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DOE OSTI2026

Boron-Based Neutron Scintillator Screen Characterization with X-Rays and Neutrons

Recent work on boron-based neutron scintillator screens suggests these screens can offer superior performance when compared to commonly used screens. Borated neutron scintillator screens perform well in terms of light output (5-6 times greater than a standard Gadox screen) and detection effi-ciency (larger than standard LiF+ZnS screens). However, previously manu-factured boron-based screens have exhibited non-uniform surface coating and a poor mixture between phosphor and converter particles. The objective of this work was to evaluate newly fabricated scintillator screens to deter-mine if enhanced fabrication methods produced a more homogeneous distribution between neutron converter and scintillation phosphor particles. Uniformity of scintillator material deposition was also inspected. This new iteration of screens appeared more uniform than previous generations with the new coating method improving surface chemistry and scintillator material homogeneity. Additionally, a new methodology for screen characterization, involving the correlation of a neutron image taken with a borated scintillator screen to X-ray computed tomography of that same screen, was demonstrated to elucidate a relationship between scintillator screen thickness and relative light output of the screen under neutron exposure. This method suggested that the ideal thickness of scintillator material was ~150 µm to maximize light output of the screen.

36 - MATERIALS SCIENCE↗

NASA NTRS1981

Unusual weathering products of oldhamite parentage in the Norton County enstatite achondrite

Oldhamite, CaS, is found only in enstatite chondrites and enstatite achondrites. During the course of a comprehensive study of Norton County, oldhamite was found in several polished thin sections of enstatite achondrite. Inspection of thousands of specimens of Norton County showed that occasionally white, pale-yellow and brown specks, generally a few millimeters in size, occur on their surfaces. X-ray powder analysis of these materials shows that they contain portlandite, Ca(OH)2, vaterite (CaCO3, hexagonal), calcite (CaCO3, trigonal), bassanite (CaSO4 1/2 H2O) and one unknown species. It is suggested that these minerals were produced by terrestrial weathering of oldhamite.

Okada, A.↗

NASA NTRS1985

X-ray determination of parts alignment

A method for determining the alignment of adjoining metal objects is provided. The method comprises producing an X-ray image of adjoining surfaces of the two metal objects. The X-ray beam is tangential to the point the surfaces are joined. The method is particularly applicable where the alignment of the two metal objects is not readily susceptible to visual inspection.

Nelson, C. W.↗

NASA NTRS1993

Scanning electron microscope/energy dispersive x ray analysis of impact residues in LDEF tray clamps

Detailed optical scanning of tray clamps is being conducted in the Facility for the Optical Inspection of Large Surfaces at JSC to locate and document impacts as small as 40 microns in diameter. Residues from selected impacts are then being characterized by Scanning Electron Microscopy/Energy Dispersive X-ray Analysis at CNES. Results from this analysis will be the initial step to classifying projectile residues into specific sources.

Bernhard, Ronald P.↗

DOE OSTI2025

Non-destructive evaluation and machine learning methods for inspection of spent nuclear fuel canisters: A state-of-the-art review

Nuclear energy is among the cleanest and most efficient energy sources currently available. The operation of nuclear power plants (NPPs) produces large amounts of high-level radioactive waste known as spent nuclear fuel (SNF). Currently, large amounts of SNF is stored in dry cask storage systems (DCSSs) for extended interim storage until a permanent disposal solution becomes available. During the extended interim storage, the DCSS, particularly the SNF canisters, may degrade and abnormal conditions may occur. Therefore, non-destructive evaluation (NDE) and machine learning (ML) approaches are necessary for inspection of SNF canisters. This paper presents a state-of-the-art review of literature by summarizing recent progress made on the applications of NDE and ML for inspection of SNF canisters. Sixteen NDE methods are examined and compared: visual inspection, ultrasonic guided waves (UGWs), laser-based approaches, acoustic emission (AE), eddy current testing (ECT), non-invasive acoustic sensing, dynamic modal testing, cosmic ray muons tomography, neutron imaging, gamma rays detection, fiber optical sensors, through-wall communications, X-ray computed tomography (CT), vibrothermography, monoenergetic photon sources, and surface acoustic wave (SAW) sensors. The technology readiness level (TRL) for each method is assessed and compared. Recent publications on ML-enhanced visual inspection, AE, non-invasive acoustic sensing, dynamic modal testing, and neutron imaging for SNF canisters are summarized and future research needs are identified. In conclusion, this review article provides a convenient reference on the state-of-the-art applications of NDE and ML methods for inspection of SNF canisters.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

NASA NTRS1991

X-Ray Imaging System

The Model 60007A InnerView Real-time X-ray Imaging System, produced by National Imaging Systems, a division of FlouroScan Imaging Systems, Inc. (formerly HealthMate, Inc.), Northbrook, IL, is a third generation spinoff from x-ray astronomy technology. Goddard Space Flight Center developed the original technology into the Lixiscope, a small, portable, minimal radiation x-ray instrument that could be used at the scene of an accident. FlouroScan Imaging Systems, Inc., adapted this technology to develop the FlouroScan, a low-intensity, x-ray system that could be used without the lead aprons, film badges and lead-lined walls that conventional systems require. The InnerView is a spinoff of non-destructive testing and product inspection.

Source record↗

NASA NTRS1981

Thunderstorm hazards flight research: Storm hazards 1980 overview

A highly instrumented NASA F-106B aircraft, modified for the storm hazards mission and protected against direct lightning strikes, was used in conjunction with various ground based radar and lightning measurement systems to collect data during thunderstorm penetration flights. During 69 thunderstorm penetrations, there were 10 direct lightning strikes to the aircraft. No problems were encountered with any of the aircraft's systems as a result of the strikes and the research instrumentation performed as designed. Electromagnetic characteristics of nine strikes were recorded, and the results of other experiments confirm the theory that X-ray radiation and nitrous oxide gas are being produced by processes associated directly with thunderstorm electric fields and lightning discharges. A better understanding of aircraft lightning attachment mechanisms and strike zones is being accomplished by careful inspection, identification, and documentation of lightning attachment points and swept stroke paths following each strike to the aircraft.

Deal, P. L.↗

NASA NTRS1969

Apollo 6, Anomaly Report No. 6: Abnormal Structural Performance During Launch Phase

Approximately 2 minutes 13 seconds after lift-off of the Apollo 6 mission, abrupt changes of strain, vibration, and acceleration measurements were indicated in the S-IVB, instrument unit, adapter, lunar module, and command and service modules; photographs showed objects coming from the area of the adapter. The adapter, however, continued to sustain the required loads with no impairment of the mission. The investigation was first focused upon the understanding of the coupled vibration modes and characteristics of the launch vehicle and spacecraft.' Extensive test programs were conducted. It was eventually concluded that the adapter failure was not caused by vibration. Extensive study of the airborne photography and other evidence indicated that a large area of the adapter had lost inner facesheet from the honeycomb sandwich panels. Loads and stresses resulting from vibration were determined to be insufficient to initiate such a failure. The investigation was then directed toward determining the range of pressures that could have been trapped in the Apollo 6 adapter sandwich panels, and toward determining the tolerance of the panels to withstand pressure with various degrees of flaws such as adhesive voids and facesheet dents. The degradation effects of moisture and heat exposure on the adhesive strength were also studied and tested. These tests and analyses led to the conclusion that pressure internal to the sandwich panels could have caused the failure, if a large flaw existed. The pressure buildup would have been caused by aerodynamic heating effects on air and moisture trapped in the panel. The probable cause of the failure was found in the original ultrasonic inspection scan record of the affected adapter panel. In the center of the region where the adapter failed, horizontally along the station 709 panel splice, the record contained two thick anomalous lines extending several feet. Without an X-ray record of this region, the significance of this particular scan record cannot be fully understood. However, since all other evidence had indicated that the adhesive had to be weakened in a rather large area to initiate the failure, the investigation was focused intently upon the station 709 splices of other adapters. Sufficient information was developed to verify that deficient assembly techniques have consistently resulted in abnormalities in the structure at this station. These abnormalities were identified in adapters 12, 13, 14, 15, and 16. Before the splice abnormalities were pinpointed, corrective action was taken to reduce pressure "buildup in the honeycomb panels and to reduce heat degrading effects on the adhesive. This was done by drilling vent holes in the inner facesheet and covering the outer facesheet with cork. The adapters having identified abnormalities in the station 709 splice are being repaired, and the contractor is investigating ways of avoiding these -abnormalities in panels yet to be bonded.

Source record↗

NASA NTRS1973

The influence of nondestructive inspection parameters on the preproof and postproof fatigue crack detection limits for fracture mechanics applications

The results of a preliminary NDI program to examine the variability of flaw size detection limits in terms of specimen thickness and NDI procedures is reviewed and reanalyzed in terms of the variables involved. Penetrant, X-ray, eddy current, and ultrasonic methods developed independently at three separate laboratories were used to examine specimens having a range of thickness. The results are discussed in terms of the variables of thickness and NDI procedures.

Pettit, D. E.↗

NASA NTRS1993

Multilayer X-ray mirrors - Interfacial roughness, scattering, and image quality

Scattering of the multilayer coatings used for our normal incidence soft X-ray telescope at a wavelength of 63.5 A has been measured at 1.54 A and grazing angles of incidence and at soft X-rays near normal incidence. Furthermore, the edge of the moon is used as a known test target to estimate the amount of scattering in the arcsec range from images obtained on the date of the solar eclipse on July 11, 1991. The internal surfaces of the coating are inspected by high-resolution electron microscopy. A theoretical model describing the evolution and replication of roughness from layer to layer throughout the structure, which is in agreement with all experimental data, is presented. We find that practically all roughness caused by the growth of the multilayer structure occurs at spatial frequencies which are too high to produce scattering. The substrate roughness is replicated at lower spatial frequencies which might produce scattering within the field of view of an instrument. However, roughness in this range is below the 0.5 A level, again resulting in insignificant amounts of scatter.

Spiller, Eberhard↗

NASA NTRS1984

Eddy-Current Inspection of Narrow Metal Tubes

Inspection technique for narrow-bore metal tubing involves use of small internal eddy-current probe. Probe consists of thin copper wire wrapped on bobbin. Probe small enough to pass through bends in tube being measured. Technique useful for strain measurements where operating conditions or inaccessibility prevent use of such conventional methods as X-ray diffraction, electrical-resistance measurements, strain gages, or holography.

Ambrose, H. H.↗

NASA NTRS1974

Line absorption studies of the interstellar gas near 1 million GHz

The Copernicus satellite now opens up the ultraviolet region for inspection, and the number of resonance lines which may be studied has increased from 6, seen in the visible, to more than 30. The distribution and properties of an important constituent of the interstellar gas, molecular hydrogen, can be studied in detail using this instrument. A more comprehensive picture may now be developed for element depletion factors, electron densities, and sources of ionization (UV photons, low energy cosmic and X-rays).

Jenkins, E. B.↗

NASA NTRS1973

Detection of lack of fusion using opaque additives

Reliable nondestructive inspection for incomplete weldment penetration and rapid oxidation of aluminum surfaces when exposed to the atmosphere are currently two major problems in welded aluminum spacecraft structure. Incomplete-penetration defects are extremely difficult to detect and can lead to catastrophic failure of the structure. The moisture absorbed by aluminum oxide on the surface can cause weldment porosity if the surface is not cleaned before welding. The approach employed in this program to solve both problems was to employ copper as a coating to prevent oxidation of the aluminum. Also, copper was used as an opaque additive in the weldment to enhance X-ray detection in the event of incomplete penetration.

Cook, J. L.↗

DOE OSTI2025

Characterizing the pore-scale impacts of enhanced-solubilization solutions on organic-liquid morphology and fluid-fluid interfacial area with microtomography

Synchrotron X-ray microtomography was used to directly quantify the impact of enhanced-solubilization solutions on mobilization of a non-wetting fluid in a natural porous medium. Polyoxyethylene sorbitan monooleate (tween 80), hydroxypropyl-β-cyclodextrin (HPCD), sodium dodecyl sulfate (SDS), and ethanol were used as the solubilization reagents. Tetrachloroethene (PCE) was used as the entrapped organic immiscible liquid. Microtomography images were collected prior to and after successive floods with each reagent solution. The total trapping number was varied by more than three orders of magnitude by changing the velocity and viscosity of the aqueous phase as well as the interfacial tension between fluid phases. The results were compared to those obtained from equivalent experiments conducted with water flooding. Inspection of images indicated that mobilization caused a change in PCE morphology and distribution for all reagents with the exception of HPCD, for which a lower trapping number was determined compared to the other experiments. Mobilization of organic liquid was observed at total trapping numbers that were consistent with prior work. The enhanced-solubilization solutions had minimal impact on the configuration or magnitude of fluid-fluid interfacial area.

Interfacial area↗

NASA NTRS1975

Early detection of fatigue damage in composite materials

Early detection of fatigue damage in composite materials by nondestructive inspection (NDI) techniques has been demonstrated for glass/epoxy, graphite/glass/epoxy, and graphite/epoxy composites. Modulus and temperature were monitored and a correlation between them observed. Axial modulus and torsional modulus changes were a function of the laminate orientation. Torsional modulus measurements and coin tap tests were performed at 0, 1 million, 5 million, and 10 million cycles, on axial fatigue specimens. Three distinct regions were noted. In the primary region a small but rapid change in stiffness was noted in the first few thousand cycles. This was followed by a secondary region of little or no stiffness change. The tertiary region was characterized by an increasing rate of stiffness change leading to fracture. NDI procedures including holographic interferometry, ultrasonics, penetrant, and X-ray radiography were evaluated for fatigue damage detection.

Salkind, M. J.↗

NASA NTRS1993

Multicolor photometry of x ray selected Abell clusters

Strong evidence of evolution in cluster of galaxies at relatively low redshift has been indicated by recent x-ray studies. We are conducting a comprehensive optical study of a sample of Abell clusters that are strong x-ray emitters in order to test the x-ray evolution scenarios that have been proposed. The initial observations consist of three-color (B, R, I) imaging of low-redshift (0.025 less than z less than 0.25) Abell clusters using the T2KA CCD on the 0.9m telescope at KPNO the large field (23 ft. x 23 ft., approx. 1 Mpc at z = 0.025 and approx. 7 Mpc at z = 0.25) gives the unprecedented ability to sample most of the extent of the field of low-redshift clusters using a CCD. Given the advantages of CCDs over photographic plates, we expect to improve on many of the previous studies. A list of x-ray selected cluster of galaxies provides a homogeneous sample of true clusters that cannot be mistaken from apparent over-densities due to projection effects of field galaxies. Some optical indicators of cluster evolution are the population of ratios of cluster galaxies and their spatial distribution, a regular spiral-poor cluster is expected to be more evolved than an irregular spiral-rich cluster. Also regular spiral-poor clusters present high central concentrations while irregular spiral-rich are less concentrated. Variations in the Luminosity Function (LF) can indicate evolution. But in order to build reliable LFs it is necessary to determine the Hubble types of the cluster galaxies. In the past the classifications of cluster galaxies have been done by visual inspection on photographic material, this technique is very limited and can lead to errors when the galaxies are faint. The Hubble types of cluster galaxies can be determined in an objective manner by comparing colors and profiles from surface photometry. To show that this approach is feasible, I have presented preliminary results from the photometric analysis of the Abell-cluster A1213. Colors and profiles of the surface brightness distribution were compared to determine the Hubble types of the cluster galaxies.

Lopez-Cruz, Omar↗

NASA NTRS2026

Thermal Inspection for the Assessment of Adhesively Bonded Metal Adherends

Certification of adhesively bonded structures is currently a challenge for aircraft manufacturers. The ability to certify bonds in primary structure can reduce dependence on fasteners and this will enable more efficient manufacturing. For example, drilling holes and installing fasteners in bonded joints can be a potentially significant bottleneck in airframe manufacturing. In addition, fasteners increase the airframe weight and can add stress concentration areas. Reducing fastener count can accelerate manufacturing and improve aircraft performance. NASA is currently investigating nondestructive evaluation (NDE) techniques to assess bond integrity. For example, bond thickness influences bond strength and therefore NDE techniques are being investigated to determine bond thickness. For bonded metal structures, there is a large difference in the thermal diffusivity between the 7075 aluminum alloy metal adherends and aircraft grade adhesive. Multi-layered thermal models show a large variation in the thermal response for bondline adhesive thicknesses that vary from 100 to 300 microns for adherend thicknesses of 0.163 cm. Experimental through-transmission thermal measurements reveal promise to quantitatively characterize the bondline thickness. Results were validated with X-ray computed tomography and optical microscopy measurements, and influence of porosity on the thermal model and measurements are investigated.

X-ray computed tomography↗

NASA NTRS2026

Thermal Inspection for the Assessment of Adhesively Bonded Metal Adherents

bondline thickness↗