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DOE OSTI2025

Characterization of Flashback and Flame-Holding in a Jet-In-Crossflow Mixing Configuration with Methane-Hydrogen Fuel Blends

An approach that combines experimental and numerical analyses has been implemented to characterize the fundamentals of flashback events and flame-holding phenomena during high-hydrogen combustion in a jet-in-crossflow (JICF) configuration. Such flame dynamics are visualized experimentally using nanosecond (ns)-based hydroxyl planar laser-induced fluorescence (OH-PLIF) and chemiluminescence (CL) diagnostics techniques. The JICF burner has an optically accessible pre-mixing tube allowing the optical diagnostics. The testing was conducted for varied pre-mixer velocities (V) and equivalence ratio (ϕ) for 90%-100% (H2, by mole) H2/CH4 reactant mixtures at atmospheric temperature and pressure conditions. Two distinct flashbacks were identified – conventional rich flashback and lean flashback, recorded while increasing ϕ and decreasing ϕ, respectively. The cause of lean flashback was attributed to lower flux ratio which bends the jet sharply, closer toward the injection plane. The flashback was found to occur along the boundary layer, assisted by the inner wall of the pre-mixer tube. The mean OH-PLIF images characterized the flame-holding behavior where the flame was found to be stabilized on the leeward side only or on both windward and leeward sides as a lifted flame near the fuel port.

flame holding↗

DOE OSTI2025

SynopFrame: Multiscale time-dependent visual abstraction framework for analyzing DNA nanotechnology simulations

We present an open-source framework, SynopFrame, that allows DNA nanotechnology (DNA-nano) experts to analyze and understand molecular dynamics simulation trajectories of their designs. We use a multiscale multi-dimensional abstraction space, connect the representations to a projected conformational space plot of the structure’s temporal sequence, and thus enable experts to analyze the dynamics of their structural designs and, specifically, failure cases of the assembly. In addition, our time-dependent abstraction representation allows the biologists, for the first time in a smooth and structurally clear way, to identify and observe temporal transitions of a DNA-nano design from one configuration to another, and to highlight important periods of the simulation for further analysis. We realize SynopFrame as a dashboard of the different synchronized 3D spatial and 2D schematic visual representations, with a color overlay to show essential properties such as the status of hydrogen bonds. The linking of the spatial, schematic, and abstract views ensures that users can effectively analyze the high-frequency motion. We also categorize the status of the hydrogen bonds into a new format to allow us to color-encode it and overlay it on the representations. To demonstrate the utility of SynopFrame, we describe example usage scenarios and report user feedback.

Abstraction space↗

NASA NTRS1978

The ratio of carbon monoxide to molecular hydrogen in interstellar dark clouds

LTE (C-13)O column densities are compared with the corresponding values of beam-convolved visual extinction at more than 100 locations within 38 different interstellar dark clouds. A roughly linear correlation is found to exist between these two quantities for visual extinctions in the range from about 1.5 to 5 mag. It is argued that this correlation can be extended up to about 10 mag and that the standard gas-to-extinction ratio can be expected to remain valid in the sources studied. The correlation of LTE (C-13)O column density with visual extinction is used to obtain an equation for the H2 column density associated with a given (C-13)O column density. It is shown that if the clouds studied are assumed to be chemically homogeneous, the equation obtained implies that at least 12% of all gas-phase carbon is in the form of CO. Comparison of the observational data with various theories proposed for molecule formation in dark clouds indicates that Langer's (1977) ion-molecule scheme accounts well for the observations when the fractionation channel of Watson et al. (1976) is included.

Dickman, R. L.↗

DOE OSTI2021

Achieving Stable Molybdenum Oxide Cathodes for Aqueous Zinc-Ion Batteries in Water-in-Salt Electrolyte

A layered MoO 3 material with large interlayer spacing represents a promising cathode for aqueous rechargeable Zn-ion batteries (ARZIBs), but the implementation of this material is limited due to the intrinsically low conductivity and poor structural stability. A 30 m ZnCl 2 water-in-salt electrolyte (WISE) was introduced to a MoO 3 nanobelt cathode for the first time, significantly increasing the stability of MoO 3 cathodes compared to those in 3 M ZnSO 4 and 3 M ZnCl2 electrolyte. The Zn/MoO 3 cell in WISE unambiguously demonstrated significantly improved rate performance delivering 349, 253, and 222 mAh/g at 100, 500, and 1000 mA/g, denoting a 2×, and 12× capacity increase of those achieved in 3 M electrolytes at 500 and 1000 mA/g, respectively. A capacity retention rate of 73% was achieved after (dis)charging at 100 mA/g for 100 cycles, and no obvious capacity fading was observed at higher current densities of 500 mA/g and 2A/g. A compilation of structural and morphological characterization was systematically performed to provide insight into the mechanisms of the improved performance in ZnCl 2 WISE for the MoO3 cathode materials. Specifically, our data collectively suggested that the drastic fading in 3M electrolytes can be attributed to the parasitic surface deposits on Zn originated from Mo dissolution and H 2 formation due to Zn corrosion and hydrogen evolution reaction (HER), which were significantly suppressed in the ZnCl 2 WISE. The direct visualization of these side reactions was achieved for the first time in the Zn-MoO 3 system, using an in situ optoelectrochemical measurement.

25 ENERGY STORAGE↗

NASA NTRS2013

Global Response of the Space Shuttle External Tank with the Presence of Intertank Stringer Cracks and Radius Blocks

After propellant was loaded into the external tank (ET), the November 5, 2010 launch of Space Shuttle mission STS-133 was scrubbed due to a gaseous hydrogen leak located in a vent line near the ground umbilical and ET connection. Subsequent visual inspections identified cracks in the sprayed-on foam insulation in the forward end of the ET intertank segment, adjacent to the liquid oxygen (LOX) tank, as shown in Figure 1. These cracks necessitated repair of the foam due to debris concerns that violated launch constraints. As part of the repair process, the affected foam was removed to reveal cracks in the underlying external hat stiffeners on the intertank, as shown in Figure 2. Ultimately, five stiffeners were discovered to be cracked adjacent to the LOX tank. As the managing center for the ET Project, NASA Marshall Space Flight Center (MSFC) coordinated failure investigation and repair activities among multiple organizations, which included the ET prime contractor (Lockheed Martin Space Systems Michoud Operations), the Space Shuttle Program Office at the NASA Johnson Space Center (JSC), the NASA Kennedy Space Center (KSC), and the NASA Engineering and Safety Center (NESC). STS-133 utilized the external tank designated as ET-137. Many aspects of the investigation have been reported previously in Refs. 1-7, which focus on the root cause of the failures, the flight readiness rationale and the local analyses of the stringer failures and repair. This paper summarizes the global analyses that were conducted on ET-137 as part of the NESC effort during the investigation, which was conducted primarily to determine if the repairs that were introduced to the stringers would alter the global response of the ET. In the process of the investigation, a new STAGS tabular input capability was developed to more easily introduce the aerodynamic pressure loads using a method that could easily be extended to incorporate finite element property data such as skin and stiffener thicknesses and beam cross-sectional properties.

Lovejoy, Andrew E.↗

DOE OSTI2026

Reduced-Order Modeling of Hydrogen Releases from Vent Stacks and with Wind Effects

Here, the physical release behavior of hydrogen is important to understand from a safety and design perspective. The consequences of unignited pressurized gaseous hydrogen plumes exiting vent stacks were considered by extending and modifying existing general hydrogen plume models. Entrainment, vent stack backpressure, and the flow regime of hydrogen exiting the vent were found to be significant factors affecting plume shape and size, but further investigation and validation with unchoked, low-Froude-number flows is recommended to improve the model’s robustness. Additionally, models for the effects of wind on unignited plume momentum and entrainment were added to explore this behavior. Wind was assumed to increase mixing of hydrogen with the ambient air, and to affect the momentum of the released jet. Introducing wind into the plume model led to a shorter plume for all wind and jet directions. A high counter-flowing wind led to non-physical results and challenges in interpreting the visualization. The proposed jet plume wind sub-models (specifically entrainment coefficients) were fit and compared to experimental data of different releases of hydrogen into a wind tunnel, but the quantity of data available and experimental conditions were limited. Thus, collection of more empirical data and for a wider range of conditions is recommended for improvement of the proposed computational models. Developing reduced-order models for these physical phenomena can improve accessibility to predicted physical behavior and the rate at which hydrogen systems can be safely designed and deployed.

entrainment↗

NASA NTRS1989

Rotational modulation of hydrogen Lyman alpha flux from 44i Bootis

Observations with IUE that cover the entire 6.4 hr orbital cycle of the late-type contact binary 44i Bootis are presented. Intrinsic stellar hydrogen Lyman alpha emission flux was determined from low-resolution IUE spectra, compensating for geocoronal emission and for interstellar absorption. The variation of the stellar Lyman alpha emission flux correlates well with the variation of the CII and CIV emission fluxes, and shows orbital modulation in phase with the visual light curve. The ratio of Lyman alpha to CII flux (15 to 20) is similar to that observed in solar active regions. Hydrogen Lyman alpha emission is thus one of the most important cooling channels in the outer atmosphere of 44i Boo. A high-resolution spectrum of the Lyman alpha line was obtained between orbital phases 0.0 and 0.6. The integrated flux in the observed high-resolution Lyman alpha profile is consistent with the fluxes determined using low-resolution spectra, and the composite profile indicates that both components of this binary have equally active chromospheres and transition regions. The uncertainty in the interstellar hydrogen column density cannot mimic the observed variation in the integrated Lyman alpha flux, because the stellar line is very much broader than the interstellar absorption.

Vilhu, O.↗

NASA NTRS1988

Rotational modulation of hydrogen Lyman alpha flux from 44ii Bootis

Observations with IUE that cover the entire 6.4 hr orbital cycle of the late-type contact binary 44i Bootis are presented. Intrinsic stellar hydrogen Lyman alpha emission flux was determined from low-resolution IUE spectra, compensating for geocoronal emission and for interstellar absorption. The variation of the stellar Lyman alpha emission flux correlates well with the variation of the C II and C IV emission fluxes, and shows orbital modulation in phase with the visual light curve. The ratio of Lyman alpha to CII flux (15 to 20) is similar to that observed in solar active regions. Hydrogen Lyman alpha emission is thus one of the most important cooling channels in the outer atmosphere of 44i Boo. A high-resolution spectrum of the Lyman alpha line was obtained between orbital phases 0.0 and 0.6. The integrated flux in the observed high-resolution Lyman alpha profile is consistent with the fluxes determined using low-resolution spectra, and the composite profile indicates that both components of this binary have equally active chromospheres and transition regions. The uncertainty in the interstellar hydrogen column density cannot mimic the observed variation in the integrated Lyman alpha flux, because the stellar line is very much broader than the interstellar absorption.

Vilhu, O.↗

NASA NTRS1977

Infrared studies of H II regions and dust clouds near K3-50

Ground-based infrared observations of the K3-50 region are reported at wavelengths between 2 and 34 microns as well as at 1 mm. The main results are that (1) the visible nebular K3-50 is displaced from its infrared and radio counterparts; (2) component Cl (the OH source ON-3) appears very faint at wavelengths not exceeding 20 microns and is therefore probably obscured by several hundred magnitudes of visual extinction; (3) both K3-50 and component C are associated with separate condensations of molecular hydrogen, each of about 3000 solar masses; and (4) there are no strong sources in this region at 20 microns other than those associated with H II condensations.

Wynn-Williams, C. G.↗

NASA NTRS1996

Modelling the Soft X-Ray and EUV Emission in Classical Novae: EUVE and ROSAT Observations of V1974 Cygni

We have conducted an extensive analysis of the observability of Classical Novae with the EUVE Lex/B and Al/Ti/C detectors. Predicted count rates have been computed using optically thin, isothermal plasma models for solar and metal-rich compositions, and hot ONeMg white dwarf model atmospheres. We find EUVE to be quite sensitive to both the EUV and soft X-ray emission emitted by the underlying hot white dwarf during novae outbursts, except for the coolest temperatures with very high intervening hydrogen column density. These results are used to interpret the emission detected during the EUVE all-sky survey of Nova Cygni 1992 (approx. = V1974 Cyg), 279-290 days after visual maximum. We find the best fit to the observed emission from V1974 Cyg arises from a hot ONeMg white dwarf with surface temperature approx. 4 x l0(exp 5) K and a mas of approx. 1.2 solar mass, and derive an interstellar hydrogen column density of approx. 3 x 10(exp 21)/sq cm. Virtually all this emission arises from supersoft X-rays rather than the EUV. We also report the detection of V1974 Cyg with the EUVE Deep Survey detector at 549 days after visual maximum. This observation is compatible with the above properties, indicating that the mechanism responsible for the soft X-ray emission, connected with the underlying white dwarf, had not yet entirely turned off. We also present analysis of a ROSAT PSPC observation which is contemporaneous with the EUVE survey observations; this independently confirms the high column density we derived from the EUVE survey observation. Light curves for the EUVE and ROSAT observations are presented. Statistical tests for variability show that all of these observations are indeed highly variable over various time scales. The EUVE survey data shows one day variations, the EUVE DS data show approx. 30 minute fluctuations, while the ROSAT data vary rapidly on time scales of seconds. The EUVE data shows no periodic variability on any time scale. The implications of the rapid variability are briefly discussed.

Stringfellow, Guy S.↗

NASA NTRS1959

Preliminary Study of a Piston Pump for Cryogenic Fluids

Preliminary data are presented covering the performance of a low-speed, five-cylinder piston pump designed for handling boiling hydrogen. This pump was designed for a flow of 55 gallons per minute at 240 rpm with a discharge pressure of 135 pounds per square inch. Tests were made using JP-4 fuel, liquid nitrogen, and liquid hydrogen. Pump delivery and endurance characteristics were satisfactory for the range of operation covered. In connection with the foregoing pump development, the cavitation characteristics of a preliminary visual model, glass-cylinder pump and of a simple reciprocating disk were studied. Subcooling of approximately 0.60 F was obtained from the cavitation produced by reciprocating a disk in boiling nitrogen and in boiling water. The subcooling obtained in a similar manner with liquid hydrogen was somewhat less.

Biermann, Arnold E.↗

DOE OSTI2021

Insights into the rapid two-phase transport dynamics in different structured porous transport layers of water electrolyzers through high-speed visualization

In proton exchange membrane electrolyzer cells (PEMECs), maintaining efficient two-phase transport is one of the most important functions of porous transport layers (PTLs). To enhance the two-phase transport in PTLs, thin/titanium liquid/gas diffusion layers (TT-LGDLs) are introduced in PEMECs, and their difference from the conventional Ti felt PTLs are analyzed in-situ through high-speed and microscale visualization and electrochemical characterizations. The visualization results show that unfavorable large slugs can be greatly reduced in the PEMEC with a TT-LGDL compared to the PEMEC with a Ti felt PTL. More importantly, the recovery capability of water starvation with different PTLs is studied. After water starvation, the PEMEC with the TT-LGDL can recover the water starvation much more rapidly than the Ti felt cell, benefiting from its short and straight-through flow paths. Furthermore, the TT-LGDL tends to generate oxygen bubbles that are almost six times smaller and 236 times more frequently than the Ti felt PTL, indicating significantly boosted removal efficiency of produced oxygen and PEMEC performance. Finally, this study offers new insights into the dynamic processes of two-phase transport and the recovery capability of water starvation for different PTLs, which will provide valuable guidance for further optimization of PTLs and performance enhancement of PEMECs.

08 HYDROGEN↗

NASA NTRS2008

Supersonic Combusting Jet Experiments for Code Development and Validation

Computational fluid dynamics (CFD) methods based on the Reynolds averaged Navier-Stokes (RANS) equations are extensively employed in the design of hypersonic airbreathing engines. A fundamental weakness in these methods is the accurate mathematical modeling of turbulence and turbulence-combustion interactions. This paper is one of a companion pair of papers which describe the use of the combined dual pump CARS and newly developed interferometric Rayleigh scattering optical system to acquire time-accurate turbulence and mixing data with which to aid calibration and verification of the current turbulence models. This test program consisted of a pilot laboratory-scale experiment used to develop the optical system and data acquisition techniques, and a significantly larger experiment to acquire the necessary turbulence data. The flow is an axially-symmetric, supersonic, combusting, free jet that provides good optical access, consisting of a central jet of hot "vitiated air" and a coflow jet of hydrogen or ethylene fuel. In this paper the development of both experiments is described. Facility and flow visualization data are presented for various types of flames, including the flames selected for detailed study with the CARS/Rayleigh optical techniques.

Cutler, Andrew D.↗

NASA NTRS1977

A survey of interstellar HI from L alpha absorption measurements 2

The Copernicus satellite surveyed the spectral region near L alpha to obtain column densities of interstellar HI toward 100 stars. The distance to 10 stars exceeds 2 kpc and 34 stars lie beyond 1 kpc. Stars with color excess E(B-V) up to 0.5 mag are observed. The value of the mean ratio of total neutral hydrogen to color excess was found to equal 5.8 x 10 to the 21st power atoms per (sq cm x mag). For stars with accurate E(B-V), the deviations from this mean are generally less than a factor of 1.5. A notable exception is the dark cloud star, rho Oph. A reduction in visual reddening efficiency for the grains that are larger than normal in the rho Oph dark cloud probably explains this result. The conversion of atomic hydrogen into molecular form in dense clouds was observed in the gas to E(B-V) correlation plots. The best estimate for the mean total gas density for clouds and the intercloud medium, as a whole, in the solar neighborhood and in the plane of the galaxy is 1.15 atoms per cu. cm; those for the atomic gas and molecular gas alone are 0.86 atoms per cu cm and 0.143 molecules per cu cm respectively. For the intercloud medium, where molecular hydrogen is a negligible fraction of the total gas, atomic gas density was found to equal 0.16 atoms per cu cm with a Gaussian scale height perpendicular to the plane of about 350 pc, as derived from high latitude stars.

Bohlin, R. C.↗

NASA NTRSDate not supplied

High-Speed Visualization of Spray Breakup and Velocity Estimation in a Rotating Detonation Combustor Using Laser Induced Fluorescence

The underlying physical processes that liquid fuel sprays undergo in rotating detonation engines, particularly breakup and combustion, are not well understood nor are the coupling effects between the detonation and the spray. In this work, a single liquid jet of liquid fuel is inserted into a hydrogen-air RDC in order to study repetitive-one way coupled detonation interactions. High speed laser induced fluorescence of Jet-A at 300 kHz is used to visualize the dynamic processes inside the RDC for up to 10 ms per test. The employed imaging schemes allowed for unique insight into the spreading of liquid fuel in the azimuthal-axial directions via volumetric laser illumination. The Jet-A velocity field was estimated using OpenOpticalFlow and the impulse events observed colloquially agree with prior work on this test platform.

Instrumentation↗

NASA NTRSDate not supplied

High-Speed Visualization of Spray Breakup and Velocity Estimation in a Rotating Detonation Combustor Using Laser Induced Fluorescence

Instrumentation↗

DOE OSTI2020

Liquid helium fluid dynamics studies. Final Technical Report

Future high energy physics accelerators depend on a number of advanced technologies to open the many doors of scientific discovery. Among these advanced technologies, superconducting magnets and superconducting radio frequency (SRF) cavities are the backbone of the accelerator and detector systems. But all these low temperature systems depend critically on successful and reliable operation of their supporting technologies, among which the liquid helium cooling system is of the utmost importance. To improve the quality of these systems both in terms of efficiency and reliability, a robust helium cryogenics research and development (R&D) effort is required. The proposed research to be conducted by the FSU cryogenics group aims to produce fundamental knowledge that meets this R&D need. The projects that we have completed over the past grant period at Florida State University consist of experimental research on liquid helium fluid dynamics and heat transfer problems relevant to the development of future superconducting particle physics accelerators. Liquid helium is the coolant used in all such facilities and in many of these facilities He II (the low temperature phase of liquid helium also known as superfluid helium) is preferred due to its outstanding heat transfer characteristics. The work consists of two main experimental studies that probe both fundamental as well as practical aspects of liquid helium cooling. The first is a broad and fundamental study of the heat and mass transfer processes that can occur during a sudden catastrophic loss of vacuum (SCLV) incident in a superconducting accelerator. SCLV refers to the remote but extremely critical accident scenario where atmospheric pressure air is allowed to flood into the insulating vacuum system and impinge on the liquid helium cooled surfaces in the accelerator. Safe performance and recovery from such accidents is essential to the reliable operation of superconducting accelerators. The dynamics of this process is quite complex and so our approach is to conduct a series of well-orchestrated experiments that probe the various physical phenomena that can occur during an SCLV event. The experiments are coupled with analytic and numerical analysis in an effort to develop a general understanding of the process and to assist with future accelerator design and development. The second activity is directed toward fundamental understanding of heat and mass transfer in He II, which is essential to the design of superconducting magnets and radio frequency cavities in accelerators. The work consists of flow visualization of the dynamics of He II using laser assisted techniques. Two complementary techniques are used to study the fundamentals of the turbulent state. The first technique uses neutrally buoyant solid hydrogen particles to probe the flow fields of the superfluid and normal fluid components. The other technique uses laser excited He2* molecules as tracers of the normal fluid motion within the He II. The activities also included an effort to use visualization techniques to locate transient hot spots in radio frequency superconducting cavities. Such work provides valuable information about the heat transfer process in He II and its impact on the performance of superconducting devices. The research effort at Florida State University is not directly in support of a specific high energy physics experiment or facility. Rather, the work is general and coordinated with HEP accelerator laboratories to provide valuable insight that can assist with future accelerator development.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

DOE OSTI2022

Approach to using 3D laser-induced breakdown spectroscopy (LIBS) data to explore the interaction of FLiNaK and FLiBe molten salts with nuclear-grade graphite

Nuclear graphite has historically been a key component of many nuclear reactor designs and has emerged as key to numerous advanced nuclear reactor design concepts. Molten salt reactors (MSRs) are one broad group of advanced reactor designs currently being pursued by industry for commercialization. Several MSR designs under consideration use graphitic materials that directly interface with a molten salt, whether it is a fuel salt, coolant salt, or both. Therefore, the interaction of graphite materials with molten salts must be understood. To gain this required understanding, a range of data is needed including porosity, strength, and composition as a function of different salt exposure parameters. In this study, a laser-induced breakdown spectroscopy (LIBS) measurement and data analysis methodology was developed to obtain spatially resolved elemental composition information for graphite samples exposed to a molten fluoride salt. Traditional univariate emission line analysis of atomic, ionic, and molecular optical emission signals was coupled via correlation analysis with spectral decomposition of the data using principal component analysis. Elemental depth profiling and elemental mapping were also performed to visualize salt–graphite interactions. LIBS was demonstrated to be useful for measuring key analytes such as fluorine and hydrogen, which are troublesome for other analysis techniques. Evidence for complex behavior was found, thereby demonstrating the usefulness of the developed approach for future systematic studies.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗