Thermoelectric modules built using ceramic legs grown by laser floating zone
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Ferreira, N. M.↗
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Modified floating-zone crystal growth of Mg 4 Ta 2 O 9 and its scintillation performance
Rods of single crystal MgTaO 9 were produced free of macroscopic defects and their scintillation properties including afterglow were measured. The compound characteristics make it a candidate for high energy X-ray radiography applications.
Yuan, Dongsheng↗
Recombination lifetimes in gamma-irradiated P-type float zone silicon
Electron decay rate and absorption cross sections for electron holes and recombination in gamma irradiated n-type silicon
Compton, W. D.↗
Floating zone process for drawing small diameter fibers of refractory materials
New process produces controlled purity, very high strength, single crystal fibers of materials with melting points to 4000 C. Process has been used to make single crystal fibers of highly refractory ceramics such as aluminum oxide, titanium carbide and yttrium oxide.
Westfall, L. J.↗
Studies of rotating liquid floating zones on Skylab IV
Liquid zones of water, soap solution and soap foam were deployed between two aligned circular disks which were free to rotate about the zone axis in the microgravity environment of Skylab IV. Such a configuration is of interest in the containerless handling of melts for possible future space processing crystal growth experiments. Three basic types of zone surface deformation and instability were observed for these rotational conditions; axisymmetric shape changes under single disk rotation, nonaxisymmetric, whirling, C-modes for long zones with equal rotation of both disks, and capillary wave phenomena for short zones with equal rotation of both disks. The sources of these instabilities and the conditions promoting them are analyzed in detail from video tape recordings of the Skylab experiments.
Carruthers, J. R.↗
Space processing float zone thermal analysis
Thermal analysis (BETA) computer program adaptations were prepared to analyze phase change histories in crystal specimens. The first program (BETA-CYL) treats right circular cylinder configurations and the second, more general, program (BETA-BOR) treats a generalized body-of-revolution configuration. A series of computer runs were made for silicon material to determine boundary conditions which produce flat solidification interfaces while, at the same time, minimizing peak temperatures in the molten zone. Flat solidification interfaces are a goal believed by some investigators to be required to produce high quality semiconductor materials. The thermal effects of convection in a molten zone were examined and found to be negligible in comparison to the conduction heat transfer of the melt.
Pogson, J. T.↗
Analysis of surface tension driven flow in floating zone melting
Surface tension driven flow in a cylindrical melt suspended between two rods was investigated by numerical solution of the steady state differential equations for heat and momentum transfer. Radiation heating and electron beam heating were considered approximately. For small values of the driving force, one rotating ring was formed in the top half of the zone, and its mirror image in the bottom half. At larger driving forces, secondary cells form which probably would undergo oscillatory motion. The influence of Prandtl number, zone movement, and buoyancy on the convection was also studied. The primary resistance to mass transfer in the laminar regime was in the center of the zone rather than at the solid-liquid interfaces.
Chang, C. E.↗
Electron and photon degradation in aluminum, gallium and boron doped float zone silicon solar cells
Solar cells fabricated from Al, Ga and B doped Lopex silicon over a range of resistivities were tested under varying conditions of 1 MeV electron fluence, light exposures and thermal cycling. Results indicate that Al and Ga can replace B as a P type dopant to yield improved solar cell performance.
Rahilly, W. P.↗
Float zone silicon for IR detectors
An overview of the state of the art of processing silicon for use as infrared detectors is presented. Improvements in the process that could be obtained in a low-g environment were examined. The various requirements for the different types of Si detector materials are summarized.
Kern, E. L.↗
Float zone refining: Space problems and solutions. A speculative proposal
A facility for the automatic growth of 60 cm long boules of Si up to 10 cm diameter is described. The facility is 21 ft tall, weighs 17,000 lb (without the sand ballast), and consumes 60 kW power. As a point of reference, the facility will cost approximately $500K without automation which will be developed. The total price is expected to be approximately $1.2 million.
Gill, G.↗
Review of past flight experiments pertinent to float zone
Materials processing experiments performed in space since 1973 are listed. Experiments carried out in Skylab, the Apollo Soyuz mission, and on SPAR sounding rockets are included.
Mckannan, G.↗
Thermocapillary-driven convection in supported and floating-zone crystallization
Marangoni flow was induced in a thin disk of molten tin with an atomically clean surface by heating it from below in an ultra high vacuum apparatus. The radial distribution of temperature was measured and no temperature oscillations were observed. Strong mechanical disturbances introduced at a Marangoni number of about 4300 died out quickly with time indicating that the system was stable. Mathematical models indicate that strong flows in a two cell structure exist under the conditions studied, and that the velocity profile in the cell near the surface is of the boundary layer type which varies rapidly with depth.
Gill, W. N.↗
Radiation characteristics of low resistivity float zone silicon solar cells
The effects of 1-MeV electron irradiation on silicon solar cells with AM0 efficiencies ranging from 17 to 17.7 percent are described. These cells were processed on low-resistivity FZ substrates using techniques recently developed for high-efficiency terrestrial silicon solar cells. Results indicate that these cells are more susceptible to radiation damage. However, they do maintain a greater overall power output than conventional cells to which they were compared. These cells do not demonstrate post-electron-irradiation photon decay as has been described for cells processed on 1-10 ohm-cm FZ silicon.
Crotty, G. T.↗
Numerical simulation of forced convection in a two fluid layered system in a floating zone configuration
Forced convection due to rotational effects has been numerically studied in a stable two-fluid layered system in which the lighter fluid occupies the upper portion of the computational and physical domain. Results are presented for three different fluid height combinations for conditions prevailing in a microgravity environment. It is found that the heavier fluid tends to dominate the flow field, and that equal corotation and counterrotation cases produce nearly identical behavior in the flow and thermal fields.
Ramachandran, N.↗
Energy stability of thermocapillary convection in a model of the float-zone crystal-growth process
Energy stability theory has been applied to a basic state of thermocapillary convection occurring in a cylindrical half-zone of finite length to determine conditions under which the flow will be stable. Because of the finite length of the zone, the basic state must be determined numerically. Instead of obtaining stability criteria by solving the related Euler-Lagrange equations, the variational problem is attacked directly by discretization of the integrals in the energy identity using finite differences. Results of the analysis are values of the Marangoni number below which axisymmetric disturbances to the basic state will decay, for various values of the other parameters governing the problem.
Shen, Y.↗
Thermocapillary convection in a model float zone
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Hyer, J. R.↗
Steady-state thermal-solutal convection and diffusion in a simulated float zone
Models describing the steady-state thermal diffusion in a pure system, the thermal-solutal diffusion in a binary system, and heat and momentum transverse in a pure system are presented. The geometry of the model is described by a 2D Cartesian coordinate system that is applicable for crystal sheets. The melting, solidifying, and melt/gas interfacial shapes as well as the thermal, flow, and solutal profiles are analytically evaluated as functions of the heat and ambient temperature profiles and material properties. The solution procedure involves a coupled asymptotic/numerical approach which reduces the coupled set of partial differential equations to ordinary type. The results should be applicable in situations where melt flows are not intense enough to change the thermal field in pure systems, or where the physical properties of the melt are such that the convective field is decoupled from the thermal field, the latter being established primarily by diffusion.
Young, G. W.↗
Linear-stability theory of thermocapillary convection in a model of float-zone crystal growth
Linear-stability theory has been applied to a basic state of thermocapillary convection in a model half-zone to determine values of the Marangoni number above which instability is guaranteed. The basic state must be determined numerically since the half-zone is of finite, O(1) aspect ratio with two-dimensional flow and temperature fields. This, in turn, means that the governing equations for disturbance quantities will remain partial differential equations. The disturbance equations are treated by a staggered-grid discretization scheme. Results are presented for a variety of parameters of interest in the problem, including both terrestrial and microgravity cases.
Neitzel, G. P.↗