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At least 109 records · Page 6

The fracture morphology of nickel-base superalloys tested in fatigue and creep-fatigue at 650 C

The fracture surfaces of compact tension specimens from seven nickel-base superalloys fatigue tested at 650 C were studied by scanning electron microscopy and optical metallography to determine the nature and morphology of the crack surface in the region of stable growth. Crack propagation testing was performed as part of an earlier study at 650 C in air using a 0.33 Hz fatigue cycle and a creep-fatigue cycle incorporating a 900 second dwell at maximum load. In fatigue, alloys with a grain size greater than 20 micrometers, HIP Astroloy, Waspaloy, and MERL 76, exhibited transgranular fracture. MERL 76 also displayed numerous fracture sites which were associated with boundaries of prior powder particles. The two high strength, fine grain alloys, IN 100 and NASA IIB-7, exhibited intergranular fracture. Rene 95 and HIP plus forged Astroloy displayed a mixed failure mode that was transgranular in the coarse grains and intergranular in the fine grains. Under creep-fatigue conditions, fracture was found to be predominantly intergranular in all seven alloys.

Gayda, J.↗

Definition of Mutually Optimum NDI and Proof Test Criteria for 2219 Aluminum Pressure Vessels. Volume 2: Optimization and Fracture Studies

Certain behavioral aspects associated with fracture and crack extension that cannot be studied using other techniques were evaluated with the ultrasonic method. Characterization of collimated beam techniques showed that significant beam width reduction could be accomplished. Techniques for collimation are given. The crack-opening displacement-gage correction-factor study showed that displacement resulting from crack opening and that from plasticity could be readily differentiated. Crack closure studies using both ultrasonic and crack-opening displacement measurements showed an opening and closing behavior associated with load-unload curves. The results of this work were in general agreement with the closure concepts of Elber. Ultrasonic measurements used to study the nature of flaw extension characteristics associated with failure of the ligament between the flaw front and back surface showed that penetration could occur by an abrupt fracturing after subcritical growth or by continuous growth.

Schwartzberg, F. R.↗

Hypervelocity Dust Impact in Olivine: Fib/Tem Characterization and Comparison of Experimental and Natural Microcraters

The flux of objects impacting the surfaces of solar system airless bodies is dominated by micrometeoroids less than 1 mm diameter whose impact effects play a major role in the space weathering of airless body surfaces. To obtain better understanding of how small scale impact effects vary as a function of impact speed in an important lunar and asteroidal mineral, we produced artificial microcraters in San Carlos olivine using Fe metal dust particles 0.10 to 5 µm in diameter electrostatically accelerated to speeds between 0.35 to 25 km s-1. The crater morphologies, size distrrubiton and microstruc-tures were characterized by field-emission SEM (FE-SEM) and also by FIB cross sectioning of selected craters for field-emission scanning transmission electron microscopy (FE-STEM). These same techniques were also applied to study a natural 20 µm-diameter microcrater in a olivine grain on the surface of lunar rock 12075. Measured microcrater diameters in the experimental sample range between 0.20 to 5 µm with larger craters having more irregular outlines dominated by spallation fractures. FE-SEM and FE-STEM imaging docu-ment the formation of shock melt in the size population of experimental craters below approximately 1 µm in diameter, corresponding to particle impact speeds in the 10-25 km s-1 range. The natural olivine crater exhibits similar shock melt features along the perimeter of its cavity, but the shock melt also contains nanophase Fe metal particles, something not observed in the experimental samples. FE-STEM imaging of the experimental craters reveals complex shock-generated dislocation and nanofracture microstructures in zones extend-ing 1-2 µm into the olivine from the crater cavity. The natural microcrater shows a lower density of shock-generated disloca-tions that extends a factor of 2 deeper into the the olivine than in the experimental samples.

Roy Gray Christoffersen↗

Fundamental tribological properties of ceramics

When a ceramic is brought into contact with itself, another ceramic, or a metal, strong bond forces can develop between the materials. Adhesion between a ceramic and itself or another solid are discussed from a theoretical consideration of the nature of the surfaces and experimentally by relating bond forces to the interface resulting from solid state contact. Elastic, plastic, and fracture behavior of ceramics in solid-state contact are discussed as they relate to friction and wear. The contact load necessary to initiate fracture in ceramics is shown to be appreciably reduced with tangential motion. Both friction and wear of ceramics are anisotropic and relate to crystal structure as with metals. Both free energy of oxide formation and the d valence bond character of metals are related to the friction and wear characteristics for metals in contact with ceramics. Lubrication is found to increase the critical load necessary to initiate fracture of ceramics with sliding or rubbing contact.

Buckley, D. H.↗

Fundamental tribological properties of ceramics

When a ceramic is brought into contact with itself, another ceramic, or a metal, strong bond forces can develop between the materials. Adhesion between a ceramic and itself or another solid are discussed from a theoretical consideration of the nature of the surfaces and experimentally by relating bond forces to the interface resulting from solid state contact. Elastic, plastic, and fracture behavior of ceramics in solid-state contact are discussed as they relate to friction and wear. The contact load necessary to initiate fracture in ceramics is shown to be appreciably reduced with tangential motion. Both friction and wear of ceramics are anisotropic and relate to crystal structure as with metals. Both free energy of oxide formation and the d valence bond character of metals are related to the friction and wear characteristics for metals in contact with ceramics. Lubrication is found to increase the critical load necessary to initiate fracture of ceramics with sliding or rubbing contact.

Buckley, D. H.↗

A Mars 2020 Perseverance SuperCam Perspective on the Igneous Nature of the Máaz Formation at Jezero Crater, Mars

The Mars2020 Perseverance rover landed in Jezero crater in February 2020,and first encountered the Máaz formation (or Crater floor-fractured rough(Cf-fr) unit previously mapped based on orbital data[1]).In this study, we use data from the SuperCam instrument(SCAM) to show that the Máaz formation has an igneous origin. SuperCam is a remote-sensing instrument onboard Perseverance, and investigates the texture, mineralogy, and chemistry of rocks and soils, as well as atmospheric features [2,3]. SuperCam comprises the Remote Micro Imager (RMI) to provide high-resolution images, laser-induced breakdown spectroscopy (LIBS)to investigate the major and minor element chemistry of materials, Raman, and passive visible-near infrared (VISIR) spectroscopy to analyze the mineralogy of targets, and time-resolved luminescence spectroscopy (TRLS)to measure organic fluorescence and inorganic luminescence. In addition, the microphone (MIC) can constrain the rock hardness through measurements of the shockwave of LIBS shots. In this study, we use LIBS-based major-oxide compositions (MOC),quantified using the calibration in [2].

Mars 2020↗

Mechanical Properties of Aerogels

Aerogels are extremely low density solids that are characterized by a high porosity and pore sizes on the order of nanometers. Their low thermal conductivity and sometimes transparent appearance make them desirable for applications such as insulation in cryogenic vessels and between double paned glass in solar architecture. An understanding of the mechanical properties of aerogels is necessary before aerogels can be used in load bearing applications. In the present study, the mechanical behavior of various types of fiber-reinforced silica aerogels was investigated with hardness, compression, tension and shear tests. Particular attention was paid to the effects of processing parameters, testing conditions, storage environment, and age on the aerogels' mechanical response. The results indicate that the addition of fibers to the aerogel matrix generally resulted in softer, weaker materials with smaller elastic moduli. Furthermore, the testing environment significantly affected compression results. Tests in ethanol show an appreciable amount of scatter, and are not consistent with results for tests in air. In fact, the compression specimens appeared to crack and begin to dissolve upon exposure to the ethanol solution. This is consistent with the inherent hydrophobic nature of these aerogels. In addition, the aging process affected the aerogels' mechanical behavior by increasing their compressive strength and elastic moduli while decreasing their strain at fracture. However, desiccation of the specimens did not appreciably affect the mechanical properties, even though it reduced the aerogel density by removing trapped moisture. Finally, tension and shear test results indicate that the shear strength of the aerogels exceeds the tensile strength. This is consistent with the response of brittle materials. Future work should concentrate on mechanical testing at cryogenic temperatures, and should involve more extensive tensile tests. Moreover, before the mechanical response of reinforced aerogels can be fully understood, more tests of unreinforced aerogels are necessary. Unreinforced aerogels are of particular use because their birefringent nature allows for visual determination of stress fields during mechanical testing. The success of any future tests depends on the availability of a large supply of quality specimens with well-documented preparation and storage histories.

Parmenter, Kelly E.↗

Comparisons of various configurations of the edge delamination test for interlaminar fracture toughness

Various configurations of Edge Delamination Tension (EDT) test specimens, of both brittle (T300/5208) and toughened-matrix (T300/BP907) graphite reinforced composite laminates, were manufactured and tested. The mixed-mode interlaminar fracture toughness, G sub C, was measured using (30/30 sub 2/30/90 sub N)sub s, n=1 or 2, (35/-35/0/90) sub s and (35/0/-35/90) sub s layups designed to delaminate at low tensile strains. Laminates were made without inserts so that delaminations would form naturally between the central 90 deg plies and the adjacent angle plies. Laminates were also made with Teflon inserts implanted between the 90 deg plies and the adjacent angle (theta) plies at the straight edge to obtain a planar fracture surface. In addition, interlaminar tension fracture toughness, GIc, was measured from laminates with the same layup but with inserts in the midplane, between the central 90 deg plies, at the straight edge. All of the EDT configurations were useful for ranking the delamination resistance of composites with different matrix resins. Furthermore, the variety of layups and configurations available yield interlaminar fracture toughness measurements needed to generate delamination failure criteria. The influence of insert thickness and location, and coupon size on G sub c values were evaluated.

Obrien, T. K.↗

Predicting the time-temperature dependent axial failure of B/A1 composites

Experimental and theoretical studies were conducted in order to understand and predict the effects of time, temperature, and stress on the axial failure modes of boron fibers and B/A1 composites. Due to the anelastic nature of boron fiber deformation, it was possible to determine simple creep functions which can be employed to accurately describe creep and fracture stress of as-produced fibers. Analysis of damping and strength data for B/6061 A1 composites indicates that fiber creep effects of creep on fiber fracture are measurably reduced by the composite fabrication process. The creep function appropriate for fibers with B/Al composites was also determined. A fracture theory is presented for predicting the time-temperature dependence of the axial tensile strength for metal matrix composites in general and B/A1 composites in particular.

Dicarlo, J. A.↗

The Characteristics of Fatigue Damage in the Fuselage Riveted Lap Splice Joint

An extensive data base has been developed to form the physical basis for new analytical methodology to predict the onset of widespread fatigue damage in the fuselage lap splice joint. The results of detailed destructive examinations have been cataloged to describe the physical nature of MSD in the lap splice joint. ne catalog includes a detailed description, e.g., crack initiation, growth rates, size, location, and fracture morphology, of fatigue damage in the fuselage lap splice joint structure. Detailed examinations were conducted on a lap splice joint panel removed from a full scale fuselage test article after completing a 60,000 cycle pressure test. The panel contained a four bay region that exhibited visible outer skin cracks and regions of crack link-up along the upper rivet row. Destructive examinations revealed undetected fatigue damage in the outer skin, inner skin, and tear strap regions. Outer skin fatigue cracks were found to initiate by fretting damage along the faying surface. The cracks grew along the faying surface to a length equivalent to two to three skin thicknesses before penetrating the outboard surface of the outer skin. Analysis of fracture surface marker bands produced during full scale testing revealed that all upper rivet row fatigue cracks contained in a dim bay region grow at similar rates; this important result suggests that fracture mechanics based methods can be used to predict the growth of outer skin fatigue cracks in lap splice structure. Results are presented showing the affects of MSD and out-of-plane pressure loads on outer skin crack link-up.

Piascik, Robert S.↗

Predicting the time-temperature dependent axial failure of B/Al composites

Theoretical and experimental studies are reviewed whose objective was to gain insight into and predict the effects of time, temperature, and stress on the axial failure modes of boron fibers and B/Al composites. Owing to the inelastic nature of boron fiber deformation, it proved possible to develop simple creep functions which can be used to describe accurately the creep and fracture stress of as-produced fibers. Analysis of damping and stress data for B/6061 Al composites indicates that fiber creep and the effects of creep of fiber fracture are measurably reduced by the composite fabrication process.

Dicarlo, J. A.↗

The crack problem for a half plane stiffened by elastic cover plates

An elastic half plane containing a crack and stiffened by a cover plate is discussed. The asymptotic nature of the stress state in the half plane around an end point of the stiffener to determine the likely orientation of a possible fracture initiation and growth was studied. The problem is formulated for an arbitrary oriented radial crack in a system of singular integral equations. For an internal crack and for an edge crack, the problem is solved and the stress intensity factors at the crack tips and the interface stress are calculated. A cracked half plane with two symmetrically located cover plates is also considered. It is concluded that the case of two stiffeners appears to be more severe than that of a single stiffener.

Delale, F.↗

Evaluation of proof testing as a means of assuring mission success for the Space Shuttle thermal protection system

The reliability analysis of a thermal protection system (TPS) incorporating low density, fibrous ceramic materials must take into account the time-dependency and variability of the system's strength. Fracture mechanics concepts can be used to estimate the allowable strength and expected lifetime, as well as to define a proof test scheme for assuring mission success of TPS. The aim of this study was to evaluate the proof testing scheme used on the TPS of the Space Shuttle with these fracture mechanics concepts. The analysis confirmed that proof testing was necessary for the undensified system and that proof testing should lead to adequate reliability with respect to the design stresses. For the undensified system, fracture mechanics predictions were confirmed by measuring the strength of samples that survived proof testing. It was also found that the time-dependent nature of the system's strength was controlled mainly by the ceramic and that this time-strength dependency is similar to that observed for bulk glasses that have compositions similar to the glass fibers present in the ceramic tiles.

Green, D. J.↗

Experimental Impacts into Chondritic Targets: Disruption of an L6 Chondrite by Multiple Impacts - Part 1

A fragment of an L6 chondrite (ALH 85017,13) with an initial mass (M(sub 0)) of 464.1 g was the target in a series of experimental impacts in which the largest remaining fragment (M(sub R)) after each shot was impacted by a 3.18-mm ceramic sphere at a nominal speed of 2 km/s. This continued until the mass of the largest remaining piece was less than half the mass of the target presented to that shot (M(sub S)). Two chunks of Bushveldt gabbro with similar initial masses were also impacted under the same conditions until M(sub R) was less than half M(sub 0). The two gabbro targets required a total of 1.51x10(exp 7) and 1.75x10(exp 7) erg/g to attain 0.27 and 0.33 M(sub R)/M(sub 0), respectively; the chondrite, however, was considerably tougher, reaching 0.40 and 0.21 M(sub R)/M(sub 0) only after receiving 2.37x10(exp 7) and 3.10x10(exp 7) erg g-1, respectively. The combined ejecta and spallation products from the gabbro impacts were coarser than those from the chondrite and in sufficient quantities that the new surface areas exceeded those from the meteorite until the fifth shot in the chondrite series, which was the number of impacts required to disrupt each gabbro target (i.e., MR/M0 = 0.5). Unlike the behavior shown in previous regolith-evolution series, neither gabbro target produced an enhancement in the size fraction reflecting the mean size of the crystals composing the rock (about 3 mm), an effect possibly related to the width of the shock pulse. The original chondrite was so fine-grained and fractured, and the variance in its grain-size distribution so large, that effects related to grain-size were relegated to the <63- m fraction. Impacts into ALH 85017 produced abundant, fine-grained debris, but otherwise the slopes of its size distributions were comparable to those from other experiments involving natural and fabricated terrestrial targets. The characteristic slopes of the chondrite's size distributions, however, were notably more constant over the entire nine-impact series than those from any of the terrestrial targets, a testament to the control over comminution apparently exerted by pre-existing fractures and other, microscopic damage in the meteorite. The enhancement in the finer fraction of debris from ALH 85017 indicates that ordinary chondrites in solar orbit would be very efficient contributors to the cosmic-dust complex. At the same time, the greater resistance to disruption displayed by ordinary chondrites relative to that exhibited by igneous rocks indicates that a selection effect could be operative between the annealed, ordinary-chondritic breccias and relatively weaker, differentiated meteorites. Preferential survival from their time in the regoliths of their parent bodies through their transit to Earth and passage through the atmosphere suggests that meteorite collections could be biased in favor of the ordinary chondrites.

Cintala, Mark J.↗

The mechanisms of dispersion strengthening and fracture in Al-based XD(tm) alloys, part 1

The influence of reinforcement size, volume fraction, and matrix deformation behavior on room and elevated temperature strength; the fracture toughness; and the fatigue crack growth rate of metal matrix composites of Al-4(pct)Cu-1.5(pct)Mg with TiB2 were examined. The influence of reinforcement volume fraction was also examined for pure aluminum with TiB2. Higher TiB2 volume fractions increased the tensile yield strength at both room and elevated temperatures, and reduced the elongation to fracture. Tensile tests also indicate that small particles provided a greater increase in strength for a given volume fraction than larger particles, whereas elongation to fracture appeared to be insensitive to reinforcement size. Interparticle spacing appears to be the factor that controls the strength of these alloys, with the exact nature of the dependence relying on the nature of dislocation slip in the matrix (planar vs. diffuse). The isothermal aging response of the precipitation strengthened Al-4(pct)Cu-1.5(pct)Mg alloys was not accelerated by the presence of TiB2. Cold work prior to artificial aging created additional geometrically necessary dislocations which serve as heterogeneous nucleation sites leading to accelerated aging, a finer precipitate size, and an increase in the strength of the alloy.

Aikin, R. M., Jr.↗

Floor-fractured crater models of the Sudbury structure, Canada

The Sudbury structure in Ontario, Canada, is one of the oldest and largest impact structures recognized in the geological record. It is also one of the most extensively deformed and volcanically modified impact structures on Earth. Although few other terrestrial craters are recognized as volcanically modified, numerous impact craters on the Moon have been volcanically and tectonically modified and provide possible analogs for the observed pattern of modification at Sudbury. We correlate the pattern of early deformation at Sudbury to fracture patterns in two alternative lunar analogs and then use these analogs both to estimate the initial size of the Sudbury structure and to model the nature of early crater modification at Sudbury.

Wichman, R. W.↗

T0TEM - T0 Test Evaluation Module Development and Verification

Transition temperature testing of ferritic steels evaluates the ductile to brittle transition temperature, where the behavior of the steel changes from controlled ductile tearing to uncontrollable brittle fracture. This testing is governed by ASTM (American Society of Testing and Materials) E1921 standard. The calculations and plots required by this standard are iterative in nature and require significant effort to produce by standard hand calculations. In addition to analysis of a complete data set, intermediate analysis during testing is beneficial to determine optimal test temperatures. Given the exhaustive nature of calculating the transition temperature, being able to quickly update target temperatures is a significant benefit to not only the quality of tests, but the number of required tests as well. T0 Test Evaluation Module (T0TEM) v1.5 is a software application created under the Layered Pressure Vessel (LPV) certification effort. To reduce the analysis time of transition temperature test data sets producedfor this effort, T0TEM was created to calculate the E1921 Master Curve along with all required data and validity checks. By creating this program, hundreds of hours of analysis time were saved. In addition, the creation of a standard program provided a significant improvement in the consistency with which results were reported. T0TEM also calculates the results and plots required for the E1921 inhomogeneity annex to determine whether a material behaves in a homogenous manner. This program was created by Levi Shelton and Cameron Bosley at NASA, with input and review from the E1921 committee. The results generated by T0TEM were compared to the validation data sets provided by ASTM with good concurrence. ASTM committee members have reviewed and applied T0TEM to other data sets with satisfactory results. T0TEM was originally released to the NASA Software Repository and publicly via SourceForge in May of 2020. Version 1.5 was released in April of 2021 with minor functionality updates and additional statistical analysis methods.

Levi Shelton↗

Neutron starquakes and the nature of gamma-ray bursts

The possibility that gamma-ray bursts originate from quakes deep in the solid crust of a neutron star is investigated. Seismic waves are radiated if shear stress is relieved by brittle fracture. However they cannot propagate directly to the surface but are temporarily trapped below a reflecting layer. The shaking of the stellar surface couples the seismic waves to Alfven waves which propagate out into the magnetosphere. The crust-magnetosphere transmission coefficient strongly increases with wave frequency and magnetic field strength. Alfven wave luminosities sufficient to power galactic gamma-ray bursts are possible if magnetic fields greater than 100 billion G cover at least part of the stellar surface. As the Alfven waves propagate out into the low density magnetosphere, they become increasingly charge starved, thereby accelerating particles to relativistic energies.

Madau, P.↗