Search NASA⌕ Search

SEARCH · Search NASA

Results for “Particulate Contamination”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 109 records · Page 6
All sourcesNASA NTRSDOE OSTI
NASA NTRS2003

Capabilities of the Materials Contamination Team at Marshall Space Flight Center

The Materials Contamination Team at the Marshall Space Flight Center (MSFC) has been recognized for its contributions supporting the National Aeronautics and Space Administration (NASA) spacecraft development programs. These programs include the Reusable Solid Rocket Motor (RSRM), Chandra X-Ray Observatory, and the International Space Station (ISS). The Environmental Effects Group, with the Materials Contamination Team and the Space Environmental Effects Team has been an integral part of NASA's success by the testing, evaluation, and qualification of materials, hardware, and processes. This paper focuses on the capabilities of the Materials Contamination Team. The Materials Contamination Team's realm of responsibility includes establishing contamination control during all phases of hardware development, including design, manufacturing, assembly, test, transportation, launch site processing, on-orbit exposure, return, and refurbishment. The team continues its mission of reducing the risk of equipment failure due to molecular or particulate contamination. Contamination is a concern in the Space Shuttle with sensitive bond-lines and reactive fluid (liquid oxygen) compatibility as well as for spacecraft with sensitive optics, such as Hubble Space Telescope and Chandra X-ray Observatory. The Materials Contamination Team has a variety of facilities and instrumentation capable of contaminant detection, identification, and monitoring. The team addresses material applications dealing with environments, including production facilities, clean rooms, and on-orbit exposure. The optically stimulated electron emission (OSEE) system, the Ultraviolet (UV) fluorescence (UVF) surface contamination detection, and the Surface Optics Corporation 400 (SOC 400) portable hand-held Fourier Transform Infrared (FTIR) spectrometer are state-of-the-art tools for in-process molecular contamination detection. The team of engineers and technicians also develop contamination calibration standards and evaluate new surface cleanliness inspection technologies. The team utilizes facilities for on-orbit simulation testing of materials for outgassing and molecular film deposition characteristics in the presence of space environmental effects, such as Atomic Oxygen (AO) and UV radiation exposure. The Materials Contamination Team maintains databases for process materials as well as outgassing and optical compatibility test results for specific environments.

Burns, Howard↗
NASA NTRS1983

Development of a clean optical telescope

Particulate contamination on astronomical mirrors degrades performance in two ways: by information loss by extinction of light; and background and noise from scattering, especially forward or Fraunhofer scattering. These effects were not generally understood, and an ambitious pilot program was outlined to measure particulate effects on telescope optical performance; develop prophylactic and cleaning procedures suitable for groundbased observatories; investigate by computational modelling the effects on telescopes in space; and communicate the results and concerns within the astronomical community.

Brown, R. A.↗
NASA NTRS2005

Analysis of Molecular Contamination on Genesis Collectors Through Spectroscopic Ellipsometry

Before the spacecraft returned to Earth in September, the Genesis mission had a preliminary assessment plan in place for the purpose of providing information on the condition and availability of collector materials to the science community as a basis for allocation requests. One important component of that plan was the evaluation of collector surfaces for molecular contamination. Sources of molecular contamination might be the on-orbit outgassing of spacecraft and science canister components, the condensation of thruster by-products during spacecraft maneuvers, or the condensation of volatile species associated with reentry. Although the non-nominal return of the Genesis spacecraft introduced particulate contamination to the collectors, such as dust and heatshield carbon-carbon, it is unlikely to have caused any molecular deposition. The contingency team's quick action in returning the damaged payload the UTTR cleanroom by 6 PM the evening of recovery help to ensure that exposure to weather conditions and the environment were kept to a minimum.

McNamara, K. M.↗
NASA NTRS1975

Contamination control in hybrid microelectronic modules. Part 3: Specifications for coating material and process controls

Resin systems for coating hybrids prior to hermetic sealing are described. The resin systems are a flexible silicone junction resin system and a flexible cycloaliphatic epoxy resin system. The coatings are intended for application to the hybrid after all the chips have been assembled and wire bonded, but prior to hermetic sealing of the package. The purpose of the coating is to control particulate contamination by immobilizing particles and by passivating the hybrid. Recommended process controls for the purpose of minimizing contamination in hybrid microcircuit packages are given. Emphasis is placed on those critical hybrid processing steps in which contamination is most likely to occur.

Himmel, R. P.↗
NASA NTRS1991

LDEF contaminants analysis data

Modification of surface texture for Ram Facing FEP Teflon on the Long Duration Exposure Facility (LDEF) satellite is documented. Photos of changes in surface texture if thermal blanket material with position on tray C-08 are presented. Infrared spectra and photographic documentation of molecular film deposits on LDEF surfaces by location is reported. Results of a survey of the functional groups and elemental composition of the brown film found widely distributed on the surface of LDEF is shown. A partial photographic catalog of LDEF particulate contaminants is included. A set of photos of particles collected or photographed in place on the surface of LDEF is shown. Particle counts and surface obscuration data for the LDEF satellite are reported. The surface data in tables and charts is presented for the LDEF satellite by location.

Crutcher, E. Russ↗
NASA NTRS1983

OSS-1/STS-3 Shuttle induced atmosphere experiment

Direct light form the Sun and the sunlit Earth, and indirect light from these same sources reflected off parts of the orbiter and its payload were the two major sources of light seen in the bay during spacecraft day. Brightness arising from sunlight reflected off particulates originating from the spacecraft (corona or induced atmosphere) were tentatively identified. Sources of light observed during spacecraft night include large scale diffuse glows associated with Vernier thruster firings, surface glows on the orbiter in the direction of orbiter n motion, and periodic sky brightness structures observed primarily at 4200 A and 6300 A. Some information was obtained on the size and trajectories of individual contaminant particulates. Astronomical data were obtained from large regions of the Milky Way and zodiacal light, including large regions to within 35 deg of the Sun and possibly closer. Coordinated and sometimes simultaneous observations were successfully made from Hawaii and from STS-3 to provide unique information on atmospheric sources and sinks of radiation.

Weinberg, J. L.↗
NASA NTRS1972

Design principles for contamination abatement in scientific satellites.

It is shown that deposition of contamination films on satellite optics can be controlled by the following means: isolating critical optical surfaces from the rest of the spacecraft; avoiding or minimizing the use of nonmetallic material, particularly near or in line of sight of optical surfaces; avoiding materials with high vapor pressures; subjecting materials to vacuum baking prior to use, to drive off the volatile outgassing products; keeping the critical surfaces at temperatures above the ambient; avoiding elevated operational temperatures for nonmetallic materials; paying special attention to optics exposed to intense UV-, X-ray, or particular radiation; avoiding water-vapor sources; and directing RCS plumes away from critical surfaces. Methods of controlling particulate contaminants are also proposed.

Naumann, R. J.↗
NASA NTRS1993

Contamination on LDEF: Sources, distribution, and history

An introduction to contamination effects observed on the Long Duration Exposure Facility (LDEF) is presented. The activities reported are part of Boeing's obligation to the LDEF Materials Special Investigation Group. The contamination films and particles had minimal influence on the thermal performance of the LDEF. Some specific areas did have large changes in optical properties. Films also interfered with recession rate determination by reacting with the oxygen or physically shielding underlying material. Generally, contaminant films lessen the measured recession rate relative to 'clean' surfaces. On orbit generation of particles may be an issue for sensitive optics. Deposition on lenses may lead to artifacts on photographic images or cause sensors to respond inappropriately. Particles in the line of sight of sensors can cause stray light to be scattered into sensors. Particles also represent a hazard for mechanisms in that they can physically block and/or increase friction or wear on moving surfaces. LDEF carried a rather complex mixture of samples and support hardware into orbit. The experiments were assembled under a variety of conditions and time constraints and stored for up to five years before launch. The structure itself was so large that it could not be baked after the interior was painted with chemglaze Z-306 polyurethane based black paint. Any analysis of the effects of molecular and particulate contamination must account for a complex array of sources, wide variation in processes over time, and extreme variation in environment from ground to launch to flight. Surface conditions at certain locations on LDEF were established by outgassing of molecular species from particular materials onto adjacent surfaces, followed by alteration of those species due to exposure to atomic oxygen and/or solar radiation.

Pippin, Gary↗
DOE OSTI2025

Evaluation of a high-throughput method for processing sponge-stick samples to detect viable, non-spore-forming biothreat agents

After a bioterrorism incident, surface sampling is often used to determine the extent of contamination and exposure, guiding decontamination efforts and decisions for re-occupancy of affected sites. The sponge-stick (SS) is a preferred and commonly used device for sample collection to detect both spore-forming and non-spore-forming biothreat agents from non-porous surfaces. Here, in this study, a recently developed high-throughput method (HTM) for processing SS samples to detect viable Bacillus anthracis spores was adapted for detection of non-spore-forming biothreat agents, Yersinia pestis and Francisella tularensis. The scalable HTM was used to process up to 20 SS samples simultaneously, compared to the current stomacher-based method which processes one SS at a time. Comparisons of the HTM and the stomacher-based method were statistically indistinguishable for most experiments (P > 0.05) with HTM recoveries of 37–60 % for Y. pestis inoculated at 102–103 cells/SS and held 48 h at 4 °C to mimic sample transport/storage. The HTM was integrated with Rapid Viability-Polymerase Chain Reaction (RV-PCR) analysis to detect viable Y. pestis in the presence of particulate contamination (Arizona Test Dust, ATD). This approach detected Y. pestis inoculated at 20 cells/SS and ATD did not impact detection (P > 0.05). F. tularensis showed significantly lower recoveries between no-hold time and 48-h hold time (4 °C, P < 0.05) using the HTM, which further testing showed could be due to toxicity of the neutralizing buffer used for SS pre-wetting. With modifications, this method could enhance throughput capacity while maintaining similar recovery efficiencies to current methods for other non-spore-forming bacterial pathogens.

Biological and medical sciences↗
DOE OSTI2025

Development of a high-throughput method for processing sponge-stick samples to detect viable Bacillus anthracis spores

Since the national validation of the sponge-stick based method for detection of Bacillus anthracis spores in environmental samples, there have not been focused efforts to address the low throughput nature of the method, which processes only one sample at one time. Sample processing remains a serious bottleneck for rapidly analyzing large numbers of samples expected from a biological warfare attack. Therefore, we developed a high-throughput method to simultaneously process multiple sponge-stick samples to be better prepared for rapid response and recovery after wide area anthrax incidents. In this method, sponges are placed in 50 mL tubes containing 25 mL extraction buffer and shaken to release spores, after which the suspension is recovered for analysis. Here, we determined that an additional extraction step, conducted in the same tubes with 10 mL buffer, further increased spore recovery from sponge-stick by approximately 10 %. We determined that orbital shaking and multi-tube vortexing were both more effective than reciprocating shaking for recovering spores. We conducted simultaneous processing of up to 12 sponge-stick samples and demonstrated comparable spore recovery efficiencies to the traditional low-throughput stomacher-based method (approximately 60 % recovery at 10 2 -spore level and 75 % recovery at 10 4 -spore level for both methods in three replicate experiments, P > 0.05 for two-tailed t-tests for each experiment and spore level). We also demonstrated that our high-throughput method could be integrated with Rapid Viability-Polymerase Chain Reaction (RV-PCR) analysis and could detect levels as low as 40 spores per sponge even when challenged by a PCR particulate contaminant.

Anthrax↗
NASA NTRS1975

Coronagraph particulate measurements. Skylab flight experiment T025

Major results of the Skylab T025 Coronagraph experiment designed to monitor the particulate contamination about the spacecraft and to study the earth's atmospheric aerosol distribution are presented. A model for comet outbursts based on the properties of amorphous ice and ground based narrow-band and white light photography of comet Kohoutek ten days to perihelion are included. The effect of atmospheric refraction on the analysis of the T025 atmospheric data was also investigated.

Greenberg, J. M.↗
NASA NTRS1976

Introducing controlled matter into a fluid system

Device consisting of capsule holder and glass inner tube has been developed to handle controlled particulate-contamination samples. Premeasured quantity of particles can be injected into closed fluid system without contamination.

Hoffman, C. E.↗
NASA NTRS1976

Automated solvent concentrator

Designed for automated drug identification system (AUDRI), device increases concentration by 100. Sample is first filtered, removing particulate contaminants and reducing water content of sample. Sample is extracted from filtered residue by specific solvent. Concentrator provides input material to analysis subsystem.

Griffith, J. S.↗
NASA NTRS1977

A study of Minnesota land and water resources using remote sensing

The author has identified the following significant results. Both LANDSAT imagery and digital data were studied for usefulness in surveying water conditions of Minnesota lakes. Initial consideration was given to analysis of LANDSAT image densities because of the low technologic and cost requirements. The techniques employed, however, yield inconsistent and unreliable results. A set of criteria are given for using LANDSAT data in identification of three categories of particulate contaminants in Lake Superior. A linear transformation giving the relationship between the residual LANDSAT intensities and concentrations of three contaminants was obtained from correlation of remote sensing data with insitu measurements. LANDSAT imagery was found useful in placing peat bogs and fens in their respective geologic settings. Artificial disturbances and drainageways in peatlands could be recognized and classified.

Shepherd, W. G.↗
NASA NTRS1979

Building penetration analysis

The airborne exposure to carbon fibers experienced within a building may be substantially less than that outside the building. By their very nature, buildings provide a barrier to the free flow of airborne particulate contaminants through the air space they occupy. The objective of this report is an evaluation of the degree to which buildings and other structures will attenuate potential exposures to carbon fibers. Most if not all types of buildings, and all phenomena which may influence the extent to which fibers in outdoor air can penetrate structures are addressed.

Source record↗
NASA NTRS1980

Photovoltaic module soiling studies, May 1978 - October 1980

Comparative electrical and optical performance data from photovoltaic modules and materials subjected to outdoor exposure at field test sites throughout the United States were collected and examined. The results show significant time and site dependence. During periods when natural removal processes do not dominate, the rate of particulate contamination accumulation appears to be largely material-independent. The effectiveness of natural removal processes, especially rain, is strongly material-dependent. Glass and acrylic top cover materials retain fewer particles than silicone rubber does. Side by side outdoor exposure testing for long duration is presently the most effective means of evaluating soiling differences between materials. Changes in spectral transmission as a function of time and location and limited scattering data are presented.

Hoffman, A. R.↗