for reuse. Thus, the U(IV)/U(III) reference electrode is suitable for use in rigorous electrochemical studies in molten fluoride salts. As a result, it may be useful as a common standard, facilitating the advancement of nuclear applications such as isotope separation or online monitoring of reactor systems through improved certainty in the measurement of thermodynamic potentials.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
DOE OSTI2026

A reproducible study design for the MIMIC-IV in-hospital mortality task

Open, tabular electronic health record (EHR) datasets such as MIMIC-III and MIMIC-IV have become critical resources for developing machine learning (ML) models addressing clinical prediction tasks, including hospital readmission, length of stay, and in-hospital mortality (IHM). While MIMIC-III has benefited from well-established preprocessing pipelines and standardized feature sets, MIMIC-IV remains comparatively challenging to work with because there are no standardized benchmarks to support reproducibility and comparability across studies. To address this limitation, we present a rigorously curated MIMIC-IV custom feature set optimized for IHM prediction, constructed through a reproducible preprocessing pipeline and feature selection strategy.

97 MATHEMATICS AND COMPUTING↗
NASA NTRS1975

An upper limit on interstellar C IV in the spectrum of gamma-2 Velorum

An upper limit on the column density of C IV along the line of sight to gamma-2 Vel is derived from upper limits placed on the equivalent widths of the interstellar C IV doublet with rest wavelengths at 1548.20 A and 1550.77 A. A lower limit of 250,000 K is calculated for the electron temperature of O VI emitting regions by combining the C IV results with a measurement of the column density of interstellar O VI for the same star and using calculations for the relative ionization of some abundant elements as a function of electron temperature in a low-density plasma. Since gamma-2 Vel is in the central part of the Gum Nebula, the high temperature suggested by these results is shown to support the idea that a high-temperature phase of the interstellar medium, possibly maintained by supernova explosions, may exist.-

Lengyel-Frey, D.↗
NASA NTRS1977

Relationships between convective storms and their environment in AVE IV determined from a three-dimensional subsynoptic-scale, trajectory model

The paper describes interrelationships between synoptic-scale and convective-scale systems obtained by following individual air parcels as they traveled within the convective storm environment of AVE IV. (NASA's fourth Atmospheric Variability Experiment, AVE IV, was a 36-hour study in April 1975 of the atmospheric variability and structure in regions of convective storms.) A three-dimensional trajectory model was used to calculate parcel paths, and manually digitized radar was employed to locate convective activity of various intensities and to determine those trajectories that traversed the storm environment. Spatial and temporal interrelationships are demonstrated by reference to selected time periods of AVE IV which contain the development and movement of the squall line in which the Neosho tornado was created.

Wilson, G. S.↗
NASA NTRS1978

The distribution of S IV and Ne II in NGC 7027

Results are reported for measurements of the S IV 10.5-micron and Ne II 12.8-micron IR emission lines at four positions in NGC 7027 and of the Ar III 9.0-micron line at one position in the same planetary nebula. Ionic abundances are calculated using the data obtained at one position and are combined with published optical data for other ionization states to obtain total elemental abundances. The S IV and Ne II line-intensity distributions are compared with an 8.1-GHz radio map of the nebula. The S IV distribution indicates a density of about 500,000 per cu cm, and the Ne II is found to be contained in low-ionization regions distributed inhomogeneously throughout the nebula. The total abundances relative to hydrogen are determined to be 0.000015 for S, 0.000053 for Ne, and 0.000007 for Ar; these abundances are shown to be within the range of published average values for planetary nebulae.

Bregman, J. D.↗
NASA NTRS1980

Atomic data for S IV and solar observations of the 3x/2/3p /2/P-3s3p/2/ /4/P multiplet

High resolution observations of intersystem lines of S IV near 1400 A are available from Skylab. These lines are potentially useful as density diagnostics for the solar atmosphere. Energy levels, transition probabilities and collision strengths have, therefore, been calculated for S IV, including the configurations 3x(2)3p, 3s3p(2), and 3s(2)3d. Line intensities and level populations have been calculated as a function of electron density. The calculated population of the 3s3p(2) (4)P(5/2) level is found to reach a pseudo-Boltzmann equilibrium at a density which is four times higher than is inferred from solar spectra and level population calculations of lighter ions such as O IV.

Bhatia, A. K.↗
NASA NTRS1982

Visible light observations of a dense plasmoid associated with a moving Type IV solar radio burst

A coronal transient rising above the eastern limb of the sun was observed simultaneously on April 27, 1980 by the Coronagraph/Polarimeter (C/P) aboard the Solar Maximum Mission spacecraft and by the Culgoora radioheliograph (CRH). The C/P observed an outward-moving loop transient followed by a plasmoid of dense ionized material, while the CRH observed several types of radio bursts, including a moving Type IV burst at 80 MHz whose position coincided with the bright plasmoid. An estimate of the reasonable lower limit of the electron density in the moving Type IV burst indicates that this burst could have resulted from emission at either the fundamental or the second harmonic of the plasma frequency. This is a new result because in the past it was thought that the density in the moving Type IV source region would be too low for plasma radiation.

Stewart, R. T.↗
NASA NTRS1983

The morphology and kinematics of the Cep IV star formation region

Rossano et al. (1980) have discussed the morphology and kinematics of Cep IV star formation region. The present investigation is concerned with H2CO observations which have been conducted to examine the relationship between the neutral and ionized gas in the Cep IV star formation region and to study the origin of the unusual kinematics and morphology of the stars, gas, and dust in this region. Six-cm H2CO observations were undertaken throughout a one half degree square area centered on the H II region W1. In addition, VLA observations of the Cep IV region at 6 and 20 cm were also performed. The neutral gas in the vicinity of W1 is found to be located in clouds having velocities of -13, -7, and 1 km/s. The gas at - 7 km/s appears to be undisturbed gas from the original dark cloud complex.

Grayzeck, E. J.↗
NASA NTRS1984

Dynamics of solar filaments. III - Analysis of steady flows in H-alpha and C IV lines

A statistical analysis of intensities and radial velocities of several solar plage filaments (i.e. prominences seen on the solar disk) observed at disk center is presented. Intensity and radial (= vertical) velocity maps were derived from simultaneous 2D measurements of the H-alpha chromospheric line with the Multichannel Subtractive Double Pass spectrograph operating on the Meudon solar tower, and also obtained from 2D recordings of the C IV transition-zone line (1548 A) with the UV Spectrometer and Polarimeter aboard the Solar Maximum Mission satellite. A good correlation (around 0.5) is found between intensities in both lines, as well as between velocities. Persistent upflows are measured in both lines at the filament location. The mean vertical velocities are respectively 0.5 km/s in H-alpha and 5.6 km/s in C IV. The analysis of mass fluxes suggests that C IV upflows occur in the transition region around prominences rather than below, in the chromosphere-corona transition zone.

Schmieder, B.↗
NASA NTRS1987

A type IV burst associated with a coronal streamer disruption event

A type IV burst was observed on February 17, 1985 with the Clark Lake Radio Observatory multifrequency radioheliograph operating in the frequency range 20-125 MHz. This burst was associated with a coronal streamer disruption event. From two-dimensional images produced at 50 MHz, evidence of a type II burst and a slow moving type IV burst are shown. The observations of the moving type IV burst suggests that a plasmoid containing energetic electrons can result from the disruption of a coronal streamer.

Kundu, M. R.↗
NASA NTRS1988

The C IV doublet ratio intensity effect in symbiotic stars

High-resolution UV spectra in the 1200-2000 wavelength range of the symbiotic variable R Aqr and its nebular jet were obtained in July 1987 with the IUE. The line profile structure of the C IV 1548, 1550 doublet in the jet indicates multicomponent velocity structure from an optically thin emitting gas. The C IV doublet profiles in the compact H II region engulfing the Mira and hot companion binary also suggest multicomponent structure with radial velocities up to about -100 km/s. The value of the doublet intensity ratio in the R Aqr H II region has been observed in other similar symbiotic stars, such as RX Pup. It is suggested that the anomalous behavior of the C IV doublet intensities may be useful for studying the spatial structure and temporal nature of winds in symbiotic stars.

Michalitsianos, A. G.↗
NASA NTRS1988

Design and test of a modified passive orbital disconnect strut (PODS-IV)

The design and testing of a modification to the Passive Orbital Disconnect Struts (PODS) III system (designed to reduce support conductance and superfluid-helium-tank dewar weights), PODS IV, are discussed. The PODS IV design was found to achieve a nominal increase of 630-812 percent in side-load resistance over the PODS-III design, with a predicted 15-percent increase in thermal conductance. It is noted that the increase in side-load resistance largely removes the limitation on length of the orbit tube inherent in the PODS III design. The higher resistance of the longer orbit tube results in lower total conductance for the PODS-IV design.

Spradley, Iran E.↗
NASA NTRS1991

Determining the IV fluids required for a ten day medical emergency on Space Station Freedom - Comparison of packaged vs. on-orbit produced solutions

To aid planning for the storage of supplies onboard Space Station Freedom, an estimate was made of the amount of intravenous (IV) fluid required to support a patient who has suffered a medical emergency for a period of up to 10 days. Six different medical scenarios were evaluated, and the volume of IV fluids required for each scenario was estimated. Up to 220 liters of fluid would be required to support a patient for all of the scenarios. When optimizing the volumes to support any single scenario, a total of 123 liters is required. Use of a water polishing system to produce sterile water for injection from potable supplies and on-station formulation of IV fluids results in a smaller mass and volume requirement for the Fluid Therapy Subsystem than carrying prepackaged bags of fluid.

Creager, Gerald J.↗
NASA NTRS1997

NASA software independent verification and validation (IV and V): An upfront approach to mission success

Software independent verification and validation (IV and V) implementation methods, specific approaches and accomplishments in the application of IV and V to NASA programs are discussed. Because software is mission critical, software assurance is a critical aspect of NASA's safety and mission assurance program. An overview of NASA's software IV and V facility is given.

Gregory, Frederick D.↗
NASA NTRS2001

GSFC IVS Technology Development Center Report

This report summarizes the activities of the Goddard Space Flight Center's (GSFC's) International Very Long Base Interferometry (VLBI) Service (IVS)Technology Development Center from the establishment of IVS to the end of 2000. The report forecasts activities planned for the year 2001. The GSFC IVS Technology Development Center (TDC) develops station software including the Field System (FS), scheduling software (SKED), hardware including tools for station timing and meteorology, scheduling algorithms, operational procedures, and provides a pool of individuals to assist with station implementation, check-out, upgrades, and training.

Himwich, Ed↗