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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 109 records · Page 6

An experiment on the use of disposable plastics as a reinforcement in concrete beams

Illustrated here is the concept of reinforced concrete structures by the use of computer simulation and an inexpensive hands-on design experiment. The students in our construction management program use disposable plastic as a reinforcement to demonstrate their understanding of reinforced concrete and prestressed concrete beams. The plastics used for such an experiment vary from plastic bottles to steel reinforced auto tires. This experiment will show the extent to which plastic reinforcement increases the strength of a concrete beam. The procedure of using such throw-away plastics in an experiment to explain the interaction between the reinforcement material and concrete, and a comparison of the test results for using different types of waste plastics are discussed. A computer analysis to simulate the structural response is used to compare the test results and to understand the analytical background of reinforced concrete design. This interaction of using computers to analyze structures and to relate the output results with real experimentation is found to be a very useful method for teaching a math-based analytical subject to our non-engineering students.

Chowdhury, Mostafiz R.↗

Development of Advanced Alloys using Fullerenes

Development of advanced alloys using fullerenes is currently underway to produce materials for use in the extravehicular mobility unit (EMU). These materials will be directed toward commercial usages as they are continually developed. Fullerenes (of which the most common is C(sub 60)) are lightweight, nanometer size, hollow molecules of carbon which can be dispersed in conventional alloy systems to enhance strength and reduce weight. In this research, fullerene interaction with aluminum is investigated and a fullerene-reinforced aluminum alloy is being developed for possible use on the EMU. The samples were manufactured using standard commercial approaches including powder metallurgy and casting. Alloys have been processed having 1.3, 4.0 and 8.0 volume fractions of fullerenes. It has been observed that fullerene dispersion is related to the processing approach and that they are stable for the processing conditions used in this research. Emphasis will be given to differential thermal analysis and wavelength dispersive analysis of the processed alloys. These two techniques are particularly useful in determining the condition of the fullerenes during and after processing. Some discussion will be given as to electrical properties of fullerene-reinforced materials. Although the aluminum and other advanced alloys with fullerenes are being developed for NASA and the EMU, the properties of these materials will be of interest for commercial applications where specific Dual-Use will be given.

Sims, J.↗

Rapid Fabrication of Carbide Matrix/Carbon Fiber Composites

Composites of zirconium carbide matrix material reinforced with carbon fibers can be fabricated relatively rapidly in a process that includes a melt infiltration step. Heretofore, these and other ceramic matrix composites have been made in a chemical vapor infiltration (CVI) process that takes months. The finished products of the CVI process are highly porous and cannot withstand temperatures above 3,000 F (approx.1,600 C). In contrast, the melt-infiltration-based process takes only a few days, and the composite products are more nearly fully dense and have withstood temperatures as high as 4,350 F (approx.2,400 C) in a highly oxidizing thrust chamber environment. Moreover, because the melt- infiltration-based process takes much less time, the finished products are expected to cost much less. Fabrication begins with the preparation of a carbon fiber preform that, typically, is of the size and shape of a part to be fabricated. By use of low-temperature ultraviolet-enhanced chemical vapor deposition, the carbon fibers in the preform are coated with one or more interfacial material(s), which could include oxides. The interfacial material helps to protect the fibers against chemical attack during the remainder of the fabrication process and against oxidation during subsequent use; it also enables slippage between the fibers and the matrix material, thereby helping to deflect cracks and distribute loads. Once the fibers have been coated with the interfacial material, the fiber preform is further infiltrated with a controlled amount of additional carbon, which serves as a reactant for the formation of the carbide matrix material. The next step is melt infiltration. The preform is exposed to molten zirconium, which wicks into the preform, drawn by capillary action. The molten metal fills most of the interstices of the preform and reacts with the added carbon to form the zirconium carbide matrix material. The zirconium does not react with the underlying fibers because they are protected by the interfacial material(s). The success of the melt-infiltration step depends on interface material selection and uniform coating of the fibers, infiltration with the correct amount of carbon, and careful control of temperature and rate of heating.

Williams, Brian E.↗

Rheological and Structural Properties of k‐Carrageenan/Xanthan Gum Gummies Architected With a New Natural Additive

ABSTRACT Biohybrids (BHs)based on bentonite and anthocyanins can be produced as alternatives to synthetic colorants. However, no information is available on the interaction of biohybrid with food system. This research studies the rheological properties of gummies containing k‐carrageenan and xanthan gum incorporated with a BH. The incorporation of BH (≤ 2% w/w) increased the flow consistency index and shear thinning effect in melted gummies at 85°C. During cooling from 90°C to 25°C, the presence of BH altered the sol–gel transition temperature typical in carrageenan systems, probably by the formation of carrageenan complexes. At 25°C, all gummies had a solid‐like response with elastic modulus ( G ') higher than viscous modulus ( G "). G ' values increased linearly with BH concentration, and the linear viscoelastic region and breaking strain decreased with BH concentration, indicating that this natural additive acted as a reinforcing material.

Valencia, German Ayala [Department of Chemical and↗

Energy absorption of architectured PrintCast interpenetrating composites in tension

Additively manufactured (AM) metal-metal composites consisting of PrintCasted 316 L austenitic stainless-steel lattice structures infiltrated with A356 casting alloy, have recently been developed for use in high energy absorption systems with potential applications ranging from static load bearing to dynamic blast containment structures. This system has a unique mechanical behavior as the volume fraction of lattice increases showing a transition from localized to de-localized failure and dramatic increase in energy absorption capability. In this work, PrintCast A356/316 L composite tensile specimens were produced with lattice volume fractions ranging from 20 % to 50 % to capture the range of this behavior. Finite element simulations support neutron diffraction measurements of stress state. Results illustrate that in tension, the reinforcement material is in tension while the matrix support material is in compression, information offering significant insight into the transition to de-localized failure. Moreover, the simulation results provide further insight into how interfacial bonding (or lack of bonding) affects the energy absorption capabilities of the PrintCast composites.

36 MATERIALS SCIENCE↗

Boron carbide whiskers produced by vapor deposition

Boron carbide whiskers have an excellent combination of properties for use as a reinforcement material. They are produced by vaporizing boron carbide powder and condensing the vapors on a substrate. Certain catalysts promote the growth rate and size of the whiskers.

Source record↗

Development of a process for producing ribbon shaped filaments

Silicon carbide (SiC) ribbon filaments were produced on a carbon ribbon substrate, about 1500 microns (60 mils) wide and 100 microns (4 mils) thick in lengths up to 2 meters (6 ft), and with tensile strengths up to 142 KN/cm sq (206 Ksi). During the course of the study, ribbon filaments of boron were also produced on the carbon ribbon substrate; the boron ribbon produced was extremely fragile. The tensile strength of the SiC ribbon was limited by large growths or flaws caused by anomalies at the substrate surface; these anomalies were either foreign dirt or substrate imperfections or both. Related work carried out on round 100 micron (4 mils) diameter SiC filaments on a 33 micron (1.3 mil) diameter, very smooth carbon monofilament substrate has shown that tensile strengths as high as 551 KN/cm sq (800 Ksi) are obtainable with the SiC-carbon round substrate combination, and indicates that if the ribbon substrate surface and ribbon deposition process can be improved similar strengths can be realizable. Cost analysis shows that 100 micron x 5-10 micron SiC ribbon can be very low cost reinforcement material.

Debolt, H. E.↗

Development of design data for graphite reinforced epoxy and polyimide composites

Processing techniques and design data were characterized for a graphite/epoxy composite system that is useful from 75 K to 450 K, and a graphite/polyimide composite system that is useful from 75 K to 589 K. The Monsanto 710 polyimide resin was selected as the resin to be characterized and used with the graphite fiber reinforcement. Material was purchased using the prepreg specification for the design data generation for both the HT-S/710 and HM-S/710 graphite/polyimide composite system. Lamina and laminate properties were determined at 75 K, 297 K, and 589 K. The test results obtained on the skin-stringer components proved that graphite/polyimide composites can be reliably designed and analyzed much like graphite/epoxy composites. The design data generated in the program includes the standard static mechanical properties, biaxial strain data, creep, fatigue, aging, and thick laminate data.

Scheck, W. G.↗

Flight service evaluation of PRD-49/epoxy composite panels in wide-bodied commercial transport aircraft

Fairing panels were fabricated to evaluate the fabrication characteristics and flight service performance of PRD-49 (Kevlar-49) a composite reinforcing material and to compare it with the fiberglass which is currently in use. Panel configurations were selected to evaluate the PRD-49 with two resin matrix materials in sandwich and solid laminate construction. Left and right hand versions of these configurations were installed on L-1011's which will accumulate approximately 3000 flight hours per year per aircraft. The direct substitution of PRD-49 for fiberglass produced a twenty-six percent weight reduction on the panel configurations. Examination of these panels revealed that there was no visible difference between the PRD-49 and adjacent fiberglass panels.

Wooley, J. H.↗

Elastic moduli of transversely isotropic graphite fibers and their composites

The paper demonstrates that it is possible to calculate the complete set of elastic mechanical properties for graphite-epoxy fiber-reinforced materials at any fiber-volume fraction by modifying equations previously developed to include transversely isotropic graphite-fiber properties. Experimental verification of the modified equations is demonstrated by using these equations to curve fit elastic-property data obtained ultrasonically over a range of fiber-volume fractions. Material systems under consideration are T300/5208, AS-3501 and Modomor II/LY558 graphite epoxy. Using the modified equations it is possible to extrapolate for fiber properties. From Modomor II/LY558 ultrasonic data, it is shown that five out of seven extrapolated graphite-fiber properties are consistent with the assumption that graphite fibers are transversely isotropic. Elastic properties for T300/5208 and AS-3501 are ultrasonically evaluated by propagating stress waves through six individual specimens cut at various angles from a block of unidirectional material. Particular attention is devoted to specimen dimensions. To demonstrate the need for accurately calculating or experimentally measuring all lamina elastic properties, a brief discussion is included on the effect that variations in lamina elastic properties have on calculating interlaminar stresses.

Kriz, R. D.↗

Residual strength assessment of low velocity impact damage of graphite-epoxy laminates

This report contains the study of Low Velocity Transverse Impact Damage of graphite-epoxy T300/5208 composite laminates. The specimen, 100 mm diameter clamped plates, were impact damaged by a cantilever-type instrumented 1-inch diameter steel ball. Study was limited to impact velocity 6 m/sec. Rectangular strips, 50 mm x 125 mm, were cut from the impact-damage specimens so that the impact damage zone was in the center of the strips. These strips were tested in tension to obtain their residual strength. An energy dissipation model was developed to predict the residual strength from fracture mechanics concepts. Net energy absorbed I(a) was evaluated from coefficient of restitution concepts based on shear dominated theory of fiber-reinforced materials, with the modification that during loading and unloading the shear deformation are respectively elastic-plastic and elastic. Delamination energy I(d) was predicted by assuming that the stiffness of the laminate dropped due to debonding. Fiber-breakage energy, assumed to be equal to the difference of I(a) and I(d), was used to determine the residual strength. Predictions were compared with test results.

Lal, K. M.↗

Orbit on demand - Structural analysis finds vertical launchers weigh less

Structural considerations arising from favored design concepts for the next generation on-demand launch vehicles are explored. The two emerging concepts are a two stage fully reusable vertical take-off vehicle (V-2) and a horizontal take-off, two stage subsonic boost launch vehicle (H-2-Sub). Both designs have an 1100 n. mi. cross-range capability, with the V-2 orbiter having small wings with winglets for hypersonic trim and the H-2-Sub requiring larger, swept wings. The rockets would be cryogenic, while airbreathing initial boosters would be either turbofans, turbojets and/or ramjets. Dynamic loading is lower in the launch of a V-2. The TPS is a critical factor due to thinner leading edges than on the Shuttle and may require heat-pipe cooling. Airframe structures made of metal matrix composites have passed finite element simulations of projected loads and can now undergo proof-of-concept tests, although whisker-reinforced materials may be superior once long-whisker technology is developed.

Taylor, A. H.↗

Pin Inserts for Plug Welds

Leakage through minute cracks eliminated. Electron-beam-welded pins reinforce material around coolant holes during plug welding and subsequent remachining. Pins removed in final machining of 0.188-in diameter hole.

Penninger, Michael↗

Innovative design of composite structures: Use of curvilinear fiber format to improve structural efficiency

To increase the effectiveness and efficiency of fiber-reinforced materials, the use of fibers in a curvilinear rather than the traditional straightline format is explored. The capacity of a laminated square plate with a central circular hole loaded in tension is investigated. The orientation of the fibers is chosen so that the fibers in a particular layer are aligned with the principle stress directions in that layer. Finite elements and an iteration scheme are used to find the fiber orientation. A noninteracting maximum strain criterion is used to predict load capacity. The load capacities of several plates with different curvilinear fibers format are compared with the capacities of more conventional straightline format designs. It is found that the most practical curvilinear design sandwiches a group of fibers in a curvilinear format between a pair of +/-45 degree layers. This design has a 60% greater load capacity than a conventional quasi-isotropic design with the same number of layers. The +/-45 degree layers are necessary to prevent matrix cracking in the curvilinear layers due to stresses perpendicular to the fibers in those layers. Greater efficiencies are achievable with composite structures than now realized.

Hyer, M. W.↗

Potential for on-orbit manufacture of large space structures using the pultrusion process

On-orbit manufacture of lightweight, high-strength, advanced-composite structures using the pultrusion process is proposed. This process is adaptable to a zero-gravity environment by using preimpregnated graphite-fiber reinforcement systems. The reinforcement material is preimpregnated with a high-performance thermoplastic resin at a ground station, is coiled on spools for compact storage, and is transported into Earth orbit. A pultrusion machine is installed in the Shuttle cargo bay from which very long lengths of the desired structure is fabricated on-orbit. Potential structural profiles include rods, angles, channels, hat sections, tubes, honeycomb-cored panels, and T, H, and I beams. A potential pultrudable thermoplastic/graphite composite material is presented as a model for determining the effect on Earth-to-orbit package density of an on-orbit manufacture, the package density is increased by 132 percent, and payload volume requirement is decreased by 56.3 percent. The fabrication method has the potential for on-orbit manufacture of structural members for space platforms, large space antennas, and long tethers.

Wilson, Maywood L.↗

Use of curvilinear fiber format to increase structural efficiency

To increase the effectiveness and efficiency of fiber-reinforced materials, the use of fibers in a curvilinear rather than the traditional straightline format is explored. The capacity of a laminated square plate with a central circular hole loaded in tension is investigated. The orientation of the fibers is chosen so that the fibers in a particular layer are aligned with the principle stress directions in that layer. Finite elements and an iteration scheme are used to find the fiber orientation. A noninteracting maximum strain criterion is used to predict load capacity. The load capacities of several plates with different curvilinear fibers format are compared with the capacities of more conventional straightline format designs. It is found that the most practical curvilinear design sandwiches a group of fibers in a curvilinear format between a pair of +/-45 degree layers. This design has a 60 percent greater load capacity than a conventional quasi-isotropic design with the same number of layers. The +/-45 degree layers are necessary to prevent matrix cracking in the curvilinear layers due to stresses perpendicular to the fibers in those layers. Greater efficiencies are achievable with composite structures than now realized.

Hyer, M. W.↗

Durability of composites

Fiber reinforced materials (composites) are considered very seriously for use in primary loadbearing structures. However, the pace at which they will actually be introduced into the structural designs of the future very much depends on the solution of a critical problem, which is the inability to predict the long term behavior of the material in a given service environment. The research and development of integrity evaluation and lifetime prediction schemes for composite materials is thus a burning issue. The information presented is part of an ongoing program which is directed toward and accelerated determination of the endurance limits of composite materials. Real-time testing is simply not feasible because enough integrity has to be designed into composite structures such that they have a service life which is often as long as twenty or thirty years.

Hiel, Clem C.↗

Pultrusion Process Development for Long Space Boom Model

Long flexible-boom models were required to develop ground-vibration test methods for very-low-frequency space structures with applications to the proposed Space Station. Pultruded quasi-isotropic composite beams were selected as an option over extruded aluminum alloy structures because of the lower cost potential, the higher specific strength, the flexural properties, and the dynamic similarity considerations. The reinforcement material that was used was biaxial (0 deg/90 deg) fiberglass roving held in place with knitted polyester yarn such that equal fiber volume in 0 deg and 90 deg orientations provided nearly equal strength in both longitudinal and transverse directions. An isophthalic polyester resin system was used as the matrix. Continuous lengths up to 270 ft were easily pultruded with biaxial fabric. Tracking problems were encountered with similar unidirectional fabrics. Analyses of processing problems were conducted to determine causes for delamination, scaling, and sloughing. Ultrasonic C-scanning and scanning electron microscope examinations were conducted as well as mechanical testing to failure. Test results indicate that pultrusion processes can be used to produce quasi-isotropic composite structures.

Wilson, Maywood L.↗