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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 109 records · Page 6
All sourcesNASA NTRSDOE OSTI
NASA NTRS2024

Development of Cryogenic Phase Change Materials for Lunar Sample Return

One of the scientific goals of NASA’s Artemis missions is to return regolith samples from the lunar surface. To maintain scientific integrity of these samples, including any volatiles that may exist, cryogenic stowage is desired. FROSTE (Frozen Return Of Samples To Earth) is the element of the Moon to Mars architecture that is tasked with developing and advancing concepts related to this goal. Both active and passive solutions are being considered, but active solutions (cryo-coolers) have high mass and cost penalties. Phase change materials (PCMs) are commonly used as passive thermal management solutions, particularly for sensitive scientific samples. However, there are currently no PCMs capable of providing cooling at the cryogenic temperatures needed to enable lunar sample return with volatiles intact (<120 K). FROSTE has identified two possible candidate materials that could fill this gap. Testing is required to verify the thermal performance of these materials, as well as gain experience with their handling characteristics. We are conducting this testing at the Marshall Space Flight Center’s Space Environmental Effects laboratory, in vacuum, with liquid nitrogen providing cooling ability below the freezing point of the materials. In this talk, we will present an overview of the FROSTE program element and share results from the initial development testing of two cryogenic phase change materials.

phase change material↗
NASA NTRS1998

Cryogenic Magnetostrictive Actuators: Materials and Applications

Magnetostrictive actuators based on TbDy alloys show promise for use as actuators on cryogenic devices. They can be made to deliver large forces and useful displacements below liquid nitrogen temperatures, with many advantages over piezoelectric actuators or motion feedthroughs from higher temperature actuators.

Magnetostrictive↗
DOE OSTI2023

Ultra low noise materials and devices for cryogenic superconductors and quantum bits

Materials, products, methods of use and fabrication thereof are disclosed. The materials are particularly well suited for application in products such as superconducting devices and quantum computing, due to ability to avoid undesirable effects from inherent noise and decoherence. The materials are formed from select isotopes having zero nuclear spin into a single crystal-phase film or layer of thickness depending on the desired application of the resulting device. The film/layer may be suspended or disposed on a substrate. The isotopes may be enriched from naturally-occurring sources of isotopically mixed elemental material(s). The single crystal is preferably essentially devoid of structural defects such as grain boundaries, inclusions, impurities and lattice vacancies.

Pereverzev, Sergey↗
NASA NTRS2018

Experimental Thermal Performance Testing of Cryogenic Tank Systems and Materials

A comparative study was conducted to collect and analyze thermal conductivity data on a wide variety of low density materials, as well as thermal performance data on a number of vacuum-jacketed cryogenic tank systems. Although a vast number of these types of materials and cryogenic tank systems exist, the thermal conductivity of insulation materials and the thermal performance of cryogenic tank systems is often difficult to compare because many industrial methods and experimental conditions are available and utilized. The availability of a new thermal conductivity measurement device, the Macroflash Cup Cryostat, which is applicable for assessing a variety of materials, is accessible at NASA's Cryogenic Test Laboratory (CTL) at the Kennedy Space Center (KSC). The convenience of this device has resulted in the ability to rapidly measure the thermal conductivity properties of these materials by using a flat-plate liquid nitrogen (LN2) boiloff technique that employs a guarded heat flow test methodology in order to determine the effective thermal conductivity (ke) of a test specimen. As the thermal conductivities are measured at cryogenic temperatures, materials suitable for both future space missions and cryogenic tank systems can be identified and experimentally analyzed. Also recognizable are materials which may help increase energy efficiency by limiting the thermal losses encountered under various environmental conditions. The overall focus of this work consisted of two parts. One part, was to produce and analyze thermal conductivity data on a wide variety of materials with suitable properties conducive to those needed to aid in the production of a calibration curve for the "low end" of the Macroflash instrument. (Low end meaning materials with a thermal conductivity rating below 100 milliwatts per meter-Kelvin). The second part was to collect and analyze heat transfer data for a variety of small vacuum-jacketed vessels (cryogenic tank systems) in order to compare the thermal performance between them.

Myers, Wesley C.↗
NASA NTRS2003

Material Damping Experiments at Cryogenic Temperatures

A unique experimental facility has been designed to measure damping of materials at cryogenic temperatures. The test facility pays special attention to removing other sources of damping in the measurement by avoiding frictional interfaces, decoupling the test specimen from the support system, and by using a non-contacting measurement device; Damping data is obtained for materials (AI, GrEp, Be, Fused Quartz), strain amplitudes (less than 10-6 ppm), frequencies (20Hz-330Hz) and temperatures (20K-293K) relevant to future precision optical space missions. The test data shows a significant decrease in viscous damping at cryogenic temperatures and can be as low as 10-4%, but the amount of the damping decrease is a function of frequency and material. Contrary to the other materials whose damping monotonically decreased with temperature, damping of Fused Quartz increased substantially at cryo, after reaching a minimum at around l50 K. The damping is also shown to be insensitive to strain for low strain levels. At room temperatures, the test data correlates well to the analytical predictions of the Zener damping model. Discrepancies at cryogenic temperatures between the model predictions and the test data are observed.

cryogenic↗
NASA NTRS1981

Thallous halide materials for use in cryogenic applications

Thallous halides, either alone or in combination with other ceramic materials, are used in cryogenic applications such as heat exchange material for the regenerator section of a closed-cycle cryogenic refrigeration section, as stabilizing coatings for superconducting wires, and as dielectric insulating materials. The thallous halides possess unusually large specific heats at low temperatures, have large thermal conductivities, are nonmagnetic, and are nonconductors of electricity. They can be formed into a variety of shapes such as spheres, bars, rods, or the like and can be coated onto substrates.

Lawless, William N.↗
DOE OSTI2023

Rapid Cryogenic Electrical Characterization of Materials and Devices Using Gifford-McMahon Cryocoolers

Thin-film heterostructures are necessary building blocks for superconducting and phononic quantum computing devices. Many new generations of quantum hardware demand extensive materials research to optimize performances at cryogenic temperatures (below 10 K). Here, we demonstrate compact cryogenic measurement systems capable of reaching sub-10K temperatures in less than three hours with the ability to measure AC/DC resistance and dielectric properties of thin-film materials. Our platform utilizes Gifford-McMahon (GM) cryocoolers as effective tools for providing high throughput cooling-warming cycles. We successfully used the GM-based measurement systems to measure 1) the superconducting transition temperature for Nb thin films (T c ~7.8 K), and 2) the temperature dependence of the dielectric constant in SiO 2 thin films down to 10 K. The fast electrical characterization feedback will be critical in developing robust materials and components for cryogenic computing devices.

36 MATERIALS SCIENCE↗
NASA NTRSDate not supplied

Development of an Apparatus and Process for Precision Measurement of Cryogenic Thermal Expansion of Materials

NASA frequently needs thermal contraction data for materials to be used in cryogenic space flight missions. To satisfy this need, we developed an apparatus and a high-precision technique for performing such measurements using a commercial fiber-optic-based position sensor. We describe the measurement process and its verification using a copper sample. We also present data for two materials which we characterized for potential NASA use.

Cryogenic↗
NASA NTRS2008

Using Composite Materials in a Cryogenic Pump

Several modifications have been made to the design and operation of an extended-shaft cryogenic pump to increase the efficiency of pumping. In general, the efficiency of pumping a cryogenic fluid is limited by thermal losses which is itself caused by pump inefficiency and leakage of heat through the pump structure. A typical cryogenic pump includes a drive shaft and two main concentric static components (an outer pressure containment tube and an intermediate static support tube) made from stainless steel. The modifications made include replacement of the stainless-steel drive shaft and the concentric static stainless-steel components with components made of a glass/epoxy composite. The leakage of heat is thus reduced because the thermal conductivity of the composite is an order of magnitude below that of stainless steel. Taking advantage of the margin afforded by the decrease in thermal conductivity, the drive shaft could be shortened to increase its effective stiffness, thereby increasing the rotordynamic critical speeds, thereby further making it possible to operate the pump at a higher speed to increase pumping efficiency. During the modification effort, an analysis revealed that substitution of the shorter glass/epoxy shaft for the longer stainless-steel shaft was not, by itself, sufficient to satisfy the rotordynamic requirements at the desired increased speed. Hence, it became necessary to increase the stiffness of the composite shaft. This stiffening was accomplished by means of a carbon-fiber-composite overwrap along most of the length of the shaft. Concomitantly with the modifications described thus far, it was necessary to provide for joining the composite-material components with metallic components required by different aspects of the pump design. An adhesive material formulated specially to bond the composite and metal components was chosen as a means to satisfy these requirements.

Batton, William D.↗
NASA NTRS1973

Effects of environmental exposure on cryogenic thermal insulation materials

Investigation was made to optimize selection of insulation materials for reusable space vehicles which will be repeatedly operated over periods of up to ten years. Results of study are summarized in two reports. Volume I describes tests and significant findings. In Volume II, extensive test data obtained are organized in handbook form.

Parmley, R. T.↗
NASA NTRS1992

Development of magnetostrictive active members for control of space structures

The goal of this Phase 2 Small Business Innovative Research (SBIR) project was to determine the technical feasibility of developing magnetostrictive active members for use as truss elements in space structures. Active members control elastic vibrations of truss-based space structures and integrate the functions of truss structure element, actively controlled actuator, and sensor. The active members must control structural motion to the sub-micron level and, for many proposed space applications, work at cryogenic temperatures. Under this program both room temperature and cryogenic temperature magnetostrictive active members were designed, fabricated, and tested. The results of these performance tests indicated that room temperature magnetostrictive actuators feature higher strain, stiffness, and force capability with lower amplifier requirements than similarly sized piezoelectric or electrostrictive active members, at the cost of higher mass. Two different cryogenic temperature magnetostrictive materials were tested at liquid nitrogen temperatures, both with larger strain capability than the room temperature magnetostrictive materials. The cryogenic active member development included the design and fabrication of a cryostat that allows operation of the cryogenic active member in a space structure testbed.

Johnson, Bruce G.↗
NASA NTRS2009

Cryogenic Chamber for Servo-Hydraulic Materials Testing

A compact cryogenic test chamber can be cooled to approximately 5 to 6 Kelvin for materials testing. The system includes a temperature controller and multiple sensors to measure specimen temperature at different locations. The testing chamber provides a fast and easy method to perform materials testing at lower than liquid nitrogen temperature (77 K). The purpose of the chamber is to cool a composite lap shear specimen to approximately 20 K so that tensile test force and displacement data may be acquired at this cryogenic temperature range.

Francis, John J.↗