Preliminary examination of lunar samples
Geochemical and minerological analyses of Apollo 12 soil and rock samples
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Growth of the lower continental crust
One of the largest uncertainties in crustal composition and growth models is the nature of the lower continental crust. Specifically, by what processes is it formed and modified, and when is it formed, particularly in reference to the upper crust? The main reason for this lack of information is the scarcity of lower crustal rock samples. These are restricted to two types: rocks which outcrop in granulite facies terrains and granulite facies xenoliths which are transported to the earth's surface by young volcanics. The important conclusions arising from the xenolith studies are: the majority of mafic lower crustal xenoliths formed through cumulate process, resitic xenoliths are rare; and formation and metamorphism of the deep crust is intimately linked to igneous activity and/or orogeny which are manifest in one form or another at the earth's surface. Therefore, estimates of crustal growth based on surface exposures is representative, although the proportion of remobilized pre-existing crust may be significantly greater at the surface than in the deep crust.
Rudnick, Roberta L.↗
Sampling Mars: Analytical requirements and work to do in advance
Sending a mission to Mars to collect samples and return them to the Earth for analysis is without doubt one of the most exciting and important tasks for planetary science in the near future. Many scientifically important questions are associated with the knowledge of the composition and structure of Martian samples. Amongst the most exciting questions is the clarification of the SNC problem- to prove or disprove a possible Martian origin of these meteorites. Since SNC meteorites have been used to infer the chemistry of the planet Mars, and its evolution (including the accretion history), it would be important to know if the whole story is true. But before addressing possible scientific results, we have to deal with the analytical requirements, and with possible pre-return work. It is unlikely to expect that a possible Mars sample return mission will bring back anything close to the amount returned by the Apollo missions. It will be more like the amount returned by the Luna missions, or at least in that order of magnitude. This requires very careful sample selection, and very precise analytical techniques. These techniques should be able to use minimal sample sizes and on the other hand optimize the scientific output. The possibility to work with extremely small samples should not obstruct another problem: possible sampling errors. As we know from terrestrial geochemical studies, sampling procedures are quite complicated and elaborate to ensure avoiding sampling errors. The significance of analyzing a milligram or submilligram sized sample and putting that in relationship with the genesis of whole planetary crusts has to be viewed with care. This leaves a dilemma on one hand, to minimize the sample size as far as possible in order to have the possibility of returning as many different samples as possible, and on the other hand to take a sample large enough to be representative. Whole rock samples are very useful, but should not exceed the 20 to 50 g range, except in cases of extreme inhomogeneity, because for larger samples the information tends to become redundant. Soil samples should be in the 2 to 10 g range, permitting the splitting of the returned samples for studies in different laboratories with variety of techniques.
Koeberl, Christian↗
Evidence for a Meteoritic Component in Impact Melt Rock from the Chicxulub Structure
The Chicxulub structure in Yucatan, Mexico, has recently been recognized as a greater then 200-km-diameter multi-ring impact crater of K-T boundary age. Crystalline impact melt rocks and breccias from within the crater, which have compositions similar to those of normal continental crustal rocks and which show shock metamorphic effects, have been studied for trace element and Re-Os isotope compositions. Re-Os isotope systematics allow the sensitive and selective determination of an extraterrestrial component in impact-derived rocks. A melt rock sample shows elevated iridium concentrations, an osmium concentration of 25 ppb, and a low Os-187/Os-188 ratio of 0.113, which are incompatible with derivation from the continental crust. Even though the Os-187/Os-188 ratio is slightly lower than the range so far measured in meteorites, a mantle origin seems unlikely for mass balance reasons and because the cratering event is unlikely to have excavated mantle material. The data support the hypothesis of a heterogeneously distributed meteoritic component in the Chicxulub melt rock. A sample of impact glass from the Haitian K-T boundary at Beloc yielded about 0.1 ppb osmium and an Os-187/0s-188 ratio of 0.251, indicating the presence of a small meteoritic component in the impact ejecta as well.
Koeberl, Christian↗
Analysis and simulation of the Ultrasonic/Sonic Driller/Corer (USDC)
The USDC was developed to address the challenges to the NASA objective of planetary in-situ rock sampling analysis. A computer program was developed to simulate the operation of the USDC and successfully predicted the characteristic behavior of the new device. This paper covers the theory, the analytical models and the algorithms that were developed and predicted the results.
piezoelectric↗
Search for magnetic monopoles in the lunar samples of Apollo 11
Magnetic monopoles electromagnetic search in Apollo 11 rock samples
Alvarez, L. W.↗
Isotopic composition of thorium and uranium in Apollo 12 samples
Isotopic composition of U and Th in Apollo 12 lunar rock samples from mass and alpha spectrometry
Rosholt, J. N.↗
High Temperature Piezoelectric Drill
The current NASA Decadal mission planning effort has identified Venus as a significant scientific target for a surface in-situ sampling/analyzing mission. The Venus environment represents several extremes including high temperature (460 deg C), high pressure (~9 MPa), and potentially corrosive (condensed sulfuric acid droplets that adhere to surfaces during entry) environments. This technology challenge requires new rock sampling tools for these extreme conditions. Piezoelectric materials can potentially operate over a wide temperature range. Single crystals, like LiNbO3, have a Curie temperature that is higher than 1000 deg C and the piezoelectric ceramics Bismuth Titanate higher than 600 deg C. A study of the feasibility of producing piezoelectric drills that can operate in the temperature range up to 500 deg C was conducted. The study includes the high temperature properties investigations of engineering materials and piezoelectric ceramics with different formulas and doping. The drilling performances of a prototype Ultrasonic/Sonic Drill/Corer (USDC) using high temperate piezoelectric ceramics and single crystal were tested at temperature up to 500 deg C. The detailed results of our study and a discussion of the future work on performance improvements are presented in this paper.
rock sampling↗
Ultrasonic/Sonic Drill for High Temperature Application
Venus is one of the many significant scientific targets for NASA. New rock sampling tools with the ability to be operated at high temperatures of the order of 460 deg C are required for surface in-situ sampling/analysis missions. Piezoelectric materials such as LiNbO? crystals and Bismuth Titanate are potentially operational at the temperature range found on the surface of Venus. A study of the feasibility of producing piezoelectric drills for a temperature up to 500 deg C was conducted. The study includes investigation of the high temperature properties of piezoelectric crystals and ceramics with different formulas and doping. Several prototypes of Ultrasonic/Sonic Drill/Corers (USDC) driven by transducers using the high temperate piezoelectric ceramics and single LiNbO? crystal were fabricated. The transducers were analyzed by scanning the impedance at room temperature and 500 deg C under both low and high voltages. The drilling performances were tested at temperature up to 500 deg C. Preliminary results were previously reported [Bao et al, 2009]. In this paper, the progress is presented and the future works for performance improvements are discussed.
Piezoelectric Drill↗
Development of the Potassium-Argon Laser Experiment (KArLE) Instrument for In Situ Geochronology
Absolute dating of planetary samples is an essential tool to establish the chronology of geological events, including crystallization history, magmatic evolution, and alteration. Traditionally, geochronology has only been accomplishable on samples from dedicated sample return missions or meteorites. The capability for in situ geochronology is highly desired, because it will allow one-way planetary missions to perform dating of large numbers of samples. The success of an in situ geochronology package will not only yield data on absolute ages, but can also complement sample return missions by identifying the most interesting rocks to cache and/or return to Earth. In situ dating instruments have been proposed, but none have yet reached TRL 6 because the required high-resolution isotopic measurements are very challenging. Our team is now addressing this challenge by developing the Potassium (K) - Argon Laser Experiment (KArLE) under the NASA Planetary Instrument Definition and Development Program (PIDDP), building on previous work to develop a K-Ar in situ instrument [1]. KArLE uses a combination of several flight-proven components that enable accurate K-Ar isochron dating of planetary rocks. KArLE will ablate a rock sample, determine the K in the plasma state using laser-induced breakdown spectroscopy (LIBS), measure the liberated Ar using quadrupole mass spectrometry (QMS), and relate the two by the volume of the ablated pit using an optical method such as a vertical scanning interferometer (VSI). Our preliminary work indicates that the KArLE instrument will be capable of determining the age of several kinds of planetary samples to +/-100 Myr, sufficient to address a wide range of geochronology problems in planetary science.
Cohen, Barbara A.↗
The Potassium-Argon Laser Experiment (KARLE): In Situ Geochronology for Planetary Robotic Missions
Isotopic dating is an essential tool to establish an absolute chronology for geological events, including crystallization history, magmatic evolution, and alteration events. The capability for in situ geochronology will open up the ability for geochronology to be accomplished as part of lander or rover complement, on multiple samples rather than just those returned. An in situ geochronology package can also complement sample return missions by identifying the most interesting rocks to cache or return to Earth. The K-Ar Laser Experiment (KArLE) brings together a novel combination of several flight-proven components to provide precise measurements of potassium (K) and argon (Ar) that will enable accurate isochron dating of planetary rocks. KArLE will ablate a rock sample, measure the K in the plasma state using laser-induced breakdown spectroscopy (LIBS), measure the liberated Ar using mass spectrometry (MS), and relate the two by measuring the volume of the ablated pit by optical imaging. Our work indicates that the KArLE instrument is capable of determining the age of planetary samples with sufficient accuracy to address a wide range of geochronology problems in planetary science. Additional benefits derive from the fact that each KArLE component achieves analyses useful for most planetary surface missions.
Cohen, B. A.↗
Compositions and mineralogy of lithic fragments in 1-2 mm soil samples 14002,7 and 14258,33.
The compositional data obtained are combined with existing data from larger rock samples and compared with bulk analyses of soils to determine compositional ranges and dominant igneous rock types present in the regolith and breccias. Criteria are presented for the recognition of three types of igneous fragments in a limited sample of Apollo 14 material. Explanations for the differences between glass and rock compositions are discussed.
Steele, I. M.↗
Moessbauer instrumental analysis of Apollo 12 lunar rock and soil samples
Mossbauer instrumental analysis of Apollo 12 rock and soil samples, measuring nuclear gamma resonance of iron 57
Herzenberg, C. L.↗
Mineralogy and petrology of Apollo 11 and Apollo 12 samples Final report
Investigating mineral composition of Apollo 11 and 12 lunar rock samples
Mc Callum, I. S.↗
Paleointensity determinations at elevated temperatures - Sample preparation technique
A technique has been developed for the encapsulation of rock samples in order to prevent the chemical alterations which commonly accompany paleointensity measurements at elevated temperatures. The technique involves vacuum pumping at about 100 C of the sample as placed in a silica tube. The tube containing the sample and a Ti 'getter' are sealed under vacuum. Measurements can be made at 200 and 300 C. Immediately after this, the sample is sealed-off from the getter. The sample is now ready for measurements at higher temperatures.
Taylor, L. A.↗
New K-feldspar Pb isotope results for Mesozoic arc crust in the Pacific Northwest, U.S.A. and Canada: comparison with the Mojave-Salinia province of southern California and Implications for Baja-BC
Measurements of lead isotopic compositions in detrital K-feldspar have been increasingly used as a tool to assess sediment provenance. We compiled a database of previously published Pb isotope data from 700 bedrock K-feldspar samples and 1,423 age-corrected bedrock whole rock samples from western North American igneous and metamorphic bodies. Additionally, we report 66 new K-feldspar Pb isotope data for plutons throughout the Pacific Northwest region of the United States and British Columbia. Results show that the Pb isotope values of plutonic K-feldspar depend on the isotopically juvenile or evolved nature of underlying crust. Samples obtained from the mid Cretaceous – mid Eocene Coast Plutonic Complex, North Cascades, and Intermontane superterrane that occur west of the initial 87 Sr/ 86 Sr (Sri) = 0.706 isopleth exhibit a highly restricted 207 Pb/ 206 Pb and 208 Pb/ 206 Pb values centred upon 0.83 and 2.03, respectively. Conversely, rocks overlying older continental crust further east such as the Middle Jurassic – Late Cretaceous Omineca crystalline belt, Idaho batholith, and Boulder Batholith exhibit far greater variation of Pb isotope values that parallel the 100 Ma isochron calculated from a two-stage Pb evolution model. We demonstrate that Pb isotopic results from the Idaho and Boulder Batholith region can be used to define distinctive subregions for Pb isotopic provenance analysis, and compare these signatures to the Mojave-Salinian batholith of southern California and western Arizona, as these two areas have previously been proposed as source regions for extraregional sediment that was deposited within the Nanaimo Basin during the Campanian – Maastrichtian. Future Pb isotopic analysis of detrital K-feldspar from the Nanaimo Basin of southwestern British Columbia may effectively distinguish between potential extraregional sources separated by thousands of kilometres.
Coast Plutonic Complex↗
Cause of secondary magnetization in lunar samples, part C
The unstable component of the magnetization found in lunar samples was investigated by returning a demagnetized tracer igneous rock sample from Apollo 12 to the moon on Apollo 16. After the return of the sample, the soft component was similar to the original soft component of the first trip. It is concluded that the soft component is an artifact of the trip.
Pearce, G. W.↗
Nuclear magnetic resonance properties of lunar samples.
Nuclear magnetic resonance spectra of Na-23, Al-27, and P-31 in fines samples 10084,60 and 14163,168 and in crystalline rock samples 12021,55 and 14321,166, have been recorded over a range of frequencies up to 20 MHz. A shift in the field at which maximum absorption occurs for all of the spectra relative to the field at which maximum absorption occurs for terrestrial analogues is attributed to a sample-dependent magnetic field at the Na, Al, and P sites opposing the laboratory field. The magnitude of these fields internal to the samples is sample dependent and varies from 5 to 10 G. These fields do not correlate with the iron content of the samples. However, the presence of single-domain particles of iron distributed throughout the plagioclase fraction that contains the principal fraction of Na and Al is inferred from electron magnetic resonance spectra shapes.
Kline, D.↗