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NASA NTRSDate not supplied

Phosphate Textural Diversity in CI Chondrites and C-Type Asteroids

Introduction: Apatite, Ca 5 (PO 4 ) 3 (CL/F/OH-), is a ubiquitous phosphate found throughout the solar system, including the most primitive solids, CI-chondrites [1,2] and related samples of carbonaceous asteroids Ryugu [3] and Bennu [4], returned by JAXA’s Hayabusa2 and NASA’s OSIRIS-REx missions, respectively. Apatite in these primitive solids is found as individual grains or mineral clusters and has been inferred to form from the hydrothermal sequence during cooling of their respective parent body or bodies. To better understand the formation history and reworking of these early phosphates we have undertaken a highly coordinated study of phosphate microstructures, geochemistry and U/Pb geochronology from a suite of CI meteorites and carbonaceous asteroid samples. These data have identified novel phosphate microstructures and complex relationships across a suite of apatite grains from the early solar system, indicating multiple episodes of growth and modification on the CI parent body(ies). Methods: Samples of CI chondrites, Alais, Ivuna, Orgueil, Oued Chebeika 002, Yamato (Y) 82162, Y980115, Y980134, and two chips of Hayabusa2 Ryugu particles (A0262 and C0263) have been acquired for analysis. The bulk texture of the samples were first scanned by X-ray Computed Tomography (XCT) using the Nikon XT H 320 within the XFACT facility at NASA JSC or the Xradia 620 Versa at the UTCT facility. Based on the identification of petrofabrics or features of interest from the XCT data, samples were chipped, oriented, potted in epoxy and thick sections were prepared. After anhydrously polishing the samples with silicon carbide and dry diamond powder down to 1 µm, the samples were ion polished using a Hitachi ArBlade. Energy dispersive Xray spectrometry (EDS) maps were collected to ID phosphates of interest using a JEOL 7900F SEM. The internal microstructures of identified phosphates were then mapped by electron backscatter diffraction (EBSD) using the JEOL 7900F. Based on the EDS and EBSD data, domains of interest were targeted for quantitative chemical analyses using a JEOL 8530 EPMA. Subsequently, in situ U-Pb and 207 Pb/ 206 Pb ages will be collected using a Cameca ims1290 secondary ion mass spectrometer at UCLA across a range of microstructures. Results: Apatite grains are ubiquitous throughout the CI chondrites and carbonaceous asteroid materials, found as individual grains, disseminated clusters or grain aggregates. Apatite grains are associated with serpentine, magnet-ite, and/or carbonate. Of particular interest, we have identified individual and aggregate polycrystalline grains ex-hibiting an internal ‘honeycomb’ texture (Fig. 1). Some of these grains appear overprinted by subsequent alteration while others remain unaltered. Apatite halogen sites are dominated by the missing component, assumed to be OH, and F, comparable to published values from Bennu, Ryugu and CM-chondrites [3-5]. However, the Yamato CI-like meteorites show a broader range of Cl values, and one grain from Alais is dominated by CL. Summary: Apatite growth features indicate a protracted and complex growth history, consistent with precipitation from an evolving fluid system. The ‘honeycomb’ texture identified in some CI meteorites is, to the best of our knowledge, the first report of such a microstructure in meteoritic phosphate. The microtextures and zoning will guide subsequent age analyses, to better constrain the formation and reworking of phosphate in CI(-like) materials. Acknowledgments: We thank the National Institute of Polar Research, Japan for samples of Y82162, 980115 and 980134 meteorites, ASU’s Buseck Center for Meteorite Studies for samples of Ivuna and Alais meteorites, and JAXA curation for chips of Ryugu material. This work was funded by NASA ROSES LARS grant 24-LARS24-0014. References: [1] Morlok et al., 2016, GCA 70:5371-5394. [2] Alfin g et al., 2019, Geochemistry 79:125532. [3] Nakamura et al. (2022) Science 379:1-15. [4] Seifert et al. (2026) MAPS 61:504-521. [5] Piralla et al. (2021) MAPS 56:809-828.

CI chondrites↗
NASA NTRS2018

The Hayabusa2 Sample Return Mission and Its Small Carry-On Impactor Experiment

On December 3, 2014 the Hayabusa2 Spacecraft was launched by JAXA to investigate and return samples from carbonaceous Asteroid (162173) Ryugu. The spacecraft's payload contains several remote sensing instruments that are designed to characterize the asteroid's surface and to help identify scientifically interesting locations from which samples can be obtained safely. The data collected by these instruments will also help place any obtained samples in context with respect to the global characteristics of Ryugu. In addition to the suite of remote sensing instruments and the sampling device, Hayabusa2 also includes a small carry-on impactor (SCI) payload experiment, which is designed to impact the surface of the asteroid and excavate fresh material for subsequent collection. The SCI consists of a 30 cm diameter 2 kg copper disk that is accelerated by an explosive charge into the surface of Ryugu at approximately 2 km/s. The resultant crater formed during this experiment is estimated to be approximately between 2 - 10 meters in diameter with an ejecta blanket extending to 10 - 100 meters on the asteroid. Hayabusa2 will not be able to observe the impact experiment directly due to considerations of spacecraft safety since there is some risk of collisions with debris from the explosion and ejecta from the crater. However, prior to moving safely away, the spacecraft will deploy a small imaging system called Deployable Camera 3 (DCAM3). DCAM3 will detach from Hayabusa2 just before the detonation of the SCI and will image the moment of impact, crater formation, and ejecta propagation. These data will be transmitted to Hayabusa2 and will help constrain the near-surface properties of Ryugu and also impact scaling laws for small bodies in low gravity environments. These data could also be useful for gaining insights into determining asteroid physical properties from higher velocity impact events (e.g., DART and HERA data of Didymos).

Abell, Paul A.↗
NASA NTRS2020

Thermal Decomposition of the Murchison CM2 Carbonaceous Chondrite: Implications of Space Weathering Processes for Sample Return Missions

Primitive carbonaceous asteroids are the target bodies for the JAXA Hayabusa2 mission to Ryugu and the NASA OSIRIS-REx mission to Bennu. Both asteroids share spectral characteristics of CI/CM type carbonaceous chondrites. Ryugu, in particular, appears to have undergone thermal processing that has modified its spectral properties. The nature and extent of space weathering processes on the surfaces of Bennu and Ryugu are under active investigation using remote sensing data from the missions [4] and through laboratory studies on analog materials. The analog studies are needed in order to understand the mineralogical and chemical changes that occur in space weathered samples that give rise to the observed optical effects measured by remote-sensing and to prepare for the analysis of returned samples. The space weathering effects of micrometeorite impact and solar wind irradiation on primitive carbonaceous chondrites have been simulated by analog studies on the Murchison CM2 chondrite. We performed a coordinated mineralogical, chemical and spectroscopic study to examine in detail the effects of thermal metamorphism on Murchison samples as an analog to processes that may have occurred on Ryugu. The bulk measurements including X-ray diffraction (XRD), Mössbauer spectroscopy, UV-VIS-NIR spectroscopy, thermogravimetric analysis, and evolved gas analysis are reported in a companion paper. Here we report on our preliminary nanoscale mineralogical and chemical analyses of pre- and post-heated Murchison samples using multiple electron beam techniques to understand how the mineralogical, chemical, and physical characteristics of carbonaceous chondrites change with increasing thermal effects.

Lee, S.↗
NASA NTRS2024

Investigating Bennu’s Volatile Accretion History Through Step-Heating N-Ne-Ar Analyses of Single Aggregate Particles

NASA’s OSIRIS-REx spacecraft delivered a sample from the carbonaceous asteroid (101955) Bennu to Earth on September 24, 2023. Since Bennu presumably accreted in the outer protoplanetary disk, beyond Jupiter’s orbit, the collected material is expected to be rich in highly volatile elements such as H, C, N, and noble gases—similar to Ivuna-type (CI) carbonaceous chondrites and material from asteroid (162173) Ryugu returned by JAXA’s Hayabusa2 spacecraft. This type of material may have contributed to the volatile inventory of Earth and the other terrestrial planets. Bulk CI chondrites record a narrow range of δ 15 N values (i.e., the permil difference from the atmospheric 15 N/ 14 N ratio), averaging between +42 and 49‰. In contrast, recent analyses at CRPG’s noble gas facility revealed that two pelletized Ryugu samples have lower δ 15 N values of +18.1 ± 0.9‰ and +19.5 ± 0.9‰. Together with the low measured N abundances, this observation suggests that Ryugu has lost a 15 N-rich, labile organic phase due to pervasive aqueous alteration. Subsequent high-resolution step-heating analyses of an additional Ryugu particle demonstrated that the δ 15 N value varies significantly during successive extraction steps (between +1.0 ± 1.0‰ and 65.8 ± 1.1‰); the variable N isotopic composition points to the presence of several isotopically distinct N-carrier phases in CI-type material. Here, we report preliminary N-Ne-Ar results obtained for individual particles from an aggregate Bennu sample using the Noblesse-HR (Nu Instruments) noble gas mass spectrometer at CRPG’s noble gas facility. In a companion abstract, we will present the noble gas (He, Ne, Ar, Kr, Xe) characteristics of other aggregate particles determined with a HELIX MC Plus. Whereas the abundance and isotopic composition of noble gases permit detection of various presolar phases and the so-called phase Q, as well as quantification of solar wind–derived and cosmogenic components, the abundance and isotopic composition of N are expected to provide further insights into the origin and evolution of N-bearing phases in carbonaceous asteroids.

E Füri↗
NASA NTRS2024

Ubiquitous Presence of Sodium-Bearing Magnesium Phosphate in CI Chondritic Materials

The discovery that the asteroid Ryugu samples returned by the JAXA Hayabusa2 spacecraft are chemically and mineralogically nearly identical to CI chondrites has made us re-recognize the importance of CI chondrites in the early solar system [e.g., 1]. These CI chondritic materials have undergone strong aqueous alteration in their parent bodies, resulting in the formation of abundant Mg-Fe phyllosilicates along with other altered minerals such as carbonates, magnetite, and pyrrhotite. Initial and subsequent AO analyses of the Ryugu samples have found that they are brecciated on the mm~μm scale and that a small amount of forsterite and other primary minerals survive in some of the brecciated clasts with evidence of less degrees of aqueous alteration (“less altered clast”) [e.g., 1]. In addition, these less altered clasts contain a rare Na-bearing Mg phosphate that is still poorly characterized. Despite the analytical attempt to identify its mineral species, their identity has not been clarified yet. These rare Mg phosphates could be one of the key phases to understanding the evolution of CI chondritic bodies since a similar Na-bearing Mg phosphate has been reported from the asteroid Bennu sample returned by the NASA OSIRIS REx mission, and the importance of these materials has been suddenly highlighted. Since the initial analysis of the Ryugu sample, we have been paying attention to these Mg phosphates in CI chondrites as well as Ryugu samples, and here we report the present results on their mineralogical analysis.

T Mikouchi↗
NASA NTRSDate not supplied

Initial Analysis of Volatile Components in the Hayabusa2 Samples

The major objectives of the Hayabusa2-initial-analysis volatile team are (1) to determine the pristine volatile components in the parental materials of the returned Ryugu samples, and (2) to elucidate the origin and chronological history of the asteroid Ryugu, as well as the evolution of the solar system through determination of volatile carrier phases and abundances of volatile components (e.g., presolar grain abundances). Our analytical data will be linked with remote sensing (NIRS3, ONCs, TIR, and LIDAR) data and theoretical modeling [e.g., 1-5]. For example, the erosion rate and the degree of gardening of the surface layer of the asteroid Ryugu can be estimated based on trapped solar wind (SW) and cosmic ray produced (cosmogenic) nuclides, which will be discussed in conjunction with the results based on the remote sensing data [3-5]. Taken together, these will provide characteristics of the surface materials, such as the degree and duration of the alteration by SW/cosmic ray irradiation and micrometeorite bombardments.

volatiles↗
NASA NTRS2020

X-Ray Diffraction and Reflectance Spectroscopy of Murchison Powders (CM2) After Thermal Analysis Under Reducing Conditions to Final Temperatures Between 300 and 1300°c

The asteroids Ryugu and Bennu have spectral characteristics in common with CI/CM type carbonaceous chondrites and are target bodies for JAXA’s Hayabusa2 and NASA’s OSIRIS-Rex missions, respectively. Analog studies, based primarily on the Murchison CM2 chondrite, provide a pathway to separate spectral properties resulting space weathering from those inherent to parent-body, mineralogy, chemistry, and processes. Ryugu shares spectral properties with thermally metamorphosed and partly dehydrated CI/CM chondrites. We have undertaken a multidisciplinary study of the thermal decomposition of Murchison powder samples as an analog to metamorphic process that may have occurred on Ryugu. Bulk analyses include thermal And evolved gas analysis, X-ray diffraction (XRD), and VIS-NIR and Mössbauer spectroscopy; micro- to nanoscale analyses included scanning and transmission electron microscopy and electron probe micro analysisWe report here XRD and VIS-NIR analyses of pre- and post-heated Murchison powders, and in a companion paper report results from multiple electron beam techniques.

Morris, R. V.↗
NASA NTRSDate not supplied

New Hayabusa2 and OSIRIS REx Curation Facilities at Nasa Johnson Space Center

Asteroids are made up of rocky material that is left over from the formation of our solar system [1]. This material holds the key to unlocking information about the history of the planets and our sun. Hayabusa2 and OSIRIS-REx are two sample return missions that have collected rocky material from carbonaceous asteroids which are rich in water, carbon, and organic compounds [1]. Hayabusa2 is a spacecraft that collected samples from asteroid Ryugu launched by the Japan Aerospace Exploration Agency (JAXA). Samples were returned to Earth in December 2020 and 10 percent of the collected material is currently housed in a state-of-the-art laboratory at NASA Johnson Space Center (JSC) dedicated to Ryugu material [1]. OSIRIS-REx is a spacecraft launched by NASA that collected samples from asteroid Bennu. The samples are on their journey to Earth and will arrive in September 2023. They will be stored in a separate cleanroom dedicated to Bennu material. From these two missions, scientists will examine dust particles and rocky material to research clues on how the early solar system formed and how life began [2]. Because these samples are so precious and rare, it is important to keep them free from Earth contamination. In September of 2020, a massive construction project began to provide curation facilities to meet the needs of two incoming asteroid collections, Hayabusa2 and OSIRIS-REx. Despite numerous setbacks caused by the coronavirus pandemic, these facilities have been completed in the fall of 2021. Some of these setbacks included strict PPE requirements, keeping safe working distances as well as access to the facilities as NASA was operating under a Stage 3 condition in response to the pandemic. These facilities will provide curation laboratories to safely house the precious asteroid samples as well as facilities to manipulate samples, do sample preparation and process samples into and out of the labs for future studies by the scientific community. The lab suite consists of several different rooms including an initial anteroom (ISO 7), a staging area (ISO 7), two gowning areas (one for OSIRIS-REx and one for Hayabusa2; both ISO 6)), the Haybusa2 Curation Laboratory (ISO 5), the OSIRIS-REx Curation Laboratory (ISO 5), an ultramicrotomy laboratory (ISO 7) and a thin section laboratory (not a cleanroom). To maintain cleanliness levels necessary for these lab spaces quarterly to monthly Balazs organic and inorganic sampling has been conducted on a regular basis before, during and after the construction project to monitor the cleanliness levels in the new labs that will house the asteroid samples. These new facilities feature a Ruuvi (Grafana) monitoring system that measures temperature, humidity, and pressure of the lab suite. This is a small puck shaped sensor that sends signals to the Grafana cloud where the data can be plotted and set up on dashboards within the lab suite. These sensors are easy to set up and install and they run off a cell battery that is good for 3-5 years before needing replacement. This system can deliver text messages and emails to the appropriate personnel when values fall outside of set limits. In addition to the monitoring system, this new lab suite features viewing windows from several different locations and sliding motion censored doors. We have obtained some state-of-the-art equipment to outfit the lab spaces (desiccators, microscopes, ultramicrotome) and are in the process of outfitting the suite with additional items such as: nitrogen gloveboxes, additional desiccators, micromanipulators, etc. The Hayabusa2 samples provided to NASA by JAXA included 23 millimeter sized grains and 4 containers with finer material. OSIRIS-REx is expected to return as much as 400 grams of asteroid Bennu. Samples will be stored in a nitrogen glove box and separated into nitrogen sealed transfer containers. Small Bennu and Ryugu particles will be handled and prepared (e.g., ultra-thin sections for scanning electron microscopy (SEM) or transmission electron microscopy (TEM)) using an Axis Pro micromanipulator and Leica EM UC7 ultramicrotome. Analyzing samples at the atomic scale will provide greater insight to the origins of the solar system and life formation on Earth. All the curation preparation for these sample collections is essential to ongoing research and efforts to understand our solar system, both nowand for future generations.

Curation↗
NASA NTRSDate not supplied

New Directions in the Quest for Unaltered Ci-Like Material From the Early Solar System

CI meteorites have bulk chemical compositions closely matching the solar photosphere (except volatiles) and thus are considered to represent the starting composition of the Solar System. The return of CI-like samples from asteroid (162173) Ryugu by Hayabusa2 has greatly bolstered studies of CI. However, both CI and the Ryugu samples are CI1, i.e., they were extensively altered by aqueous fluids on their parent bodies so the mineralogy, textures, and oxygen isotope compositions of their CI3 precursors have been obscured. Fortunately, they contain rare remnants of primordial minerals in the form of small anhydrous silicate and Ca-Al-rich grains, and detailed petrologic and isotopic studies of these grains have helped elucidate the nature of their precursors. Here, we continue our work on petrologic and isotopic studies of such phases in Ryugu particle C0137.

C A Goodrich↗
NASA NTRS2016

Unique View of C Asteriod Regolith from the Jbilet Winselwan CM Chondrite

C-class asteroids frequently exhibit reflectance spectra consistent with thermally metamor-phosed carbonaceous chondrites, or a mixture of phyllosilicate-rich material along with regions where they are absent. One particularly important example appears to be asteroid 162173 Ryugu, the target of the Hayabusa 2 mission, although most spectra of Ryugu are featureless, suggesting a heterogeneous regolith. Here we explore an alternative cause of dehydration of regolith of C-class asteroids impact shock melting. Impact shock melting has been proposed to explain some mineralogical characteristics of CB chondrites, but has rarely been considered a major process for hydrous carbonaceous chondrites. Jbilet Winselwan (JW) is a very fresh CM breccia from Morocco, with intriguing characteristics. While some lithologies are typical of CM2s, other clasts show evidence of brief, though significant impact brecciation and heating. The first evidence for this came from preliminary petrographic and stable isotope studies. We contend that highly-brecciated, partially-shocked, and dehydrated lithologies like those in JW dominate C-class asteroid regolith.

Zolensky, Michael↗
NASA NTRS2016

The Nature of C Asteroid Regolith Revealed from the Jbilet Winselwan CM Chondrite

C-class asteroids frequently exhibit reflectance spectra consistent with thermally metamorphosed carbonaceous chondrites, or a mixture of phyllosilicate-rich material along with regions where they are absent. One particularly important example appears to be asteroid 162173 Ryugu, the target of the Hayabusa 2 mission, although most spectra of Ryugu are featureless, suggesting a heterogeneous regolith. Here we explore an alternative cause of dehydration of regolith of C-class asteroids - impact shock melting. Impact shock melting has been proposed to ex-plain some mineralogical characteristics of CB chondrites, but has rarely been considered a major process for hydrous carbonaceous chondrites.

Zolensky, Michael↗
NASA NTRS2017

Impact Record of a Asteroid Regolith Recorded in a Carbonaceous Chrondrite

C-class asteroids frequently exhibit reflectance spectra consistent with thermally metamor-phosed carbonaceous chondrites [1], or a mixture of phyllosilicate-rich material along with regions where they are absent [2]. One particularly important example appears to be asteroid 162173 Ryugu, the target of the Hayabusa 2 mission [1], although most spectra of Ryugu are featureless, suggesting a heterogeneous regolith [3]. Here we explore an alternative cause of dehydration of regolith of C-class asteroids - impact shock melting. Impact shock melting has been proposed to ex-plain some mineralogical characteristics of CB chondrites [4], but has rarely been considered a major process for hydrous carbonaceous chondrites [5]. Jbilet Winselwan (JW) is a very fresh CM breccia from Morocco, with intriguing characteristics. While some lithologies are typical of CM2s (Figure 1, top), other clasts show evidence of brief, though significant impact brecciation and heating. The first evidence for this came from preliminary petrographic and stable isotope studies [6,7]. We contend that highly-brecciated, partially-shocked, and dehydrated lithologies like those in JW dominate C-class asteroid regolith.

Zolensky, Michael↗
NASA NTRS2018

Physical, Chemical, and Petrological Characteristics of Chondritic Materials and Their Relationships to Small Solar System Bodies: Chapter - 2

Chondrite materials with varying abundances of volatile-bearing phases are expected at the destinations for the asteroid sample-return missions Hayabusa2 and OSIRIS-REx. The targets of the missions are 162173 (1999 JU3) Ryugu and 101955 (1999 RQ36) Bennu. Spectroscopic analyses of these asteroids suggest that their surface materials are related to types 1 and 2 carbonaceous chondrites. Some studies suggest that the parent bodies of these chondrites may have also experienced some thermal and/or shock metamorphism. The physical properties of boulders at asteroid surfaces and fine particles in asteroid regoliths are consequences of the diverse processes that fragmented them, mobilized them, and redeposited them in unique accumulations. Sample-return missions are likely to encounter a broad range of carbonaceous chondrite (CC)-like materials, to which aqueous alteration, thermal, and shock metamorphism imparted changes affecting their sub-micron- to meter-scale physical properties. Consequently, implementation of scale-dependent analytical techniques to the study of the chemical, physical, and geotechnical characteristics of these CC-like materials is fundamental to safe mission operations, sample selection, and return. However, most of the available knowledge for informing and formulating expectations about regolith processes, products, and properties on carbonaceous small bodies comes from missions that studied anhydrous (e.g., Itokawa studied by Hayabusa) and/or much larger asteroids (e.g., Vesta studied by Dawn). No previous mission is likely directly relevant to small ice-free carbonaceous NEOs 162173 Ryugu or 101955 Bennu, although the Rosetta Spaceraft performed a flyby of the large asteroid Lutetia which has variously been classified as M and C type (Pätzold et al., 2011). Carbonaceous chondrites carry the best record of the history, distribution, and activity of water in the early solar system. Ordinary and Enstatite chondrites carry only partial records, but these are still critical to understanding the full story. We will describe the records of water-rock interactions on asteroids, as recorded in these meteorites, with particular emphasis on the timing, nature, settings, and fluid compositions. An integral part of this story is the rare, but fortunate, preservation of actual early solar system water as aqueous fluid inclusions.

Zolensky, Michael E.↗
NASA NTRS2020

Irradiation-energy Dependence on the Spectral Changes of Hydrous C-Type Asteroids Based on 4kev and 20kev He Exposure Experiments of Murchison Cm Chondrite

C-type asteroid 162173 Ryugu was observed by remote sensing apparatus onboard Hayabusa2 spacecraft and found to be very dark object whose reflectance is (1.60 ± 0.15) % at 0.55μm and showed a small 2.7μm absorption band indicative of phyllosilicates. The optical navigation camera detected color variations of Ryugu’s surface in the wavelength range from 0.4 to 0.95μm: Bluer spectra are ob-served at both poles and on the equatorial ridge, both of which are topographic highs and thus may be fresh material exposed by gradual erosion. On the other hand, many locations at middle-latitude areas exhibit redder and darker colors. Similar color variations are also detected in the near-infrared wavelength range. These observations suggest that a surface-correlated process is responsible for the color variation, most prob-ably from blue to red, but the mechanism for the change is not yet identified. Space weathering is one possible mechanism responsible for the color variation, but the spectral changes of C-type asteroids from space weathering are far from being fully understood. Past experimental studies using hydrous carbonaceous chondrites such as Murchison and Tagish Lake show that He exposure (simulating solar wind irradiation) changes spectra to bluer and brighter. Recently our He exposure experiments indicate that spectral changes depend on physical properties such as porosity of exposed material. In this study, we per-formed further He exposure experiments using Murchison CM chondrite in order to understand energy dependence on the spectral changes. We found that He energy is a critical parameter, as well as physical properties of the samples, that affects spectral changes of space weathering of hydrated C-type asteroids.

Nakamura, T.↗
NASA NTRS2020

Brecciation of CM Chondrites: Cold Bokkeveld

C-complex asteroids frequently exhibit reflectance spectra consistent with thermally metamor-phosed or shocked carbonaceous chondrites, and brecciation, including Ryugu, and Bennu. Petrographic evidence of brecciation has been presented for CM, and here we reexamine Cold Bokkeveld, one of the most diverse CM breccias, as a preview of the samples to be returned from Ryugu and Bennu.

Zolensky, M.↗
NASA NTRS2020

Photometry of Asteroid (101955) Bennu with OVIRS on OSIRIS-REx

NASA’s OSIRIS-REx spacecraft arrived at its sampling target, asteroid (101955) Bennu, in December 2018 and started a series of global observation campaigns. Here we investigate the global photometric properties of Bennu as observed by the OSIRIS-REx Visible and InfraRed Spectrometer (OVIRS) over the time period December 9, 2018, to September 26, 2019. In this study we used observations obtained over wavelengths ranging from 0.4 to 3.7 μm, with a solar phase angle range of 5.3° to 132.6°. Our aim is to characterize the global average disk-resolved photometric properties of Bennu with multiple models. The best-fit model is a McEwen model with an exponential phase function and an exponential polynomial partition function. We use this model to correct the OVIRS spectra of Bennu to a standard reference viewing and illumination geometry at visible to infrared wavelengths for the purposes of global spectral mapping. We derive a bolometric Bond albedo map in which Bennu’s surface values range from 0.021 to 0.027. We find a phase reddening effect, and our model is effective at removing this phase reddening. Our average model albedo shows a blueish spectrum with a >10% absorption feature centered at 2.74 μm. Of all comparisons with previously visited asteroids and comets, only 28P/Neujmin, 2P/Encke, and (162173) Ryugu are darker than Bennu. We find that Bennu is a few percent brighter than Ryugu in the wavelengths respectively observed by the OSIRIS-REx and Hayabusa2 missions (from 0.48 to 0.86 μm). We also compare our spectroscopic photometry of Bennu with the OSIRIS-REx imaging photometry and with ground-based predictions.

Asteroid Bennu↗
NASA NTRS2023

Investigating the Role of Incident Ion Flux in Solar Wind Space Weathering of Carbon-Rich Asteroidal Regolith Via H+ and He+ Irradiation of the Murchison Meteorite

We present results from a set of low and high flux 1 keV/amu H + and He + irradiation experiments performed on slabs of the Murchison CM2 carbonaceous chondrite. The low flux conditions for H + and He + irradiation were ~1-1.5 orders of magnitude lower than the high flux conditions, and each experiment was irradiated to a total fluence between ~3 × 10 16 to ~6 × 10 16 ions/cm 2 . Irradiation-induced changes in the surface chemistry and optical properties of the Murchison samples were evaluated using in situ X-ray photoelectron spectroscopy (XPS) and visible and near-infrared spectroscopy (VNIR). We characterized the microstructure and composition of ion damaged rims in focused ion beam (FIB) cross-sections extracted from olivine and matrix material in each irradiated Murchison slab using transmission electron microscopy (TEM). XPS results suggest that both low flux and high flux H + and He + irradiation cause minor sputtering of surface carbon as well as a reduction in the valence state of iron, from Fe 3+ to Fe 2+ . Slope bluing is observed in VNIR spectra of the irradiated samples which may reflect carbonization and dehydrogenation of organic species and contrasts with reddening trends associated with npFe 0 formation. Although we do not observe a strong flux-dependence on the crystallinity of ion-damaged olivine, TEM analyses reveal a variety of microstructures in all olivine FIB-sections, suggesting that crystallographic orientation affects amorphization efficiency. Analyses of matrix FIB-sections indicate that phyllosilicate alteration is mainly driven by He+ irradiation, where the higher incident flux leads to greater amorphization and the formation of more distinct ion-damaged layers, similar to smooth layers in returned Ryugu particles. TEM results also provide some evidence that higher ion flux leads to greater vesiculation, with He + irradiation being more efficient at vesiculation than H + irradiation, and that higher ion flux may promote the segregation of Mg and Si into laterally extensive lenses and layers in olivine samples. We discuss the implications of these findings for constraining the role that ion flux plays in the development of space weathering characteristics in silicate phases present in carbonaceous asteroidal regoliths. These results will be important for understanding the complexity of this process and how it operates on carbon-rich airless bodies like asteroids Bennu and Ryugu.

meteorites↗
NASA NTRSDate not supplied

Assessing the Oxygen Permeability of Candidate Asteroid Sample Containers With Optochemical Sensors

The Astromaterials Acquisition and Curation Office at NASA Johnson Space Center currently curates 500 mg (10%) of carbonaceous asteroid Ryugu regolith collected by the Japan Aerospace and Exploration Agency’s Hayabusa II spacecraft and returned to Earth in 2021. In September 2023, NASA’s OSIRIS-REx spacecraft returned at least 70 grams of regolith collected from the surface of Carbonaceous Asteroid Bennu. These new astromaterials collections are stored and handled in gloveboxes and desiccators that are continuously purged with ultrapure nitrogen in order to minimize contamination and alteration of extraterrestrial samples from terrestrial environments, e.g., reaction with terrestrial oxygen and water. Ito et al. have previously reported on the development of containers to transport samples between facilities in inert, sealed environments; Hayabusa2 samples allocated to investigators by JAXA’s Extraterrestrial Sample Curation Center (ESCuC) are shipped in these Facility-to-Facility Transfer Containers (FFTCs). NASA curation has also been investigating sealed containers for storage, transportation, and allocation of Bennu and Ryugu regolith in sealed anoxic environments. In order to assess the ability of candidate sample containers to maintain nitrogen environments, we have utilized optochemical sensors to measure trace oxygen levels within sealed volumes.

C J Snead↗