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At least 109 records · Page 6

Shield materials recommended for space power nuclear reactors

Lithium hydride is recommended for neutron attenuation and depleted uranium is recommended for gamma ray attenuation. For minimum shield weights these materials must be arranged in alternate layers to attenuate the secondary gamma rays efficiently. In the regions of the shield near the reactor, where excessive fissioning occurs in the uranium, a tungsten alloy is used instead. Alloys of uranium such as either the U-0.5Ti or U-8Mo are available to accommodate structural requirements. The zone-cooled casting process is recommended for lithium hydride fabrication. Internal honeycomb reinforcement to control cracks in the lithium hydride is recommended.

Kaszubinski, L. J.↗

Tungsten fiber reinforced superalloys - A status review

After a review of refractory metal fiber/alloy matrix composite development, a discussion is presented of the fabrication techniques used in production of tungsten fiber reinforced superalloys (TFRS), their most significant properties, and their potential applications in the hot section components of gas turbine engines. Emphasis is given the development of airfoil-fabrication technology, with a view to the production of TFRS turbine blades, and attention is given the first-generation TFRS material, a tungsten alloy fiber/FeCrAlY composite currently under evaluation. Detailed properties, design criteria and cost data are presented for this material. Among the properties covered are stress-rupture strength, high and low cycle fatigue, thermal fatigue, impact strength, oxidation and corrosion and thermal conductivity.

Petrasek, D. W.↗

Tensile Behavior of Tungsten/Niobium Composites at 1300 to 1600 K

The tensile behavior of continuous tungsten fiber reinforced niobium composites (W/Nb), fabricated by an arc-spray process, was studied in the 1300 to 1600 K temperature range. The tensile properties of the fiber and matrix components as well as of the composites were measured and were compared to rule of mixtures (ROM) predictions. The deviation from the ROM was found to depend upon the chemistry of the tungsten alloy fibers, with positive deviations for ST300/Nb (i.e., stronger composite strength than the ROM) and negative or zero deviations for 218/Nb.

Yun, Hee Mann↗

Solar Probe thermal shield design and testing

This paper discusses the major thermal shield subsystem development activities in support of the Solar Probe study being conducted at JPL. The Solar Probe spacecraft will travel to within 4 solar radii of the sun's center to perform fundamental experiments in space physics. Exposure to 2900 earth suns at perihelion requires the spacecraft to be protected within the shadow envelope of a protective shield. In addition, the mass loss rate off of the shield at elevated temperature must comply with plasma instrument requirements and has become the driver of the shield design. This paper will focus on the analytical design work to size the shield and control the shield mass loss rate for the various spacecraft options under study, the application of carbon-carbon materials for shield components, development and preparation of carbon-carbon samples for materials testing, and a materials testing program for carbon-carbon and tungsten alloys to investigate thermal/optical properties, mass loss (carbon-carbon only), material integrity, and high velocity impact behavior.

Millard, Jerry M.↗

Tensile strain-rate sensitivity of tungsten/niobium composites at 1300 to 1600 K

The tensile behavior of continuous tungsten fiber reinforced niobium composites (W/Nb), fabricated by an arc-spray process, was studied in the 1300 to 1600 K temperature range. The tensile properties of the fiber and matrix components as well as of the composites were measured and were compared to rule of mixtures (ROM) predictions. The deviation from the ROM was found to depend upon the chemistry of the tungsten alloy fibers, with positive deviations for ST300/Nb (i.e., stronger composite strength than the ROM) and negative or zero deviations for 218/Nb.

Yun, H. M.↗

An Evanescent Microwave Probe for Super-Resolution Nondestructive Imaging of Metals, Semiconductors, Dielectrics, Composites and Biological Specimens

Using evanescent microwaves with decay lengths determined by a combination of microwave wavelength (lambda) and waveguide termination geometry, we have imaged and mapped material non-uniformities and defects with a resolving capability of lambda/3800=79 microns at 1 GHz. In our method a microstrip quarter wavelength resonator was used to generate evanescent microwaves. We imaged materials with a wide range of conductivities. Carbon composites, dielectrics (Duroid, polymers), semiconductors (3C-SiC, polysilicon, natural diamond), metals (tungsten alloys, copper, zinc, steel), high-temperature superconductors, and botanical samples were scanned for defects, residual stresses, integrity of brazed junctions, subsurface features, areas of different film thickness and moisture content. The evanescent microwave probe is a versatile tool and it can be used to perform very fast, large scale mapping of a wide range of materials. This method of characterization compares favorably with ultrasound testing, which has a resolution of about 0.1 mm and suffers from high absorption in composite materials and poor transmission across boundaries. Eddy current methods which can have a resolution on the order of 50 microns are restricted to evaluating conducting materials. Evanescent microwave imaging, with careful choice of operating frequency and probe geometry, can have a resolution of up to 1 micron. In this method we can scan hot and moving objects, sample preparation is not required, testing is non-destructive, non-invasive and non-contact, and can be done in air, in liquid or in vacuum.

Pathak, P. S.↗

Experimental Shock Decomposition of Siderite and the Origin of Magnetite in Martian Meteorite ALH84001

Shock recovery experiments to determine whether magnetite could be produced by the decomposition of iron-carbonate were initiated. Naturally occurring siderite was first characterized by electron microprobe (EMP), transmission electron microscopy (TEM), Mossbauer spectroscopy, and magnetic susceptibility measurements to be sure that the starting material did not contain detectable magnetite. Samples were shocked in tungsten-alloy holders (W=90%, Ni=6%, Cu=4%) to further insure that any iron phases in the shock products were contributed by the siderite rather than the sample holder. Each sample was shocked to a specific pressure between 30 to 49 GPa. Previously reported results of TEM analyses on 49 GPa experiments indicated the presence of nano-phase spinel-structured iron oxide. Transformation of siderite to magnetite as characterized by TEM was found in the 49 GPa shock experiment. Compositions of most magnetites are greater than 50% Fe sup(+2) in the octahedral site of the inverse spinel structure. Magnetites produced in shock experiments display the same range of single-domain, superparamagnetic sizes (approx. 50 100 nm), compositions (100% magnetite to 80% magnetite-20% magnesioferrite), and morphologies (equant, elongated, euhedral to subhedral) as magnetites synthesized by Golden et al. (2001) or magnetites grown naturally by MV1 magnetotactic bacteria, and as the magnetites in Martian meteorite ALH84001. Fritz et al. (2005) previously concluded that ALH84001 experienced approx. 32 GPa pressure and a resultant thermal pulse of approx. 100 - 110 C. However, ALH84001 contains evidence of local temperature excursions high enough to 1 melt feldspar, pyroxene, and a silica-rich phase. This 49 GPa experiment demonstrates that magnetite can be produced by the shock decomposition of siderite as a result of local heating to greater than 470 C. Therefore, magnetite in the rims of carbonates in Martian meteorite ALH84001 could be a product of shock devolatilization of siderite as well.

Bell, Mary Sue↗

Latest Progress on the Gamma-Ray Imager/Polarimeter for Solar Flares (GRIPS)

We present the latest progress on building the balloon-borne Gamma-Ray Imager/Polarimeter for Solar flares (GRIPS) instrument, including testing and calibration of the detectors and development of the imaging and aspect systems. A continental-US test flight is slated for fall 2012. GRIPS will provide a near-optimal combination of high-resolution imaging, spectroscopy, and polarimetry of solar-flare gamma-ray/hard X-ray emissions from approx.20. keV to > approx.10 MeV. The spectrometer/polarimeter consists of sixteen 3D position-sensitive germanium detectors (3D-GeDs), where each energy deposition is individually recorded with an energy resolution of a few keV FWHM and a spatial resolution to within <0.1 cu mm. Imaging is accomplished by a single multi-pitch rotating modulator (MPRM), a 2.5-cm thick tungsten-alloy grid with pitches that range quasi-continuously from 1 to 13 mm. With the MPRM situated 8 meters from the spectrometer, this instrument will provide excellent image quality and unparalleled angular resolution at gamma-ray energies (12.5 arcsec FWHM), sufficient to separate the 2.2 MeV footpoint sources for almost all flares. Polarimetry is accomplished by analyzing the anisotropy of reconstructed Compton scattering in the 3D-GeDs (i.e. as an active scatterer), with an estimated minimum detectable polarization of a few percent at 150-650 keV in an X-class flare. GRIPS will address questions relevant to particle acceleration and energy release that ha-.e been raised by recent solar flare observations, such as: What causes the spatial separation between energetic electron producing hard X-rays and energetic ions producing gamma-ray lines? How anisotropic are the accelerated electrons, and why do relativistic electron dominate in the corona? How does the composition of accelerated and ambient material vary with space and time, and why?

Shih, Albert Y.↗

The Gamma-Ray Imager/Polarimeter for Solar Flares (GRIPS)

The balloon-borne Gamma-Ray Imager/Polarimeter for Solar flares (GRIPS) instrument will provide a near-optimal combination of high-resolution imaging, spectroscopy, and polarimetry of solar-flare gamma-ray/hard X-ray emissions from approximately 20 keV to greater than approximately 10 MeV. GRIPS will address questions raised by recent solar flare observations regarding particle acceleration and energy release, such as: What causes the spatial separation between energetic electrons producing hard X-rays and energetic ions producing gamma-ray lines? How anisotropic are the relativistic electrons, and why can they dominate in the corona? How do the compositions of accelerated and ambient material vary with space and time, and why? The spectrometer/polarimeter consists of sixteen 3D position-sensitive germanium detectors (3D-GeDs), where each energy deposition is individually recorded with an energy resolution of a few keV FWHM and a spatial resolution of less than 0.1 cubic millimeter. Imaging is accomplished by a single multi-pitch rotating modulator (MPRM), a 2.5-centimeter thick tungsten alloy slit/slat grid with pitches that range quasi-continuously from 1 to 13 millimeters. The MPRM is situated 8 meters from the spectrometer to provide excellent image quality and unparalleled angular resolution at gamma-ray energies (12.5 arcsec FWHM), sufficient to separate 2.2 MeV footpoint sources for almost all flares. Polarimetry is accomplished by analyzing the anisotropy of reconstructed Compton scattering in the 3D-GeDs (i.e., as an active scatterer), with an estimated minimum detectable polarization of a few percent at 150-650 keV in an X-class flare. GRIPS is scheduled for a continental-US engineering test flight in fall 2013, followed by long or ultra-long duration balloon flights in Antarctica.

Shih, Albert Y.↗

Feasibility of producing cast-refractory metal-fiber superalloy composites

A study was conducted to evaluate the feasibility of direct casting as a practical method for producing cast superalloy tungsten or columbium alloy fiber composites while retaining a high percentage of fiber strength. Fourteen nickel base, four cobalt, and three iron based matrices were surveyed for their degree of reaction with the metal fibers. Some stress-rupture results were obtained at temperatures of 760, 816, 871, and 1093 C for a few composite systems. The feasibility of producing acceptable composites of some cast nickel, cobalt, and iron matrix alloys with tungsten or columbium alloy fibers was demonstrated.

Mcintyre, R. D.↗

High strength forgeable tantalum base alloy

Increasing tungsten content of tantalum base alloy to 12-15% level will improve high temperature creep properties of existing tantalum base alloys while retaining their excellent fabrication and welding characteristics.

Buckman, R. W., Jr.↗

High Performance Arcjet Engines

This effort sought to exploit advanced single crystal tungsten-tantalum alloy material for fabrication of a high strength, high temperature arcjet anode. The use of this material is expected to result in improved strength, temperature resistance, and lifetime compared to state of the art polycrystalline alloys. In addition, the use of high electrical and thermal conductivity carbon-carbon composites was considered, and is believed to be a feasible approach. Highly conductive carbon-carbon composite anode capability represents enabling technology for rotating-arc designs derived from the Russian Scientific Research Institute of Thermal Processes (NIITP) because of high heat fluxes at the anode surface. However, for US designs the anode heat flux is much smaller, and thus the benefits are not as great as in the case of NIITP-derived designs. Still, it does appear that the tensile properties of carbon-carbon can be even better than those of single crystal tungsten alloys, especially when nearly-single-crystal fibers such as vapor grown carbon fiber (VGCF) are used. Composites fabricated from such materials must be coated with a refractory carbide coating in order to ensure compatibility with high temperature hydrogen. Fabrication of tungsten alloy single crystals in the sizes required for fabrication of an arcjet anode has been shown to be feasible. Test data indicate that the material can be expected to be at least the equal of W-Re-HfC polycrystalline alloy in terms of its tensile properties, and possibly superior. We are also informed by our colleagues at Scientific Production Association Luch (NP0 Luch) that it is possible to use Russian technology to fabricate polycrystalline W-Re-HfC or other high strength alloys if desired. This is important because existing engines must rely on previously accumulated stocks of these materials, and a fabrication capability for future requirements is not assured.

Kennel, Elliot B.↗

Creep Resistance of Disk Alloy CH98 with Tungsten and Niobium Additions

Gas turbine engines for future subsonic transports will likely have higher pressure ratios which will require nickel-base superalloy disks with temperature capability up to 1400 F, an increase of about 200 F over current engines. Several advanced disk alloys are being developed to fill this need. One of these, CH98, is a promising candidate for gas turbine engines and is being studied in NASA's AST Program. Additions of the refractory elements tungsten and niobium have been shown to improve tensile and creep properties while maintaining good high temperature fatigue crack growth resistance. Further improvements in creep and crack growth resistance can be achieved with a coarse grain microstructure. The purpose of the present study is aimed at providing a detailed assessment of 0.2 percent creep rates for coarse grain CH98 with tungsten and niobium additions over a range of temperatures and stresses of interest to disk applications.

Gayda, John↗

Thermal expansion method for lining tantalum alloy tubing with tungsten

A differential-thermal expansion method was developed to line T-111 (tantalum - 8 percent tungsten - 2 percent hafnium) tubing with a tungsten diffusion barrier as part of a fuel element fabrication study for a space power nuclear reactor concept. This method uses a steel mandrel, which has a larger thermal expansion than T-111, to force the tungsten against the inside of the T-111 tube. Variables investigated include lining temperature, initial assembly gas size, and tube length. Linear integrity increased with increasing lining temperature and decreasing gap size. The method should have more general applicability where cylinders must be lined with a thin layer of a second material.

Watson, G. K.↗