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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 109 records · Page 6
All sourcesNASA NTRSDOE OSTI
NASA NTRS2018

Achieving Improved Reliability with Failure Analysis

Reliability is the ability of a product to properly function, within specified performance limits, for a specified period of time, under the life cycle application conditions. Failure analysis is a vital tool in the effort to ensure reliability of electronic products and systems throughout their product lifecycle. Today, organizations involved in activities within the electronics supply chain are facing new challenges, not just from complex assembly styles, harsher lifecycle environments, and sophisticated supply chains, but also from customers who are demanding a quicker turn-around. Unfortunately, root cause failure analysis is often performed incompletely, leading to a poor understanding of failure mechanisms and causes and, customer dissatisfaction due to recurring failures. The PDC starts with an introduction to reliability concepts, physics of failure and an overview of failure mechanisms that affect PCBs, PCBAs and components. The PDC then dives into root cause hypothesizing techniques (Pareto, FMEA, fishbone, FTA), non-destructive and destructive analysis and, materials characterization will be discussed. Numerous failure analysis case studies will be used to illustrate the techniques and analysis principles to arrive at the root cause(s) of field failures on printed circuit boards, active components, and assemblies. What Will You Learn: Topics include: Overview of Reliability Concepts Failure mechanisms of electronic products Root cause analysis Failure analysis techniques -Non-destructive techniques (optical, CSAM etc.) -Destructive analysis (DPA, Decap, FIB etc.) -Materials characterization (XRF, EDS, TMA/DSC etc.) Who Will Benefit: Reliability engineers, failure analysis engineers, engineering managers, design engineers, component engineers, quality assurance functions and, personnel involved with reliability activities within their company.

non-destructive techniques↗
NASA NTRS1985

Metallurgical and mechanical phenomena due to rubbing of titanium against sintered powder Nichrome

Metallurgical and mechanical changes occurring during high-speed rubbing of Ti-6Al-4V blade specimens against an abradable Nichrome aircraft engine seal material were studied using optical microscopy, electron microscopy, and microhardness techniques. Evidence of temperatures above the beta transus of Ti-6Al-4V (1000 C) and of thermal hardening was found on blade tips that exhibited undesirable abrading characteristics resulting in high forces of interaction, high temperatures, and smearing. The material within the layer of the corresponding seals was found to be work-hardened to a depth of about 0.1 mm and showed evidence of densification extending to a depth of about 0.5 mm below the rubbed surface. Wear particles produced by rub interactions that generated cleanly abraded seal surfaces were found to be several times larger than those produced during interactions which showed evidence of surface smearing and seal densification.

Zenas, R.↗
NASA NTRS1983

Application of mass spectrometry to process control for polymer material in autoclave curing

Mass spectrometer analysis of gas samples collected during a cure cycle of polymer materials can be used as a process control technique. This technique is particularly helpful in studying the various types of solvents and resin systems used in the preparation of polymer materials and characterizing the chemical composition of different resin systems and their mechanism of polymerization.

Smith, A. C.↗
NASA NTRS1982

Aerodynamic levitation of laser-heated solids in gas jets

The aerodynamic levitation technique is developed for studies of high-temperature material properties and gas/condensed-phase reaction kinetics. Stable levitation is demonstrated in a supersonic jet from a 0.081 cm nozzle with 0.03-0.20 g 0.24-0.47 cm diameter solid spheres at a height between 0.7-2.0 cm above the nozzle and ambient pressures between 1.1-18 Torr. A model of supersonic jet levitation is developed which accurately predicts the values of height vs pressure over the full range of conditions investigated. It is found that the efficiency with which jet momentum is converted into levitation force decreases with the jet/specimen diameter ratio and the jet Reynolds number, and the rate of jet spreading with distance from the nozzle is found to agree with that measured by pitot tube traverses of the jet. In addition, laser heating is shown to reduce the jet momentum required for levitation at a given height and to increase levitation stability. Measurements of sphere levitation in subsonic gas jets show that the required jet momentum flow rate exceeds the specimen weight by about 2/the specimen drag coefficient at its terminal free-fall speed under ambient conditions.

Nordine, P. C.↗
NASA NTRS1991

An evaluation of bearings operating in a cryogenic environment with silicon nitride rolling elements

The bearings used in the space shuttle main engine (SSME) high pressure oxidizer turbopump (HPOTP) do not meet the expected life goals that were set for them. In an effort to improve their performance, many solutions are being studied. New bearing materials are being developed, better manufacturing techniques are being investigated, and improved cage materials for better lubrication are being tested. The focus is on the replacement of steel balls with ones made of silicon nitride in 57-mm HPOTP bearings. The bearings were then installed in a test rig and run at near turbopump operating conditions. The results from this test series are encouraging, with silicon nitride showing good wear resistance and thermal stability.

Gibson, H. G.↗
NASA NTRS1990

Experiment K-6-18. Study of muscarinic and gaba (benzodiazepine) receptors in the sensory-motor cortex, hippcampus and spinal code

Frontal lobe samples of rat brains flown aboard Cosmos 1887 were processed for the study of muscarinic (cholinergic) and GABA (benzodiazepine) receptors and for immunocytochemical localization of the neurotransmitter gamma-aminobutyric acid (GABA) and glial fibrillary acidic protein (GFAP). Although radioactive labeling of both muscarinic cholinergic and GABA (benzodiazepine) receptors proved to be successful with the techniques employed, distinct receptor localization of individual laminae of the frontal neocortex was not possible since the sampling of the area was different in the various groups of animals. In spite of efforts made for proper orientation and regional identification of laminae, it was found that a densitometric (quantitation of autoradiograms) analysis of the tissue did not contribute to the final interpretation of the effects of weightlessness on these receptors. As to the immunocytochemical studies the use of both markers, GFAP and GABA antiserum, confirmed the suitability of the techniques for use in frozen material. However, similar problems to those encountered in the receptor studies prevented an adequate interpretation of the effects of micro-G exposure on the localization and distribution of GABA and GFAP. This study did, however, confirm the feasibility of investigating neurotransmitters and their receptors in future space flight experiments.

Daunton, N.↗
NASA NTRS1993

Tunneling magnetic force microscopy

We have developed a powerful new tool for studying the magnetic patterns on magnetic recording media. This was accomplished by modifying a conventional scanning tunneling microscope. The fine-wire probe that is used to image surface topography was replaced with a flexible magnetic probe. Images obtained with these probes reveal both the surface topography and the magnetic structure. We have made a thorough theoretical analysis of the interaction between the probe and the magnetic fields emanating from a typical recorded surface. Quantitative data about the constituent magnetic fields can then be obtained. We have employed these techniques in studies of two of the most important issues of magnetic record: data overwrite and maximizing data-density. These studies have shown: (1) overwritten data can be retrieved under certain conditions; and (2) improvements in data-density will require new magnetic materials. In the course of these studies we have developed new techniques to analyze magnetic fields of recorded media. These studies are both theoretical and experimental and combined with the use of our magnetic force scanning tunneling microscope should lead to further breakthroughs in the field of magnetic recording.

Burke, Edward R.↗
NASA NTRSDate not supplied

Atomic Oxygen Environment and Effects Overview

Atomic oxygen is the most predominant constituent in the low Earth orbital environment between the altitudes of 180 and 650 km. It is also a major constituent of the Mars orbital environment. It is very chemically reactive and can oxidize many spacecraft surfaces to form volatile reaction products. The importance of understanding atomic oxygen reactions with materials has led to both flight experiments in low Earth orbit and ground-based testing in vacuum chambers containing atomic oxygen to study its’ effect on materials. Testing has been performed in order to determine the extent of the atomic oxygen reaction and assess material and component durability. In addition, the effectiveness of mitigation techniques such as application of a protective coating, adding fillers, or using shielding and getter materials has also been studied both in flight and ground-based experiments. This presentation will focus on defining atomic oxygen environments, discussing its effect on spacecraft materials, and describing some of the testing and mitigation techniques that have been investigated.

Atomic Oxygen, Low Earth Orbit, Low Mars Orbit, ox↗
NASA NTRS2001

Composites: Processing and Fabrication Methodologies of Nonoxide Ceramic Composites. Processing HfB2 Composites for Use in Extreme Environments

HfB2 and ZrB2 composites containing SiC are known to have good thermal shock and configurational stability at elevated temperatures. These are promising ultra-high temperature ceramics (UHTCs) for use on the sharp leading edges of next generation space vehicles. Sharp leading edges on these vehicles will need to: withstand repeated exposures to temperatures > 2200 C in oxidizing environments; have good thermal shock and ablation resistance; and withstand the mechanical stress of launch and reentry. The HfB2/SiC composite is currently undergoing processing improvements in an effort to better the performance of a material that has been studied for approx. 35 years. The potential for HfB2/SiC composites to meet the requirements of hypersonic flight depends on controlling processing techniques. This presentation will focus on understanding processing steps now being undertaken to optimize the material properties of HfB2/SiC composites at NASA Ames Research Center. Correlation between processing techniques and microstructure will be shown. Preliminary oxidation studies will also be discussed.

Gusman, Michael I.↗
NASA NTRS1974

Studies of liquid floating zones on SL-IV, the third Skylab mission

The behavior of liquid floating zones in a zero-gravity environment was studied by Dr. E. Gibson on SL-4. These experiments were designed from the results of previous work on floating zones in a simulated zero-gravity model. Molten floating zones are used on earth for the crystal growth and zone refining of reactive materials. The Skylab studies give some insight into the problems associated with the development of the technique for the future space processing of materials. Preliminary results are presented on the stability of the liquid zone surface under static, rotational and vibrational conditions without gravitational constraints.

Carruthers, J. R.↗
NASA NTRS2006

Use of Atmospheric Glow Discharge Plasma to Modify Spaceport Materials

Numerous materials used in spaceport operations require stringent evaluation before they can be utilized. It is critical for insulative polymeric materials that any surface charge be dissipated as rapidly as possible to avoid Electrostatic Discharges (ESD) that could present a danger. All materials must pass the Kennedy Space Center (KSC) standard electrostatic test [1]; however several materials that are considered favorable for Space Shuttle and International Space Station use have failed. Moreover, to minimize contamination of Mars spacecraft, spacecraft are assembled under cleanroom conditions and specific cleaning and sterilizing procedures are required for all materials. However, surface characteristics of these materials may allow microbes to survive by protecting them from sterilization and cleaning techniques. In this study, an Atmospheric Pressure Glow Discharge Plasma (APGD) [2] was used to modify the surface of several materials. This allowed the materials surface to be modified in terms of hydrophilicity, roughness, and conductivity without affecting the bulk properties. The objectives of this study were to alter the surface properties of polymers for improved electrostatic dissipation characteristics, and to determine whether the consequent surface modification on spaceport materials enhanced or diminished microbial survival.

Trigwell, S.↗
NASA NTRS1973

The earth's gravitational field from the combination of satellite and terrestrial data

This paper reviews techniques and results in the combination of gravimetric and satellite data. The estimation of mean anomalies for use in combination studies is discussed with the location of current gravity material being described. Specific techniques for combination solutions are discussed for various models. These models include those where the gravitational field is represented by a set of potential coefficients, or by a set of discrete blocks distributed on the earth. The potential coefficient solutions compared are those of the SAO Standard Earth II and III, the Goddard Earth Model 4, and a solution by the author. These solutions are compared in terms of coefficients, undulation and anomaly differences, and implied anomaly degree variances. In addition, comparisons were made through terrestrial anomaly comparisons, astrogeodetic undulation comparisons, and orbit fitting tests.

Rapp, R. H.↗
NASA NTRS1992

Nondestructive evaluation of ceramic and metal matrix composites for NASA's HITEMP and enabling propulsion materials programs

In a preliminary study, ultrasonic, x-ray opaque, and fluorescent dye penetrants techniques were used to evaluate and characterize ceramic and metal matrix composites. Techniques are highlighted for identifying porosity, fiber alignment, fiber uniformity, matrix cracks, fiber fractures, unbonds or disbonds between laminae, and fiber-to-matrix bond variations. The nondestructive evaluations (NDE) were performed during processing and after thermomechanical testing. Specific examples are given for Si3N4/SiC (SCS-6 fiber), FeCrAlY/Al2O3 fibers, Ti-15-3/SiC (SCS-6 fiber) materials, and Si3N4/SiC (SCS-6 fiber) actively cooled panel components. Results of this study indicate that the choice of the NDE tools to be used can be optimized to yield a faithful and accurate evaluation of advanced composites.

Generazio, Edward R.↗
NASA NTRS2007

Novel Thin Film Sensor Technology for Turbine Engine Hot Section Components

Degradation and damage that develops over time in hot section components can lead to catastrophic failure of the turbine section of aircraft engines. A range of thin film sensor technology has been demonstrated enabling on-component measurement of multiple parameters either individually or in sensor arrays including temperature, strain, heat flux, and flow. Conductive ceramics are beginning to be investigated as new materials for use as thin film sensors in the hot section, leveraging expertise in thin films and high temperature materials. The current challenges are to develop new sensor and insulation materials capable of withstanding the extreme hot section environment, and to develop techniques for applying sensors onto complex high temperature structures for aging studies of hot propulsion materials. The technology research and development ongoing at NASA Glenn Research Center for applications to future aircraft, launch vehicles, space vehicles, and ground systems is outlined.

Wrbanek, John D.↗