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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 109 records · Page 6

In situ dynamic TEM characterization of unsteady crystallization during laser processing of amorphous germanium

The unsteady propagation mechanism for the crystallization of amorphous germanium (a-Ge) was studied with in situ movie-mode dynamic transmission electron microscopy (MM-DTEM). We used short laser pulses to heat sputter-deposited a-Ge films and the resulting crystallization process was imaged with up to 16 sequential 50 ns long electron pulses separated by a controlled delay that was varied between 0.5 and 5 μs. The unsteady crystallization in the radial, net-growth direction was observed to occur at a decreasing rate of ~1.5–0.2 m/s through a mechanism involving the formation of discrete ~1.1 μm wide bands that grew with velocities of 9–12 m/s perpendicular to the radial direction and along the perimeter of the crystallized area. The crystallization rate and resulting microstructure were consistent with a liquid-mediated growth mechanism, which suggests that locally the band front reaches the amorphous melting temperature of Ge. Furthermore, a mechanism based on the notion of a critical temperature is proposed to explain the unsteady, banded behavior.

36 MATERIALS SCIENCE↗

Autonomous Closed-Loop Experimental Characterization and Dynamic Model Validation of a Scaled Underwater Kite

This paper presents the closed-loop experimental framework and dynamic model validation for a 1/12-scale underwater kite design. The pool-based tow testing framework described herein, which involves a fully actuated, closed-loop controlled kite and flexible tether, significantly expands upon the capabilities of any previously developed open-source framework for experimental underwater kite characterization. Specifically, the framework has allowed for the validation of three closed-loop flight control strategies, along with a critical comparison between dynamic model predictions and experimental results. In this paper, we provide a detailed presentation of the experimental tow system and kite setup, describe the control algorithms implemented and tested, and quantify the level of agreement between our multi-degree-of-freedom kite dynamic model and experimental data. Finally, we also present a sensitivity analysis that helps to identify the most influential parameters to kite performance and further explain the remaining mismatches between the model and data.

42 ENGINEERING↗

Hydrothermal synthesis and characterization under dynamic conditions of cobalt oxide nanoparticles supported over magnesium oxide nano-plates

Here, a nano-catalyst comprised of oxidized Co NPs supported on MgO nano-plates was synthesized via a hydrothermal co-precipitation strategy and calcination in O 2 and subsequently in H 2 at 250 °C. Spectro-microscopy characterization was performed by scanning transmission electron microscopy, electron energy loss spectroscopy and scanning X-ray transmission microscopy. Surface measurements under H 2 and H 2 + CO atmospheres were obtained by ambient pressure X-ray photoelectron spectroscopy and in situ X-ray absorption spectroscopy in the 225–480 °C range. These measurements at the atomic and microscopic levels demonstrated that the oxidized Co nanoparticles uniformly decorated the MgO nano-plates. The surfaces are enriched with Co, and with a mixture of Co(OH) 2 and CoO under H 2 and H 2 + CO atmospheres. Under a H 2 atmosphere, the outermost surfaces were composed of (lattice) O 2- , CO 3 2- and OH - . No inorganic carbonates were observed in the bulk. Chemisorbed CO, likely on the oxidized Co surfaces, was observed at the expense of O 2- under 300 mTorr H 2 + CO (2:1) at 225 °C. Gas phase CO 2 was detected under 32 Torr H 2 + CO (2:1) at 225 °C upon prolonged reaction time, and was attributed to a surface chemical reaction between O 2- and chemisorbed CO. Furthermore, sp 3 like carbon species were detected on the otherwise carbon free surface in H 2 + CO, which remained on the surface under the subsequent reaction conditions. The formation of sp 3 like hydrocarbons was ascribed to a surface catalytic reaction between the chemisorbed CO and OH - as the apparent hydrogen source.

36 MATERIALS SCIENCE↗

Dynamic Crush Characterization of Ice

During the space shuttle return-to-flight preparations following the Columbia accident, finite element models were needed that could predict the threshold of critical damage to the orbiter's wing leading edge from ice debris impacts. Hence, an experimental program was initiated to provide crushing data from impacted ice for use in dynamic finite element material models. A high-speed drop tower was configured to capture force time histories of ice cylinders for impacts up to approximately 100 ft/s. At low velocity, the force-time history depended heavily on the internal crystalline structure of the ice. However, for velocities of 100 ft/s and above, the ice fractured on impact, behaved more like a fluid, and the subsequent force-time history curves were much less dependent on the internal crystalline structure.

Fasanella, Edwin L.↗

Photogrammetry and Videogrammetry Methods Development for Solar Sail Structures

This report discusses the development and application of metrology methods called photogrammetry and videogrammetry that make accurate measurements from photographs. These methods have been adapted for the static and dynamic characterization of gossamer structures, as four specific solar sail applications demonstrate. The applications prove that high-resolution, full-field, non-contact static measurements of solar sails using dot projection photogrammetry are possible as well as full-field, non-contact, dynamic characterization using dot projection videogrammetry. The accuracy of the measurement of the resonant frequencies and operating deflection shapes that were extracted surpassed expectations. While other non-contact measurement methods exist, they are not full-field and require significantly more time to take data.

Pappa, Richard S.↗

Characterization and dynamics of the peculiar stream Jhelum: A tentative role for the Sagittarius dwarf galaxy

Stellar streams are a promising tool to study the Milky Way’s dark matter subhalo population, as interactions with subhalos are expected to leave visible imprints in the streams in the form of substructure. However, there may be other causes of substructure. Here we studied the kinematics and the unusual morphology of the stellar stream Jhelum. Using a combination of ground-based photometry and Gaia EDR3 astrometry, we characterized the morphology of Jhelum. We combined this new data with radial velocities from the literature to perform orbit integrations of the stream in static Galactic potentials. We also carried out N-body simulations in the presence of the Sagittarius dwarf galaxy. The new data reveal a previously unreported tertiary component in the stream, as well as several gaps and a kink-like feature in its narrow component. We find that for a range of realistic Galactic potentials, no single orbit is able to reproduce Jhelum’s radial velocity data entirely. A generic property of the orbital solutions is that they share a similar orbital plane to Sagittarius and this leads to repeated encounters with the stream. Using N-body simulations that include a massive Sagittarius, we explored its effect on Jhelum, and we show that these encounters are able to qualitatively reproduce the narrow and broad components in Jhelum, as well as create a tertiary component in some cases. We also find evidence that such encounters can result in an apparent increase in the velocity dispersion of the stream by a factor up to four due to overlapping narrow and broad components. Our findings suggest that the Jhelum stream is even more complex than once thought; however, its morphology and kinematics can tentatively be explained via the interactions with Sagittarius. In this scenario, the formation of Jhelum’s narrow and broad components occurs naturally, yet some of the smaller gap-like features remain to be explained.

79 ASTRONOMY AND ASTROPHYSICS↗

L2 Milestone 5433: Characterization of Dynamic Behavior of AM and Conventionally Processed Stainless Steel (316L and 304L)

For additive manufacturing (AM) of metallic materials, the certification and qualification paradigm needs to evolve as there currently exists no broadly accepted “ASTM- or DIN-type” additive manufacturing certified process or AM-material produced specifications. Accordingly, design, manufacture, and thereafter implementation and insertion of AM materials to meet engineering applications requires detailed quantification of the constitutive (strength and damage) properties of these evolving materials, across the spectrum of metallic AM methods, in comparison/contrast to conventionally-manufactured metals and alloys. This report summarizes the 316L SS research results and presents initial results of the follow-on study of 304L SS. For the AM-316L SS investigation, cylindrical samples of 316L SS were produced using a LENS MR-7 laser additive manufacturing system from Optomec (Albuquerque, NM) equipped with a 1kW Yb-fiber laser. The microstructure of the AM-316L SS was characterized in both the “as-built” Additively Manufactured state and following a heat-treatment designed to obtain full recrystallization to facilitate comparison with annealed wrought 316L SS. The dynamic shock-loading-induced damage evolution and failure response of all three 316L SS materials was quantified using flyer-plate impact driven spallation experiments at peak stresses of 4.5 and 6.35 GPa. The results of these studies are reported in detail in the first section of the report. Publication of the 316L SS results in an archival journal is planned. Following on from the 316L SS completed work, initial results on a study of AM 304L SS are in progress and presented herein. Preliminary results on the structure/dynamic spallation property behavior of AM-304L SS fabricated using both the directed-energy LENS and an EOS powder-bed AM techniques in comparison to wrought 304L SS is detailed in this Level 2 Milestone report.

316L SS↗

Dragonfly: A Case Study in Dynamic Stability Characterization

Next decade, the Dragonfly probe will enter Titan’s atmosphere on a mission to explore and characterize its unique and complex organic chemistry. In contrast to Mars entry missions, where the challenge is to slow down in its tenuous atmosphere before impacting the surface, Titan’s thick atmosphere provides generous drag. However, Titan has its own unique EDL challenges. Among these challenges is the long time (on the order of 90 minutes!) the vehicle will need to descend unguided through flow regimes where blunt-body entry probes are known to be dynamically unstable. This elongated timeline, both prior to drogue parachute deployment, and during the ensuing descent, has the potential to allow adverse dynamic instability properties to produce large amplitude oscillations in angle-of-attack. This, in-turn may lead to non-compliance in vehicle attitude requirements for EDL events such as parachute deployment, and lander release, or in the most extreme case, tumbling of the aeroshell and near-assured loss of mission.

EDL↗

Dragonfly: A Case Study in Dynamic Stability Characterization

Next decade, the Dragonfly probe will enter Titan’s atmosphere on a mission to explore and characterize its unique and complex organic chemistry. In contrast to Mars entry missions, where the challenge is to slow down in its tenuous atmosphere before impacting the surface, Titan’s thick atmosphere provides generous drag. However, Titan has its own unique EDL challenges. Among these challenges is the long time (on the order of 90 minutes!) the vehicle will need to descend unguided through flow regimes where blunt-body entry probes are known to be dynamically unstable. This elongated timeline, both prior to drogue parachute deployment, and during the ensuing descent, has the potential to allow adverse dynamic instability properties to produce large amplitude oscillations in angle-of-attack. This, in-turn may lead to non-compliance in vehicle attitude requirements for EDL events such as parachute deployment, and lander release, or in the most extreme case, tumbling of the aeroshell and near-assured loss of mission.

EDL↗

Assessment and Improvement Proposals for High-Pressure Rinsing Processes during Cleanroom Preparation of Superconducting Radio-Frequency Cavities for Particle Accelerators

The goal of this internship is to develop a fluid dynamics characterization of the high-pressure flow used for cleaning the internal surface of the SRF cavities. Initially, the High Pressure Rinsing (HPR) process is introduced, focusing on the problems of the SRF cavities and how this method can be used to increase their acceleration efficiency and performance. The characterization of the problem is then presented, including an introduction to the multiphase flow modeling and the analysis of the Fermilab facility for the HPR. To accomplish the goal, a preliminary estimation of the variables was performed using MATLAB. Then, multiple 2D simulations were developed with Ansys Fluent, and the influence of the main parameter was investigated. The simulation results are then presented and analysed, with a focus on the possible future developments of the HPR process fluid dynamic characterization.

43 PARTICLE ACCELERATORS↗

Plasma viscosity with mass transport in spherical inertial confinement fusion implosion simulations

The effects of viscosity and small-scale atomic-level mixing on plasmas in inertial confinement fusion(ICF) currently represent challenges in ICF research. Many current ICF hydrodynamic codes ignore the effects of viscosity though recent research indicates viscosity and mixing by classical transport processes may have a substantial impact on implosion dynamics. In this paper, we have implemented a Lagrangian hydrodynamic code in one-dimensional spherical geometry with plasmaviscosity and mass transport and including a three temperature model for ions, electrons, and radiation treated in a gray radiation diffusion approximation. The code is used to study ICF implosion differences with and without plasmaviscosity and to determine the impacts of viscosity on temperature histories and neutron yield. It was found that plasmaviscosity has substantial impacts on ICF shock dynamics characterized by shock burn timing, maximum burn temperatures, convergence ratio, and time history of neutron production rates. Finally, plasmaviscosity reduces the need for artificial viscosity to maintain numerical stability in the Lagrangian formulation and also modifies the flux-limiting needed for electron thermal conduction.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Static and dynamic aeroelastic characterization of an aerodynamically heated generic hypersonic aircraft configuration

This work-in-progress presentation describes an ongoing research activity at the NASA Langley Research Center to develop analytical methods for the prediction of aerothermoelastic stability of hypersonic aircraft including active control systems. The objectives of this research include application of aerothermal loads to the structural finite element model, determination of the thermal effects on flutter, and assessment of active controls technology applied to overcome any potential adverse aeroelastic stability or response problems due to aerodynamic heating- namely flutter suppression and ride quality improvement. For this study, a generic hypersonic aircraft configuration was selected which incorporates wing flaps, ailerons and all-moveable fins to be used for active control purposes. The active control systems would use onboard sensors in a feedback loop through the aircraft flight control computers to move the surfaces for improved structural dynamic response as the aircraft encounters atmospheric turbulence.

Heeg, Jennifer↗

Overview of Dynamic Test Techniques for Flight Dynamics Research at NASA LaRC (Invited)

An overview of dynamic test techniques used at NASA Langley Research Center on scale models to obtain a comprehensive flight dynamics characterization of aerospace vehicles is presented. Dynamic test techniques have been used at Langley Research Center since the 1920s. This paper will provide a partial overview of the current techniques available at Langley Research Center. The paper will discuss the dynamic scaling necessary to address the often hard-to-achieve similitude requirements for these techniques. Dynamic test techniques are categorized as captive, wind tunnel single degree-of-freedom and free-flying, and outside free-flying. The test facilities, technique specifications, data reduction, issues and future work are presented for each technique. The battery of tests conducted using the Blended Wing Body aircraft serves to illustrate how the techniques, when used together, are capable of characterizing the flight dynamics of a vehicle over a large range of critical flight conditions.

Owens, D. Bruce↗

Electro-Thermal Characterization of Dynamical VO 2 Memristors via Local Activity Modeling

We report translating the surging interest in neuromorphic electronic components, such as those based on nonlinearities near Mott transitions, into large-scale commercial deployment faces steep challenges in the current lack of means to identify and design key material parameters. These issues are exemplified by the difficulties in connecting measurable material properties to device behavior via circuit element models. Here, the principle of local activity is used to build a model of VO 2 /SiN Mott threshold switches by sequentially accounting for constraints from a minimal set of quasistatic and dynamic electrical and high-spatial-resolution thermal data obtained via in situ thermoreflectance mapping. By combining independent data sets for devices with varying dimensions, the model is distilled to measurable material properties, and device scaling laws are established. The model can accurately predict electrical and thermal conductivities and capacitances and locally active dynamics (especially persistent spiking self-oscillations). The systematic procedure by which this model is developed has been a missing link in predictively connecting neuromorphic device behavior with their underlying material properties, and should enable rapid screening of material candidates before employing expensive manufacturing processes and testing procedures.

36 MATERIALS SCIENCE↗

Characterization of dynamic morphological changes of tin anode electrode during (de)lithiation processes using in operando synchrotron transmission X-ray microscopy

The morphological evolution of tin particles with different sizes during the first lithiation and delithiation processes has been visualized by an in operando synchrotron transmission X-ray microscope (TXM). Here, the in operando lithium ion battery cell was operated at constant current condition during TXM imaging. Two-dimensional projection images with 40 nm resolution showing morphological evolution were obtained and analyzed. The analysis of relative area change shows that the morphology of tin particles with different sizes changed simultaneously. This phenomenon is mainly because of a negative feedback mechanism among tin particles in the battery electrode at a constant current operating condition. For irregular-shaped tin particles, the contour analysis demonstrates that the regions with higher curvature started volume expansion first, and then the entire particle expanded almost homogeneously. This study provides insights for understanding the dynamic morphological change and the particle-particle interactions in high capacity lithium ion battery electrodes.

25 ENERGY STORAGE↗

Characterization of dynamics and decay in the St. Benedict Paul trap

The St. Benedict experiment includes a linear Paul trap designed to measure the beta-neutrino angular correlation coefficient 𝑎 𝛽ν of mixed superallowed 𝛽-decay transitions between mirror nuclei via coincidence detection of 𝛽-particles and recoiling ions. The emitted 𝛽 particle and daughter ion are detected with plastic scintillators and micro-channel plate detectors, respectively, allowing for accurate measurements of their time-of-flights. From the shape of the coincidence time-of-flight distribution, a value of 𝑎 𝛽ν can be determined. This manuscript presents detailed simulations of the St. Benedict Paul trap, with a focus on ion cloud dynamics and recoiling daughter trajectories.

Linear Paul trap↗