INVESTIGATION OF COMBINED EFFECTS OF RADIATION AND VACUUM AND OF RADIATION AND CRYOGENIC TEMPERATURES ON ENGINEERING MATERIALS
Combined effects of radiation and vacuum, and of radiation and cryogenic temperature on engineering materials
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Combined effects of radiation and vacuum, and of radiation and cryogenic temperature on engineering materials
Expulsion bladders and materials for cryogenic liquids in tests involving 70 to 126 expulsion cycles
NASA frequently needs thermal contraction data for materials to be used in cryogenic space flight missions. To satisfy this need, we developed an apparatus and a high-precision technique for performing such measurements using a commercial fiber-optic-based position sensor. We describe the measurement process and its verification using a copper sample. We also present data for two materials which we characterized for potential NASA use.
Several modifications have been made to the design and operation of an extended-shaft cryogenic pump to increase the efficiency of pumping. In general, the efficiency of pumping a cryogenic fluid is limited by thermal losses which is itself caused by pump inefficiency and leakage of heat through the pump structure. A typical cryogenic pump includes a drive shaft and two main concentric static components (an outer pressure containment tube and an intermediate static support tube) made from stainless steel. The modifications made include replacement of the stainless-steel drive shaft and the concentric static stainless-steel components with components made of a glass/epoxy composite. The leakage of heat is thus reduced because the thermal conductivity of the composite is an order of magnitude below that of stainless steel. Taking advantage of the margin afforded by the decrease in thermal conductivity, the drive shaft could be shortened to increase its effective stiffness, thereby increasing the rotordynamic critical speeds, thereby further making it possible to operate the pump at a higher speed to increase pumping efficiency. During the modification effort, an analysis revealed that substitution of the shorter glass/epoxy shaft for the longer stainless-steel shaft was not, by itself, sufficient to satisfy the rotordynamic requirements at the desired increased speed. Hence, it became necessary to increase the stiffness of the composite shaft. This stiffening was accomplished by means of a carbon-fiber-composite overwrap along most of the length of the shaft. Concomitantly with the modifications described thus far, it was necessary to provide for joining the composite-material components with metallic components required by different aspects of the pump design. An adhesive material formulated specially to bond the composite and metal components was chosen as a means to satisfy these requirements.
Investigation was made to optimize selection of insulation materials for reusable space vehicles which will be repeatedly operated over periods of up to ten years. Results of study are summarized in two reports. Volume I describes tests and significant findings. In Volume II, extensive test data obtained are organized in handbook form.
The goal of this Phase 2 Small Business Innovative Research (SBIR) project was to determine the technical feasibility of developing magnetostrictive active members for use as truss elements in space structures. Active members control elastic vibrations of truss-based space structures and integrate the functions of truss structure element, actively controlled actuator, and sensor. The active members must control structural motion to the sub-micron level and, for many proposed space applications, work at cryogenic temperatures. Under this program both room temperature and cryogenic temperature magnetostrictive active members were designed, fabricated, and tested. The results of these performance tests indicated that room temperature magnetostrictive actuators feature higher strain, stiffness, and force capability with lower amplifier requirements than similarly sized piezoelectric or electrostrictive active members, at the cost of higher mass. Two different cryogenic temperature magnetostrictive materials were tested at liquid nitrogen temperatures, both with larger strain capability than the room temperature magnetostrictive materials. The cryogenic active member development included the design and fabrication of a cryostat that allows operation of the cryogenic active member in a space structure testbed.
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A compact cryogenic test chamber can be cooled to approximately 5 to 6 Kelvin for materials testing. The system includes a temperature controller and multiple sensors to measure specimen temperature at different locations. The testing chamber provides a fast and easy method to perform materials testing at lower than liquid nitrogen temperature (77 K). The purpose of the chamber is to cool a composite lap shear specimen to approximately 20 K so that tensile test force and displacement data may be acquired at this cryogenic temperature range.
Polymeric materials in expulsion bladders for cryogenic liquids, describing fabrication, flexibility, permeability, storage, transfer, control factors, etc
Ambient and cryogenic temperature mechanical properties and the ambient temperature stress corrosion properties of annealed, straightened, and centerless ground Nitronic 60 stainless steel alloy bar material are presented. The mechanical properties of longitudinal specimens were evaluated at test temperatures from ambient to liquid hydrogen. The tensile test data indicated increasing strength with decreasing temperature to -196 C. Below liquid nitrogen temperature the smooth tensile and notched tensile strengths decreased slightly while the elongation and reduction of area decreased drastically. The Charpy V-notched impact energy decreased steadily with decreasing test temperature. Stress corrosion tests were performed on longitudinal tensile specimens and transverse C-ring specimens exposed to: alternate immersion in a 3.5% NaCl bath; humidity cabinet; and a 5% salt spray atmosphere. The longitudinal tensile specimens experienced no corrosive attack. Approximately 3/4 of the transverse C-rings exposed to alternate immersion and to salt spray experienced a pitting attack on the top and bottom ends. Additional stress corrosion tests were performed on transverse tensile specimens. No failures occurred in the 90% stressed specimens exposed for 90 days in the alternate immersion and salt spray environments
Filler materials are used for surface flaws, instrumentation grooves, and fastener holes in wind tunnel models. More stringent surface quality requirements and the more demanding test environment encountered by cryogenic wind tunnels eliminate filler materials such as polyester resins, plaster, and waxes used on conventional wind tunnel models. To provide a material data base for cryogenic models, various filler materials are investigated. Surface quality requirements and test temperature extremes require matching of coefficients of thermal expansion or interfacing materials. Microstrain versus temperature curves are generated for several candidate filler materials for comparison with cryogenically acceptable materials. Matches have been achieved for aluminum alloys and austenitic steels. Simulated model surfaces are filled with candidate filler materials to determine finishing characteristics, adhesion and stability when subjected to cryogenic cycling. Filler material systems are identified which meet requirements for usage with aluminum model components.
The research testing and demonstration of new bulk-fill materials for cryogenic thermal insulation systems was performed by the Cryogenics Test Laboratory at NASA Kennedy Space Center. Thermal conductivity testing under actual-use cryogenic conditions is a key to understanding the total system performance encompassing engineering, economics, and materials factors. A number of bulk fill insulation materials, including aerogel beads, glass bubbles, and perlite powder, were tested using a new cylindrical cryostat. Boundary temperatures for the liquid nitrogen boil-off method were 293 K and 78 K. Tests were performed as a function of cold vacuum pressure from high vacuum to no vacuum conditions. Results are compared with other complementary test methods in the range of 300 K to 20 K. Various testing techniques are shown to be required to obtain a complete understanding of the operating performance of a material and to provide data for answers to design engineering questions.
Various filler materials are being investigated for applicability to cryogenic wind tunnel models. The filler materials will be used to fill surface grooves, holes and flaws. The severe test environment of cryogenic models precludes usage of filler materials used on conventional wind tunnel models. Coefficients of thermal expansion, finishing characteristics, adhesion and stability of several candidate filler materials were examined. Promising filler materials are identified.
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Spacecraft and instruments on space missions are built using a wide variety of carefully-chosen materials. It is common for NASA engineers to propose new candidate materials which have not been totally characterized at cryogenic temperatures. In many cases a material's cryogenic thermal conductivity must be known before selecting it for a specific space-flight application. We developed a test facility in 2004 at NASA's Goddard Space Flight Center to measure the longitudinal thermal conductivity of materials at temperatures between 4 and 300 Kelvin, and we have characterized many candidate materials since then. The measurement technique is not extremely complex, but proper care to details of the setup, data acquisition and data reduction is necessary for high precision and accuracy. We describe the thermal conductivity measurement process and present results for ten engineered materials, including alloys, polymers, composites, and a ceramic.
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Reinforced plastic laminate test techniques and methods to determine mechanical and thermal properties for structural applications at cryogenic temperatures
Dielectric properties of several materials measured under vacuum, reactor radiation and cryogenic conditions