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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 109 records · Page 6
All sourcesNASA NTRSDOE OSTI
NASA NTRS1990

Fractography of composite delamination

The microdamage that occurs for Mode 1 and Mode 2 delamination was examined by potting delaminated specimens in a clear epoxy, sectioning through the damage, polishing the cut sections and examining using light microscopy. For Mode 1 delamination of unidirectional carbon fiber reinforced plastic (CFRP) composites, the major observation was fiber bridging including large ligaments of fiber bundles. The Mode 2 delamination of unidirectional laminates revealed a very narrow crack opening with only occasional fiber bridging. Impact testing by repetitive impacts with increasing energy was studied and it was found that this technique does not discern changes in the type of damage with increasing cumulative impact energy. Instead, the changes in the impact response, notably stiffness, are the result of changes in the extent of damage. For laminates with a brittle thermoplastic matrix, 3501-6, there were distinct changes in stiffness that corresponded to the development of through the thickness damage and then to the extension of the damage to the specimen edges. For PEEK and polycarbonate, the changes in stiffness were not as abrupt as for the thermoset. None the less, the damage progressed in the same manner.

Bascom, W. D.↗
NASA NTRS1990

Improved melt flow and physical properties of Mitsui Toatsu's LARC-TPI 1500 series polyimide

The basic thermal properties and melt behavior of an improved form of LARC-TPI polyimide, LARC-TPI 1500, are investigated and compared with those of LARC-TPI 1000 and 2000. The LARC-TPI 1500 powders are thermally stable and melt processable. The absolute molecular weight of the polymer varies from 20,000 to 30,000, indicating recurring unit numbers of about 40-60. The melt flow properties of LARC-TPI 1500 are comparable to those of other engineering plastics, such as PEEK, PSU, and PES. The flexural modulus of injection molded parts of LARC-TPI 1500 is the highest among commercial thermoplastic polymers.

Ohta, Masahiro↗
NASA NTRS1991

Impact response of composite materials

Composite materials composed of carbon fibers and resin matrices offer great promise in reducing the weight of aerospace structures. However they remain extremely vulnerable to out of plane impact loads, which lead to severe losses in strength and stiffness. The results of an experimental program, undertaken to investigate the low velocity impact damage tolerance of composite materials is presented. The objectives were to identify key neat resin/composite properties that lead to enhancement of composite impact damage tolerance and to find a small scale test that predicts compression after impact properties of panels. Five materials were selected for evaluation. These systems represented different classes of material behavior such as brittle epoxy, modified epoxies, and amorphous and semicrystalling thermoplastics. The influence of fiber properties on the impact performance was also studied in one material, i.e., in polyether ether ketone (PEEK). Several 24 and 48 ply quasi-isotropic and 24 ply orthotropic laminates were examined using an instrumented drop weight impactor. Correlations with post impact compression behavior were made.

Tiwari, S. N.↗
NASA NTRS1992

Scaling effects in angle-ply laminates

The effect of specimen size upon the response and strength of +/- 45 degree angle-ply laminates was investigated for two graphite fiber reinforced plastic systems and several stacking sequences. The first material system was a brittle epoxy based system, AS4 fibers in 3502 epoxy, and the second was a tough thermoplastic based system, AS4 fibers in PEEK matrix. For the epoxy based system, two generic +/- 45 degree lay-ups were studied: (+45 degrees sub n/-45 degrees sub n) sub 2S (blocked plies), and (+45 degrees/-45 degrees) sub 2nS, for n=1 and 2. The in-plane dimensions of the specimens were varied such that the width/length relationship was 12.7 x n/127 x n mm, for m=1, 2, 3, or 4. It is shown that the stress/strain response and the ultimate strength of these angle-ply laminates depends on the laminate thickness and the type of generic lay-up used. Furthermore, it is shown that first ply failure occurs in the surface plies as a result of normal rather than shear stresses. The implications of the experimental findings upon the validity of the +/- 45 degree tensile test which is used to determine the in-plane shear response of unidirectional composites are discussed.

Kellas, Sotiris↗
NASA NTRS1992

Property changes induced by the space environment in polymeric materials on LDEF

Property changes that occurred in four groups of polymer-based materials in the Long Duration Exposure Facility (LDEF) due to exposure to the outer space environment for 5.8 yrs are examined. Evaluations of contamination and mass loss are presented along with optical, thermal, and electrical analyses and mechanical property evaluations for TFE Teflon, the fluorinated material Halar, the silicone-based material RTV 511, and PEEK resin.

Whitaker, Ann F.↗
NASA NTRS1991

Composite materials: Fatigue and fracture. Vol. 3

The present volume discusses topics in the fields of matrix cracking and delamination, interlaminar fracture toughness, delamination analysis, strength and impact characteristics, and fatigue and fracture behavior. Attention is given to cooling rate effects in carbon-reinforced PEEK, the effect of porosity on flange-web corner strength, mode II delamination in toughened composites, the combined effect of matrix cracking and free edge delamination, and a 3D stress analysis of plain weave composites. Also discussed are the compression behavior of composites, damage-based notched-strength modeling, fatigue failure processes in aligned carbon-epoxy laminates, and the thermomechanical fatigue of a quasi-isotropic metal-matrix composite.

O'Brien, T. K.↗
NASA NTRS1991

Composite plates impact damage - An atlas

The present volume on impact damage in composite plates presents an extensive compendium of visual and graphic data regarding a variety of material and impactor parameters. The photographs are taken with X-ray and C-scan imaging in conjunction with a dye penetrant to show matrix cracks and delaminations. Impact and static-loading tests are performed on plates of graphite-epoxy, graphite-toughened epoxy, and graphite-PEEK materials. The images are presented to yield specific visual data regarding such parameters as impactor velocity, thickness of the back ply group, impactor nose radius, and the effects of multiple delaminations. The images are grouped in eight subsets that correspond to parameters including plate length, material, and the difference in fiber orientation between adjacent ply groups. This substantial volume represents a systematic effort to study the effects of several material parameters on impact damage.

Finn, Scott R.↗
NASA NTRS1992

Compressive strength of damaged and repaired composite plates

Tests were performed assessing the effectiveness of repair in restoring the mechanical properties of damaged, solid composite plates made either of Fiberite T300/976 graphite-epoxy, Fiberite IM7/977-2 graphite-toughened epoxy, or ICI APC-2 graphite-PEEK. The plate length, the layup and the amount of damage were also varied. Damage was introduced in the plates either by impacting them with a solid projectile or by applying a transverse static load. Some (75 percent) or all (100 percent) of the damaged zone was then cut out, and the plate was repaired by plugging and patching the hole. The effectiveness of the repair was evaluated by measuring the compressive strengths of undamaged plates, damaged plates with no cutout, damaged plates with a cutout, and repaired plates. The data at an intermediate stage of repair provide information on the effect of each repair step on the compressive strength. The results indicated that for the solid plates used in these tests, the repair methods used herein did not improve the compressive strength of already damaged plates.

Finn, Scott R.↗
NASA NTRS1993

The Design of Mechanically Compatible Fasteners for Human Mandible Reconstruction

Mechanically compatible fasteners for use with thin or weakened bone sections in the human mandible are being developed to help reduce large strain discontinuities across the bone/implant interface. Materials being considered for these fasteners are a polyetherertherketone (PEEK) resin with continuous quartz or carbon fiber for the screw. The screws were designed to have a shear strength equivalent to that of compact/trabecular bone and to be used with a conventional nut, nut plate, or an expandable shank/blind nut made of a ceramic filled polymer. Physical and finite element models of the mandible were developed in order to help select the best material fastener design. The models replicate the softer inner core of trabecular bone and the hard outer shell of compact bone. The inner core of the physical model consisted of an expanding foam and the hard outer shell consisted of ceramic particles in an epoxy matrix. This model has some of the cutting and drilling attributes of bone and may be appropriate as an educational tool for surgeons and medical students. The finite element model was exercised to establish boundary conditions consistent with the stress profiles associated with mandible bite forces and muscle loads. Work is continuing to compare stress/strain profiles of a reconstructed mandible with the results from the finite element model. When optimized, these design and fastening techniques may be applicable, not only to other skeletal structures, but to any composite structure.

Roberts, Jack C.↗
NASA NTRS1991

Delaminations in composite plates under impact loads

A method is presented for calculating the locations, shapes, and sizes of delaminations which occur in a fiber reinforced composite plate subjected to non-penetrating (low velocity) impact of a solid object. The plate may be simply supported, clamped, or free along its edges. A failure model of the delamination formation was developed. This model was then coupled with a finite element analysis. The model and the finite element analysis were then implemented by a computer code (IMPACT-ST) which can be used to estimate the damage initiation load and the locations, shapes, and sizes of the delaminations. Tests were performed measuring the geometries of the delaminations in graphite-epoxy, graphite-toughened epoxy, and graphite-PEEK plates impacted by a projectile with a spherical tip having masses ranging from 0.355 lbm to 0.963 lbm and velocities from 50 in/sec to 225 in/sec. The data were compared to the results of the model, and good agreements were found between the measured and the calculated delamination lengths and widths.

Finn, Scott R.↗
NASA NTRS1991

Advanced fiber/matrix material systems

Work completed in Phase 1 of the NASA Advanced Composite Technology program is discussed. Two towpreg forms (commingled yarns and fused powder towpregs) are being characterized under the program. These towpregs will be used to evaluate textile fabrication technologies for advanced aircraft composite structures. The unique characteristic of both of these material forms is that both fiber and matrix resin are handled in a single operation such as weaving, braiding, or fiber placement. The evaluation of both commingled and fused powder towpreg is described. Various polymer materials are considered for both subsonic and supersonic applications. Polymers initially being evaluated include thermoplastic polyimides such as Larc-TPI and New-TPI, thermoplastics such as PEEK and PEKEKK as well as some toughened crosslinked polyimides. Preliminary mechanical properties as well as tow handling are evaluated.

Hartness, J. Timothy↗
NASA NTRS1992

Delaminations in composite plates under transverse static loads - Experimental results

Tests were performed measuring the damage initiation loads and the locations, shapes, and sizes of delaminations in Fiberite T300/976 graphite/epoxy, Fiberite IM7/977-2 graphite-toughened epoxy, and ICI APC-2 graphite-PEEK plates subjected to transverse static loads. The data were compared to the results of the Finn-Springer model, and good agreements were found between the measured and calculated delamination lengths and widths.

Finn, Scott R.↗
NASA NTRS1992

Properties of intermingled carbon/PEEK 3-D woven composites

The presence of voids is one of the major problems associated with resin infiltration techniques when using 3-D woven preforms. Efforts to reduce the voids invariably result in the creation of microcracks. In this paper, the use of PEEK fibers intermingled with carbon fibers into a multi-layer preform is discussed. Influence of processing parameters, such as temperature, pressure, and consolidation time, on the composite properties is presented. One of the issues emphasized is the effect of pressure on buckling of the Z-reinforcement fibers and the bending behavior.

Mohamed, M. H.↗
NASA NTRS1995

Effects of atomic oxygen on polymeric materials flown on EOIM-3

Diverse polymeric materials, including several variations of Kapton, were flown on STS-46 as part of the Evaluation of Oxygen Interaction with Materials Experiment (EOIM-3). These materials were flown in the cargo bay and exposed to the space environment July 31 - August 8, 1992, including 40 hours of direct atomic oxygen impingement. The atomic oxygen exposure was approximately 2.2 x 10(exp 20) atoms/sq cm. Polymeric materials flown on EOIM-3 include coated and uncoated Kapton, Tefzel ETFE, Lexan, FEP and TFE Teflon, bulk Halar and PEEK, S383 silicone and Viton elastomeric seal material. Analyses performed included thickness measurements using Dektak and eddy current methods, mass loss, resistance, permeability, hardness, and FTIR. The effects of stress and the space environment on Kapton were also evaluated. Previous EOIM missions on STS-5 and STS-8 and the Long Duration Exposure Facility also contained polymeric material samples. Data from these previous flights are shown for comparison, as well as ground simulation of space environment effects using both thermal energy flow tubes and 5 eV neutral atomic oxygen beam facilities. Reaction efficiencies for the various atomic oxygen exposure conditions are discussed.

Kamenetzky, Rachel R.↗
NASA NTRS1996

The history of transportation, with a peak into the future

In the first part of this presentation, a general historical review of the heydays of various modes of transportation will be given, where 'heydays' will be interpreted as periods of fundamental technological development. With this as background, focus will then be placed on the airplane -- the mode of transportation that has changed the world in the 20th century, and which in the minds of many has been the most important technological development in this century. The technical history of air transportation (the airplane) will be reviewed, with special emphasis on the aerodynamic evolution of the airplane. Some specific examples of pivotal technical advances (and breakthroughs) from the history of applied aerodynamics will be discussed. Finally, this historical perspective will be used to help us peek into the future of transportation in the 21st century.

Anderson, John D., Jr.↗
NASA NTRS1995

Evaluation of Thermal Control Coatings and Polymeric Materials Exposed to Ground Simulated Atomic Oxygen and Vacuum Ultraviolet Radiation

Numerous thermal control and polymeric samples with potential International Space Station applications were evaluated for atomic oxygen and vacuum ultraviolet radiation effects in the Princeton Plasma Physics Laboratory 5 eV Neutral Atomic Oxygen Facility and in the MSFC Atomic Oxygen Drift Tube System. Included in this study were samples of various anodized aluminum samples, ceramic paints, polymeric materials, and beta cloth, a Teflon-impregnated fiberglass cloth. Aluminum anodizations tested were black duranodic, chromic acid anodize, and sulfuric acid anodize. Paint samples consisted of an inorganic glassy black paint and Z-93 white paint made with the original PS7 binder and the new K2130 binder. Polymeric samples evaluated included bulk Halar, bulk PEEK, and silverized FEP Teflon. Aluminized and nonaluminized Chemfab 250 beta cloth were also exposed. Samples were evaluated for changes in mass, thickness, solar absorptance, and infrared emittance. In addition to material effects, an investigation was made comparing diffuse reflectance/solar absorptance measurements made using a Beckman DK2 spectroreflectometer and like measurements made using an AZ Technology-developed laboratory portable spectroreflectometer.

Kamenetzky, R. R.↗
NASA NTRS1998

Application of Rapid Prototyping Methods to High-Speed Wind Tunnel Testing

This study was undertaken in MSFC's 14-Inch Trisonic Wind Tunnel to determine if rapid prototyping methods could be used in the design and manufacturing of high speed wind tunnel models in direct testing applications, and if these methods would reduce model design/fabrication time and cost while providing models of high enough fidelity to provide adequate aerodynamic data, and of sufficient strength to survive the test environment. Rapid prototyping methods utilized to construct wind tunnel models in a wing-body-tail configuration were: fused deposition method using both ABS plastic and PEEK as building materials, stereolithography using the photopolymer SL-5170, selective laser sintering using glass reinforced nylon, and laminated object manufacturing using plastic reinforced with glass and 'paper'. This study revealed good agreement between the SLA model, the metal model with an FDM-ABS nose, an SLA nose, and the metal model for most operating conditions, while the FDM-ABS data diverged at higher loading conditions. Data from the initial SLS model showed poor agreement due to problems in post-processing, resulting in a different configuration. A second SLS model was tested and showed relatively good agreement. It can be concluded that rapid prototyping models show promise in preliminary aerodynamic development studies at subsonic, transonic, and supersonic speeds.

Springer, A. M.↗
NASA NTRS1998

High Strain Rate Deformation Modeling of a Polymer Matrix Composite: Matrix Constitutive Equations - Part 1

Recently applications have exposed polymer matrix composite materials to very high strain rate loading conditions, requiring an ability to understand and predict the material behavior under these extreme conditions. In this first paper of a two part report, background information is presented, along with the constitutive equations which will be used to model the rate dependent nonlinear deformation response of the polymer matrix. Strain rate dependent inelastic constitutive models which were originally developed to model the viscoplastic deformation of metals have been adapted to model the nonlinear viscoelastic deformation of polymers. The modified equations were correlated by analyzing the tensile/ compressive response of both 977-2 toughened epoxy matrix and PEEK thermoplastic matrix over a variety of strain rates. For the cases examined, the modified constitutive equations appear to do an adequate job of modeling the polymer deformation response. A second follow-up paper will describe the implementation of the polymer deformation model into a composite micromechanical model, to allow for the modeling of the nonlinear, rate dependent deformation response of polymer matrix composites.

Goldberg, Robert K.↗