Oxide deformation and fiber reinforcement in a tungsten metal oxide composite
Oxide deformation and fiber reinforcement in tungsten-urania and tungsten-zirconia elongated into fibers by hot extrusion
Blankenship, C. P.↗
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Analysis of pultrusion processing for long fiber reinforced thermoplastic composite system
Pultrusion is one of the composite processing technology, commonly recognized as a simple and cost-effective means for the manufacturing of fiber-reinforced, resin matrix composite parts with different regular geometries. Previously, because the majority of the pultruded composite parts were made of thermosetting resin matrix, emphasis of the analysis on the process has been on the conservation of energy from various sources, such as heat conduction and the curing kinetics of the resin system. Analysis on the flow aspect of the process was almost absent in the literature for thermosetting process. With the increasing uses of thermoplastic materials, it is desirable to obtain the detailed velocity and pressure profiles inside the pultrusion die. Using a modified Darcy's law for flow through porous media, closed form analytical solutions for the velocity and pressure distributions inside the pultrusion die are obtained for the first time. This enables us to estimate the magnitude of viscous dissipation and it's effects on the pultruded parts. Pulling forces refined in the pultrusion processing are also analyzed. The analytical model derived in this study can be used to advance our knowledge and control of the pultrusion process for fiber reinforced thermoplastic composite parts.
Tso, W.↗
Toughened Matrix SiC Fiber Reinforced Composites
First matrix cracking stress is a critical parameter for application of Sic fiber reinforced composites in highly stressed, environmentally demanding applications such as turbine blades. High matrix fracture toughness is a key property that contributes to high composite fracture stress. Silicon nitride offers reduced matrix elastic modulus, lower coefficient of thermal expansion, and potentially high fracture toughness compared to Sic matrices. All of these factors can be used to advantage to increase matrix fracture stress. As a first model system we are pursuing toughened silicon nitride matrix composites reinforced with SCS-9 fibers. Fabrication is by tape casting the matrix plies and tape lay-up with fiber plies followed by hot pressing at 1800 C. Progress toward this end will be reported.
Levine, Stanley R.↗
Design of Fiber Reinforced Foam Sandwich Panels for Large Ares V Structural Applications
The preliminary design of three major structural components within NASA's Ares V heavy lift vehicle using a novel fiber reinforced foam composite sandwich panel concept is presented. The Ares V payload shroud, interstage, and core intertank are designed for minimum mass using this panel concept, which consists of integral composite webs separated by structural foam between two composite facesheets. The HyperSizer structural sizing software, in conjunction with NASTRAN finite element analyses, is used. However, since HyperSizer does not currently include a panel concept for fiber reinforced foam, the sizing was performed using two separate approaches. In the first, the panel core is treated as an effective (homogenized) material, whose properties are provided by the vendor. In the second approach, the panel is treated as a blade stiffened sandwich panel, with the mass of the foam added after completion of the panel sizing. Details of the sizing for each of the three Ares V components are given, and it is demonstrated that the two panel sizing approaches are in reasonable agreement for thinner panel designs, but as the panel thickness increases, the blade stiffened sandwich panel approach yields heavier panel designs. This is due to the effects of local buckling, which are not considered in the effective core property approach.
Bednarcyk, Brett A.↗
Effects of High-Temperature Annealing in Air on Hi-Nicalon Fiber-Reinforced Celsian Matrix Composites
BN/SiC-coated Hi-Nicalon fiber-reinforced celsian matrix composites (CMC) were annealed for 100 h in air at various temperatures to 1200 C, followed by flexural strength measurements at room temperature. Values of yield stress and strain, ultimate strength, and composite modulus remain almost unchanged for samples annealed up to 1100 C. A thin porous layer formed on the surface of the 1100 C annealed sample and its density decreased from 3.09 to 2.90 g/cu cm. The specimen annealed at 1200 C gained 0.43 wt%, was severely deformed, and was covered with a porous layer of thick shiny glaze which could be easily peeled off. Some gas bubbles were also present on the surface. This surface layer consisted of elongated crystals of monoclinic celsian and some amorphous phase(s). The fibers in this surface ply of the CMC had broken into small pieces. The fiber-matrix interface strength was characterized through fiber push-in technique. Values of debond stress, alpha(sub d), and frictional sliding stress, tau(sub f), for the as-fabricated CMC were 0.31+/-0.14 GPa and 10.4+/-3.1 MPa, respectively. These values compared with 0.53+/-0.47 GPa and 8.33+/-1.72 MPa for the fibers in the interior of the 1200 C annealed sample, indicating hardly any change in fiber-matrix interface strength. The effects of thermal aging on microstructure were investigated using scanning electron microscopy. Only the surface ply of the 1200 C annealed specimens had degraded from oxidation whereas the bulk interior part of the CMC was unaffected. A mechanism is proposed explaining the various steps involved during the degradation of the CMC on annealing in air at 1200 C.
Bansal, Narottam P.↗
Tungsten fiber-reinforced copper composites form high strength electrical conductors
Tungsten fiber-reinforced copper composites have tensile strength, yield strength, and modulus of elasticity proportional to fiber content. The composites form high strength electrical conductors.
Mc Danels, D. L.↗
Analysis of stress-strain behavior of tungsten- fiber-reinforced copper composites.
Stress-strain behavior of tungsten fiber- reinforced copper composites, discussing room- temperature tensile and dynamic-modulus tests
TUNGSTEN ALLOY↗
Fiber reinforced composites for space systems
High strength, low weight, fiber reinforced composites for cryogenic propellant tanks
Kreft, H.↗
Tungsten fiber reinforced superalloy composite high temperature component design considerations
Tungsten fiber reinforced superalloy composites (TFRS) are intended for use in high temperature turbine components. Current turbine component design methodology is based on applying the experience, sometimes semiempirical, gained from over 30 years of superalloy component design. Current composite component design capability is generally limited to the methodology for low temperature resin matrix composites. Often the tendency is to treat TFRS as just another superalloy or low temperature composite. However, TFRS behavior is significantly different than that of superalloys, and the high environment adds consideration not common in low temperature composite component design. The methodology used for preliminary design of TFRS components are described. Considerations unique to TFRS are emphasized.
Winsa, E. A.↗
Model of brittle matrix composite toughening based on discrete fiber reinforcement
An analytical approach for the analysis of the effectiveness of fiber reinforcement in brittle matrix composites is presented. The analytical method allows consideration of discrete fiber distribution and examination of the development of crack growth parameters on microscale. The problem associated with the bridging zone development is addressed here; therefore, the bridging zone is considered to be smaller than the main preexisting crack, and the small scale approach is used. The mechanics of the reinforcement is accurately accounted for in the process zone of a growing crack. Closed form solutions characterizing the initial failure process are presented for linear and nonlinear force - fiber pullout displacement relationships. The implicit exact solution for the extended bridging zone is presented as well.
Rubinstein, Asher A.↗
Application of fiber-reinforced bismaleimide materials to aircraft nacelle structures
Existing aircraft engine nacelle structures employ advanced composite materials to reduce weight and thereby increase overall performance. Use of advanced composite materials on existing aircraft nacelle structures includes fiber-reinforced epoxy structures and has typically been limited to regions furthest away from the hot engine core. Portions of the nacelle structure that are closer to the engine require materials with a higher temperature capability. In these portions, existing nacelle structures employ aluminum sandwich construction and skin/stringer construction. The aluminum structure is composed of many detail parts and assemblies and is usually protected by some form of ablative, insulator, or metallic thermal shield. A one-piece composite inner cowl for a new-generation engine nacelle structure has been designed using fiber-reinforced bismaleimide (BMI) materials and honeycomb core in a sandwich construction. The new composite design has many advantages over the existing aluminum structure. Multiple details were integrated into the one-piece composite design, thereby significantly reducing the number of detail parts and fasteners. The use of lightweight materials and the reduction of the number of joints result in a significant weight reduction over the aluminum design; manufacturing labor and the overall number of tools required have also been reduced. Several significant technical issues were addressed in the development of a BMI composite design. Technical evaluation of the available BMI systems led to the selection of a toughened BMI material which was resistant to microcracking under thermal cyclic loading and enhanced the damage tolerance of the structure. Technical evaluation of the degradation of BMI materials in contact with aluminum and other metals validated methods for isolation of the various materials. Graphite-reinforced BMI in contact with aluminum and some steels was found to degrade in salt spray testing. Isolation techniques such as those used for graphite-reinforced epoxy structures were shown to provide adequate protection. The springback and producibility of large BMI structures were evaluated by manufacturing prototype hardware which had the full-scale cross section of the one-piece composite structure.
Peros, Vasilios↗
Oxidation of SiC Fiber-Reinforced SiC Matrix Composites with a BN Interphase
SiC-fiber reinforced SiC matrix composites with a BN interphase were oxidized in reduced oxygen partial pressures of oxygen to simulate the environment for hypersonic vehicle leading edge applications. The constituent fibers as well as composite coupons were oxidized in oxygen partial pressures ranging from 1000 ppm O2 to 5% O2 balance argon. Exposure temperatures ranged from 816 C to 1353 C (1500 F to 2450 F). The oxidation kinetics of the coated fibers were monitored by thermogravimetric analysis (TGA). An initial rapid transient weight gain was observed followed by parabolic kinetics. Possible mechanisms for the transient oxidation are discussed. One edge of the composite coupon seal coat was ground off to simulate damage to the composite which allowed oxygen ingress to the interior of the composite. Oxidation kinetics of the coupons were characterized by scanning electron microscopy since the weight changes were minimal. It was found that sealing of the coupon edge by silica formation occurred. Differences in the amount and morphology of the sealing silica as a function of time, temperature and oxygen partial pressure are discussed. Implications for use of these materials for hypersonic vehicle leading edge materials are summarized.
Opila, Elizabeth↗
Mechanics of interfaces in fiber reinforced SiC/RBSN ceramic matrix composites
The mechanical behavior of continuous fiber reinforced SiC/RBSN composites with strong and weak interface characteristics is evaluated. Both catastrophic and noncatastrophic failures are observed in tensile specimens. Effects of fiber/matrix interface debonding (splitting) parallel to the fibers are discussed. Micromechanical models incorporating residual stresses to calculate the critical matrix cracking strength, ultimate strength and work of pull-out are reviewed and used to predict composite response. Experimental results are compared to analytical predictions.
Chulya, Abhisak↗
Carbon Fiber Reinforced Carbon Composites Rotary Valves for Internal Combustion Engines
Carbon fiber reinforced carbon composite rotary, sleeve, and disc valves for internal combustion engines and the like are disclosed. The valves are formed from knitted or braided or warp-locked carbon fiber shapes. Also disclosed are valves fabricated from woven carbon fibers and from molded carbon matrix material. The valves of the present invention with their very low coefficient of thermal expansion and excellent thermal and self-lubrication properties, do not present the sealing and lubrication problems that have prevented rotary, sleeve, and disc valves from operating efficiently and reliably in the past. Also disclosed are a sealing tang to further improve sealing capabilities and anti-oxidation treatments.
Northam, G. Burton↗
Problems encountered with conventional fiber-reinforced composites
Preparational, computational, and operational problems associated with fiber-reinforced composites (FRC) are reviewed. Initial preparation of FRCs is shown to involve consideration of the type of prepreg, the setting time, cure conditions and cycles, and cure temperatures. The effects of the choice of bonding agents, the fiber transfer length, and individual fiber responses to bonding agents are noted to have an impact on fiber strength, moisture uptake, and fatigue resistance. The deformation prior to failure and the failure region are modeled through models of mini-, micro- and macro mechanics formulations employing a stiffness matrix, failure criterion, or fracture mechanics. The detection, evaluation, and repair of defects comprises the operational domain, and it is stressed that no good repair techniques exist for FRCs.
Landel, R. F.↗
The interface in tungsten fiber reinforced niobium metal-matrix composites
The creep resistance of tungsten fiber reinforced niobium metal-matrix composites was evaluated. The interface region between the fiber and matrix was characterized by microhardness and electron probe microanalysis measurements which indicated that its properties were between those of fiber and matrix. However, the measured properties of the composite exceeded those calculated by the rule of mixtures even when the interface zone was assumed to retain all the strength of the fiber. The composite structure appeared to enhance the strengths of both the fibers and the matrix above what they exhibited in stand-alone tests. The effect of fiber orientation and matrix alloy composition on the fiber/matrix interface were also evaluated. Small alloying additions of zirconium and tungsten to the niobium matrix affected the creep resistance of the composites only slightly. A decrease in the creep resistance of the composite with increasing zirconium content in the matrix was ascribed to an increase in the diffusion rate of the fiber/matrix interdiffusion reaction, and a slight increase in the creep resistance of the composite was observed with an addition of 9 w percent tungsten to the matrix. In addition, Kirkendall void formation was observed at the fiber/matrix interface; the void distribution differed depending on the fiber orientation relative to the stress axis.
Grobstein, Toni L.↗
The assessment of metal fiber reinforced polymeric composites
Because of their low cost, excellent electrical conductivity, high specific strength (strength/density), and high specific modulus (modulus/density) short metal fiber reinforced composites have enjoyed a widespread use in many critical applications such as automotive industry, aircraft manufacturing, national defense, and space technology. However, little data has been found in the study of short metal fibrous composites. Optimum fiber concentration in a resin matrix and fiber aspect ratio (length-to-diameter ratio) are often not available to a user. Stress concentration at short fiber ends is the other concern when the composite is applied to a load-bearing application. Fracture in such composites where the damage will be initiated or accumulated is usually difficult to be determined. An experimental investigation is therefore carefully designed and undertaken to systematically evaluate the mechanical properties as well as electrical properties. Inconel 601 (nickel based) metal fiber with a diameter of eight microns is used to reinforce commercially available thermoset polyester resin. Mechanical testing such as tensile, impact, and flexure tests along with electrical conductivity measurements is conducted to study the feasibility of using such composites. The advantages and limitations of applying chopped metal fiber reinforced polymeric composites are also discussed.
Chung, Wenchiang R.↗
The effect of Co alloying content on the kinetics of reaction zone growth in tungsten fiber reinforced superalloy composites
A Co-free modified superalloy similar in composition to Waspaloy is investigated in an effort to understand the effect of Co on reaction zone growth kinetics and verify the chemistry dependence of reaction zone growth in the matrix of tungsten fiber reinforced superalloy composites. The values of the parabolic rate constant, characterizing the kinetics of reaction zone growth, for the Waspaloy matrix and the C-free alloy as well as five other alloys from a previous study confirm the dependence of reaction zone growth kinetics on cobalt content of the matrix. The Co-free alloy composite exhibits the slowest reaction zone growth among all tungsten fiber reinforced composites studied to date.
Rodriguez, A.↗