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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 109 records · Page 6
All sourcesNASA NTRSDOE OSTI
DOE OSTI2025

Skyrmion-like Spin Textures Emerging in the Material Derived from Structural Frustration

Magnetic materials with complex spin textures present both fundamental and practical appeal. The complex patterns of magnetic moments emerging on underlying crystal lattices hold potential for robust information storage and processing, including the promise of topological quantum computing. The scope of materials that host such patterns, however, remains rather limited. Here, in this study, we report a discovery of a complex spin texture in a noncentrosymmetric material that emerges from the structural frustration at the boundary between centrosymmetric parent structures MnCoGe (the hexagonal Ni 2 In or the orthorhombic TiNiSi structure type) and MnCoAs (the TiNiSi structure type). Our findings demonstrate that such structural frustration provides a powerful handle for identifying compositional spaces where complex magnetic behavior and associated nontrivial magnetic structures are likely to emerge. Thus, the new phase MnCoGe 1/3 As 2/3 exhibits a modulated cycloidal antiferromagnetic arrangement of electron spins on a noncentrosymmetric lattice (of the hexagonal ZrNiAl type) that materializes in the space between centrosymmetric collinear ferromagnets. This work provides a pathway for discovering novel materials with exotic spin textures for next-generation spintronics and quantum technologies.

Wang, YiXu [Florida State University, Tallahassee,↗
DOE OSTI2025

Emergent topological polarization textures in relaxor ferroelectrics

Relaxor ferroelectrics underpin high-performance actuators and sensors, yet the nature of polar heterogeneities driving their broadband dielectric response remains debated. Using a unified, multimodal structural refinement framework— simultaneously fitting complementary X-ray and neutron total scattering, X-ray absorption spectra, and diffuse scattering—we reconstruct 3D mesoscale polarization maps in the classic relaxor system PbMg 1/3 Nb 2/3 O 3 –PbTiO 3 . We uncover self-organized swirling polarization textures with half-skyrmion (meron) vortices, challenging models of independent polar nanoregions. These textures, characterized by smooth changes in the polarization direction, originate from overlapping volumes in which the projections of locally correlated polarization vectors onto each volume’s long axis share the same sign. Vortex cores correlate strongly with local charge and strain gradients imposed by compositional heterogeneities. In this work, our results suggest that chemical disorder, acting via depolarizing and strain fields, stabilizes topological vortex textures of the polarization field, offering a route for engineering new dielectric and ferroelectric functionalities.

Eremenko, Maksim [National Institute of Standards ↗
DOE OSTI2024

AI-enabled Lorentz microscopy for quantitative imaging of nanoscale magnetic spin textures

The manipulation and control of nanoscale magnetic spin textures are of rising interest as they are potential foundational units in next-generation computing paradigms. Achieving this requires a quantitative understanding of the spin texture behavior under external stimuli using in situ experiments. Lorentz transmission electron microscopy (LTEM) enables real-space imaging of spin textures at the nanoscale, but quantitative characterization of in situ data is extremely challenging. Here, we present an AI-enabled phase-retrieval method based on integrating a generative deep image prior with an image formation forward model for LTEM. Our approach uses a single out-of-focus image for phase retrieval and achieves significantly higher accuracy and robustness to noise compared to existing methods. Furthermore, our method is capable of isolating sample heterogeneities from magnetic contrast, as shown by application to simulated and experimental data. This approach allows quantitative phase reconstruction of in situ data and can also enable near real-time quantitative magnetic imaging.

36 MATERIALS SCIENCE↗
DOE OSTI2024

Multifunctional textured graphene-based coatings on elastomeric gloves for chemical protection

Nanotechnology offers a variety of new tools for the design of next-generation personal protective equipment (PPE). One example is the use of two-dimensional materials as coatings that enhance the performance and ergonomics of elastomeric gloves designed to protect users from hazardous chemicals. Desirable features in such coatings may include molecular barrier function, liquid droplet repellency, stretchability for compatibility with the elastomer, breathability, and an ultrathin profile that preserves the user's manual dexterity and tactile sensation. The present work explores the potential of engineered graphene-based films with out-of-plane texturing as a novel platform to meet these multifold requirements. Graphene-based films in different formulations were fabricated from water-borne inks by vacuum filtration and solution casting methods on glove-derived nitrile rubber substrates. The various coatings were then subjected to tests of molecular permeation by model volatile organic compounds, droplet contact angle, breathability, and mechanical stability during stretching and solvent immersion. The films dramatically improve the barrier properties of glove-derived nitrile. The out-of-plane graphene texturing imparts stretchability through microscale folding/unfolding, while also enhancing droplet repellency in some cases through a lotus-like roughening effect. The combined results suggest that engineered textured graphene-based films are a promising platform for creating multifunctional coatings for a next generation of chemically protective gloves and other elastomer-based PPE.

36 MATERIALS SCIENCE↗
DOE OSTI2025

Surface Texture of Macroplastic Pollution in Streams Alters the Physical Structure and Diversity of Biofilm Communities

ABSTRACT Biofilms can develop on nearly any surface, and in aquatic ecosystems they are essential components of biogeochemical cycles and food webs. Plastic waste in waterways is a new type of surface for biofilm colonisation. To analyse the influence of plastic pollution on the development and diversity of microbial freshwater biofilms that colonised them, we incubated 388 cm 2 veneers of high‐density polyethylene (HDPE) with two veneer textures, smooth and rough, and tulip tree wood ( Liriodendron tulipifera ), in three rural headwater streams at the Savannah River Site (Aiken, SC, USA). We collected biofilms from veneers after 14, 28 and 56 days of incubation and analysed 16S rRNA genes and biofilm properties. We found that plastic negatively affected species richness of biofilms compared with wood, but that evenness was greatest on rough textured HDPE. Beta diversity was primarily influenced by stream site. Beta diversity differed more between wood and plastic veneers than with plastic surface texture and became more different over time. Wood had nine times more biomass than rough HDPE and 40 times more biomass than smooth HDPE. Given the projected increase of macroplastic pollution in aquatic ecosystems, our findings emphasise the need to further understand its effects on biofilm characteristics.

Lopez Avila, Fabiola [Odum School of Ecology Unive↗
DOE OSTI2025

Nanoscale engineering and dynamic stabilization of mesoscopic spin textures

Thermalization, while ubiquitous in physics, has traditionally been viewed as an obstacle to be mitigated. In contrast, we demonstrate here the use of thermalization in the generation, control, and readout of “shell-like” spin textures with interacting 13 C nuclear spins in diamond, wherein spins are polarized oppositely on either side of a critical radius. The textures span several nanometers and encompass many hundred spins; they are created and interrogated without manipulating the nuclear spins individually. Long-time stabilization is achieved via prethermalization to a Floquet-engineered Hamiltonian under the electronic gradient field: The texture is therefore metastable and robust against spin diffusion. This enables the state to endure over multiple minutes before it decays. Our work on spin-state engineering paves the way for applications in quantum simulation and nanoscale imaging.

42 ENGINEERING↗
DOE OSTI2026

Uniaxial Spin Texture in a Superconducting Electron Gas Revealed by Exchange Interactions

Two-dimensional (2D) superconductors with spin-textured Fermi surfaces can be a platform for realizing unconventional pairing states and are of substantial interest in the context of quantum information science and superconducting spintronics/orbitronics. We observed an unusual in-plane uniaxial anisotropy in the superconducting 2D electron gas (2DEG) formed at EuOx/KTaO3 (110) interfaces. This anisotropy is not evident in AlOx/KTaO3 (110) where the overlayer is nonmagnetic. Our results are consistent with a highly anisotropic “half-Rashba” spin-textured Fermi surface in 2DEGs formed at the KTaO3 (110) interface that is hidden from external magnetic fields due to a near cancellation between orbital and spin moments but revealed by exchange interactions of the electrons in the 2DEG with Eu moments near the EuOx/KTaO3 (110) interface. The interactions between the uniaxial spin texture and the magnetic overlayer offer previously unexplored ways to explore the interplay between magnetism and 2D superconductivity.

Yang, Junyi↗
NASA NTRS1974

Texturing and residual stress in metals as a result of sliding

Pole figures of the texturing produced by friction in the alloys Cu - 10 at. % Sn, Cu - 10 at. % Si, 440 C stainless steel, and AISI 52100 bearing steel were obtained with an energy-dispersive X-ray diffractometer. While the texturing behavior of these alloys is generally similar to that of pure metals, the 52100 steel and the Cu5Si phase of Cu - 10 at. % Si show no texturing at the loads and speeds used in this experiment. Photographic methods were used in an attempt to measure the uniform residual stress in the wear tracks produced on some pure metals. The stress in copper and iron was, however, below the limit of detectability - about 4.3 x 10 to the 7th power N/sq m (6000 psi). Line broadening under all test conditions in the case of copper and at high load and speed conditions in iron is attributed, at least in part, to the reduction of crystallite size and, perhaps, to nonuniform residual stress, as well.

Wheeler, D. R.↗
NASA NTRS1977

Dynamic crystallization experiments bearing on the origin of textures in impact-generated liquids

Dynamic crystallization experiments on a synthetic glass of 14310 composition show that the density and distribution of crystals present at the initiation of cooling can drastically affect the texture of the crystallized product. Experiments were performed in one-atmosphere gas-mixing furnaces at an oxygen fugacity slightly below iron-wustite, and precooling crystallization, cooling history, and melt history were systematically varied. When cooled from a complete liquid, the experimental charges were porphyritic with 1-2 mm phenocrysts set in a very fine-grained matrix (less than 0.1 mm). This result suggests that 14310 did not cool from a complete melt. When cooled from a crystal-liquid mixture, the experimental charges had widely varying textures depending on the density and distribution of crystals that act as nucleation sites. It is suggested that the close spatial association of widely divergent textures in the matrices of some breccias and rocks might arise in this manner; local variations in cooling rates are not required.

Lofgren, G. E.↗
NASA NTRS1978

Adhesive bonding of ion beam textured metals and fluoropolymers

An electron bombardment argon ion source was used to ion etch various metals and fluoropolymers. The metal and fluoropolymers were exposed to (0.5 to 1.0) keV Ar ions at ion current densities of (0.2 to 1.5) mA/sq cm for various exposure times. The resulting surface texture is in the form of needles or spires whose vertical dimensions may range from tenths to hundreds of micrometers, depending on the selection of beam energy, ion current density, and etch time. The bonding of textured surfaces is accomplished by ion beam texturing mating pieces of either metals or fluoropolymers and applying a bonding agent which wets in and around the microscopic cone-like structures. After bonding, both tensile and shear strength measurements were made on the samples. Also tested, for comparison's sake, were untextured and chemically etched fluoropolymers. The results of these measurements are presented.

Mirtich, M. J.↗
NASA NTRS1978

Adhesive bonding of ion beam textured metals and fluoropolymers

An electron-bombardment argon ion source was used to ion-etch various metals and fluoropolymers. The metal and fluoropolymers were exposed to (0.5 to 1.0)-keV Ar ions at ion current densities of 0.2 to 1.5 mA/sq cm for various exposure times. The resulting surface texture is in the form of needles or spires whose vertical dimensions may range from tenths to hundreds of micrometers, depending on the selection of beam energy, ion current density, and etch time. The bonding of textured surfaces is accomplished by ion-beam texturing mating pieces of either metals or fluoropolymers and applying a bonding agent which wets in and around the microscopic conelike structures. After bonding, both tensile and shear strength measurements were made on the samples. Also tested, for comparison's sake, were untextured and chemically etched fluoropolymers. The results of these measurements are presented in this paper.

Mirtich, M. J.↗
NASA NTRS1978

Nucleation and growth of plagioclase and the development of textures in a high-alumina basaltic melt

Detailed experiments on the nucleation and growth of plagioclase from an igneous melt are carried out to characterize the magma prior to cooling. It is shown that the nature of the melt directly preceding cooling has a strong effect on texture development, regardless of the origin of the melt. The number, size, and shape of the crystals present in a melt upon extrusion can have a drastic effect on the final textures present in the resulting rocks. Conditions necessary for the formation of poikilitic, intersertal, and porphyritic textures in basaltic rocks are defined.

Nabelek, P. I.↗
NASA NTRS1979

Automated Array Assembly Task In-depth Study of Silicon Wafer Surface Texturizing

Several aspects of silicon wafer surface texturizing were studied. A low cost cleaning method that utilizes recycled Freon in an ultrasonic vapor degreaser to remove organic and inorganic contaminants from the surface of silicon wafers as received from silicon suppliers was investigated. The use of clean dry air and high throughout wafer batch drying techniques was shown to lower the cost of wafer drying. A two stage texturizing process was examined for suitability in large scale production. Also, an in-depth gettering study with the two stage texturizing process was performed for the enhancement of solar cell efficiency, minimization of current versus voltage curve dispersion, and improvement in process reproducibility. The 10% efficiency improvement goal was exceeded for the near term implementation of flat plate photovoltaic cost reduction.

Jones, G. T.↗
NASA NTRS1981

Ion beam texturing of heat transfer surfaces

Nucleate boiling heat transfer is examined as a means of energy conservation. Nucleate boiling curves were obtained for ion beam textured copper surfaces, untreated cooper surfaces, copper surfaces which had been polished and surfaces which had been coated with a plasma deposited polymer. Results show that texturing aids heat transfer while polishing has the opposite effect. The polymer coatings did not change nucleate boiling behavior. Aging effects were observed for untreated and for polished surfaces, while no such effects were noticed for textured surfaces. These data suggest that aging may be dependent on surface microgeometry, which is important in nucleate boiling heat transfer.

Agarwal, P. K.↗
NASA NTRS1981

Chondrules in H3 chondrites - Textures, compositions and origins

Compositional and textural variations among chondrules in unequilibrated (type 3) H-group chondrites are examined in order to determine possible relations between chondrule compositions and textures. Bulk compositions of polished thin sections of 90 individual chondrules and 16 compound chondrule sets from the Sharps, Tieschitz and Bremervorde chondrites were measured by broad-beam electron probe analyses; the chondrules were also classified petrographically as barred olivine, porphyritic olivine, porphyritic pyroxene, barred pyroxene, radiating pyroxene or fine-grained. The mean compositions of each type are found to be distinct as verified by discriminant analysis, despite a large scatter, with the olivine-rich chondrules characterized by low SiO2 and high FeO and MgO contents, greater concentrations of TiO2, Al2O3, Na2O and K2O, and lower Cr2O3 and MnO relative to pyroxene-rich chondrules. Data suggest that composition, together with cooling rate, has played a conspicuous role in producing observed chrondrule textures, and are consistent with chondrule formation from mixtures of differing fractions of high-, intermediate- and low-temperature nebular condensates that underwent melting in space.

Lux, G.↗
NASA NTRS1981

Textural features for radar image analysis

Texture is seen as an important spatial feature useful for identifying objects or regions of interest in an image. While textural features have been widely used in analyzing a variety of photographic images, they have not been used in processing radar images. A procedure for extracting a set of textural features for characterizing small areas in radar images is presented, and it is shown that these features can be used in classifying segments of radar images corresponding to different geological formations.

Shanmugan, K. S.↗
NASA NTRS1981

Electron reflection and secondary emission characteristics of sputter-textured pyrolytic graphite surfaces

Measurements are presented of secondary electron emission and reflected primary electron characteristics of sputter-textured pyrolitic graphite surfaces with microstructures of various sizes and densities, made with an Auger cylindrical mirror analyzer in a high-vacuum chamber at pressures below 1.33 x 10 to the -7th N/sq m (10 to the -9th torr). A dense, tall, thin, spire-like microstructure, obtained at ion energies of 1000 eV and ion current densities of 5 mA/sq cm, is the most effective. The secondary electron emission from such a surface is lower than that of soot, whose secondary emission is among the lowest of any material. At a primary electron energy of 1000 eV, the secondary electron emission yield of smooth CU is about 350% greater than the lowest value obtained for sputter-textured pyrolitic graphite. The reflected primary electron index of smooth Cu is a factor of 80 greater. If the secondary electron emission yield is reduced to 0.3, which is possible with sputter-textured pyrolitic graphite, the traveling wave tube collector efficiency could be improved by as much as 4% over that for smooth copper.

Wintucky, E. G.↗
NASA NTRS1981

A multi-frequency measurement of thermal microwave emission from soils: The effects of soil texture and surface roughness

An experiment on remote sensing of soil moisture content was conducted over bare fields with microwave radiometers at the frequencies of 1.4 GHz, 5 GHz, and 10.7 GHz during July - September of 1981. Three bare fields with different surface roughnesses and soil textures were prepared for the experiment. Ground truth acquisition of soil temperatures and moisture contents for 5 layers down to the depths of 15 cm was made concurrently with radiometric measurements. The experimental results show that the effect of surface roughness is to increase the soils' brightness temperature and to reduce the slope of regression between brightness temperature and moisture content. The slopes of regression for soils with different textures are found to be comparable, and the effect of soil texture is reflected in the difference of regression line intercepts at brightness temperature axis. The result is consistent with laboratory measurement of soils' dielectric permittivity. Measurements on wet smooth bare fields give lower brightness temperatures at 5 GHz than at 1.4 GHz.

Wang, J. R.↗