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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 109 records · Page 6

Microscale Concentration Measurements Using Laser Light Scattering Methods

The development of lab-on-a-chip devices for microscale biochemical assays has led to the need for microscale concentration measurements of specific analyses. While fluorescence methods are the current choice, this method requires developing fluorophore-tagged conjugates for each analyte of interest. In addition, fluorescent imaging is also a volume-based method, and can be limiting as smaller detection regions are required.

Niederhaus, Charles↗

Discrete wavelength-locked external cavity laser

An external cavity laser (and method of generating laser light) comprising: a laser light source; means for collimating light output by the laser light source; a diffraction grating receiving collimated light; a cavity feedback mirror reflecting light received from the diffraction grating back to the diffraction grating; and means for reliably tuning the external cavity laser to discrete wavelengths.

Pilgrim, Jeffrey S.↗

Laser pulse detection method and apparatus

A sensor is described for detecting the difference in phase of a pair of returned light pulse components, such as the two components of a light pulse of an optical gyro. In an optic gyro, the two light components have passed in opposite directions through a coil of optical fiber, with the difference in phase of the returned light components determining the intensity of light shining on the sensor. The sensor includes a CCD (charge coupled device) that receives the pair of returned light components to generate a charge proportional to the number of photons in the received light. The amount of the charge represents the phase difference between the two light components. At a time after the transmission of the light pulse and before the expected time of arrival of the interfering light components, charge accumulating in the CCD as a result of reflections from optical components in the system, are repeatedly removed from the CCD, by transferring out charges in the CCD and dumping these charges.

Goss, Willis C.↗

System and method for performing laser powder bed fusion using controlled, supplemental in situ surface heating to control microstructure and residual stresses in formed part

The present disclosure relates to an additive manufacturing system for forming a part using a powder material. In one embodiment the system makes use of a primary heat generating subsystem to generate a fusing beam for heating and fusing at least one of select portions of a powder layer, or an entire area of a powder layer, deposited on a build plate. The system also incorporates a beam steering subsystem for steering the fusing beam over the powder layer. A supplemental heating subsystem is used to generate a wide area beam to heat a portion of the powder layer either prior to fusing, along with the fusing operation, or subsequent to fusing of the powder with the fusing beam. The wide area beam has an intensity which is insufficient to fuse the powder, and alters a microstructure of the powder layer as the powder layer is at least one of fused or as it cools, to thus relieve stress in the part.

Smith, William↗

Considerations to achieve directionality for gamma ray lasers

A method of alignment of nuclei for a gamma ray laser and a means of achieving preferential emission of radiation along the crystal axis are studied. Atomic alignment was achieved by materials researchers who made composite structures composed of needle-like single crystals all with the same orientation and all pointing in the same direction contained in a matrix of cobalt or nickel. The proposed method of preferential emission of radiation along the aligned needles is to have a symmetric field gradient at the nucleus and a sequence of excited levels of spin and parity 2(+) and 0(+). The proposed scheme reduces the density of excited states required for lasing and reduces the linewidth due to inhomogenous broadening. Mossbauer absorption experiments intended to test these ideas are outlined.

Jha, S.↗

Automated homodyne analysis instrumentation for characterizing S.C. lasers

A versatile laser characterization method is described for evaluating semiconductor lasers developed under R&D efforts and also commercially available lasers. This method features a high-resolution technique for measuring laser linewidth that was also found to introduce optical feedback to the laser. The modified delayed self-homodyne system is therefore utilized to collect a variety of laser characteristic measurements under dynamic operating conditions while simultaneously assessing the effects of optical feedback on the laser. Measurements employing scanning Fabry-Perot interferometers are described which supplement the data obtained from direct measurements and measurements made utilizing the self-homodyne system.

Hendricks, Herbert D.↗

Tetravalent chromium doped laser materials and NIR tunable lasers

A method is described to improve and produce purer Cr.sup.4+-doped laser materials and lasers with reduced co-incorporation of chromium in any other valence states, such as Cr.sup.3+, Cr.sup.2+, Cr.sup.5+, and Cr.sup.6+. The method includes: 1) certain crystals of olivine structure with large cation (Ca) in octahedral sites such as Cr.sup.4+:Ca.sub.2GeO.sub.4, Cr.sup.4+:Ca.sub.2SiO.sub.4, Cr.sup.4+:Ca.sub.2Ge.sub.xSi.sub.1-xO.sub.4 (where 0<x<1), and/or 2) high-temperature solution growth techniques that enable the growth of the crystals below the temperature of polymorphic transitions by using low melting point solvent based on oxide, fluoride and/or chloride compounds. Purer Cr.sup.4+-doped laser materials are characterized by a relatively high concentration of Cr.sup.4+-lasing ion in crystalline host that makes these materials suitable for compact high power (thin disk/wedge) NIR laser applications.

Alfano, Robert R.↗

Modeling of dynamic effects of a low power laser beam

Methods of modeling some of the dynamic effects involved in laser beam propagation through the atmosphere are addressed with emphasis on the development of simple but accurate models which are readily implemented in a physical optics code. A space relay system with a ground based laser facility is considered as an example. The modeling of such characteristic phenomena as laser output distribution, flat and curved mirrors, diffraction propagation, atmospheric effects (aberration and wind shear), adaptive mirrors, jitter, and time integration of power on target, is discussed.

Lawrence, George N.↗

High density pixel array and laser micro-milling method for fabricating array

A pixel array device is fabricated by a laser micro-milling method under strict process control conditions. The device has an array of pixels bonded together with an adhesive filling the grooves between adjacent pixels. The array is fabricated by moving a substrate relative to a laser beam of predetermined intensity at a controlled, constant velocity along a predetermined path defining a set of grooves between adjacent pixels so that a predetermined laser flux per unit area is applied to the material, and repeating the movement for a plurality of passes of the laser beam until the grooves are ablated to a desired depth. The substrate is of an ultrasonic transducer material in one example for fabrication of a 2D ultrasonic phase array transducer. A substrate of phosphor material is used to fabricate an X-ray focal plane array detector.

Wiener-Avnear, Eliezer↗

Geodetic applications of laser ranging

The paper describes the use of dynamic methods of laser ranging of a low altitude satellite along with proposed experiments involving both dynamic and geodetic methods of laser ranging of the Lageos satellite. Particular attention is given to the testing of laser ranging techniques across the San Andreas Fault in California where it is hoped that plate motion will be observable after several years of measurements.

Smith, D. E.↗

Polarization-stabilized 1.15- and 3.39-micron He-Ne lasers

Two methods for polarization stabilization of an internal-mirror 3.39-micron He-Ne laser are reported. The first relies on a concurrently lasing 1.15-micron transition by fixing the relative amplitude of two orthogonally polarized longitudinal modes that are split by a Rochon prism and detected with separate Si photodiodes. In the second method, two spatially separated orthogonally polarized adjacent 3.39-micron modes are optically balanced, differentially chopped, and recombined on a single InSb photodiode for phase-sensitive detection. The dual-wavelength scheme has been tested by beating against a methane-stabilized 3.39-micron He-Ne laser, which yields maximum excursions of less than 0.5 MHz over several hours and comparable reproducibility. The polarization-stabilized He-Ne laser has been used as a reference for a tunable color-center laser molecular-beam optothermal spectrometer and provides a precision of better than 2 MHz.

Junttila, M.-L.↗

Excess noise in tunable diode lasers

The method and the apparatus for identifying excess-noise regions in tunable diode lasers are described. These diode lasers exhibit regions of excess noise as their wavelength is tuned. If a tunable diode laser is to be used as a local oscillator in a superheterodyne optical receiver, these excess-noise regions severely degrade the performance of the receiver. Measurement results for several tunable diode lasers are given. These results indicate that excess noise is not necessarily associated with a particular wavelength, and that it is possible to select temperature and injection current such that the most ideal performance is achieved.

Rowland, C. W.↗

Laser Crystallization and Dopant Activation of a-Si:H Carrier-Selective Layer in TOPCon Si Solar Cells

Herein, we present a pulsed-laser processing method for crystallization and dopant activation of a highly n-doped amorphous silicon (a-Si:H) carrier-selective layer in a tunnel oxide passivated contact (TOPCon) Si solar cell structure. Here, the laser method provides enhanced conductivity and implied open circuit voltage while reducing emitter saturation current density and surface heating, as opposed to conventional high-temperature furnace annealing of the bulk Si wafer with a TOPCon structure. We identify an appropriate laser wavelength, fluence, and layer thickness using modeling and simulations. Raman and Hall effect measurements demonstrate increased crystallinity and dopant activation, whereas photoconductive decay shows enhanced surface and interface passivation quality. Additionally, we examine the role of subsequent SiNx deposition on further improving the passivation of laser-processed TOPCon layers to achieve a 5.9 kΩ/sq film sheet resistance, 2 ms effective carrier lifetime, 718 mV implied open-circuit voltage (iVOC), and 8.6 fA/cm 2 one-side recombination current density (J0) with the potential for further passivation improvement via laser process and a-Si layer thickness optimization.

14 SOLAR ENERGY↗

Length controlled stabilized mode-lock ND:YAG laser

A method and apparatus for stabilizing the amplitude and repetition rate of mode-locked Nd:YAG laser pulses by controlling the laser length through a feedback loop are described. The end mirror of the laser is mounted on a piezoelectric crystal which is dithered at a low frequency. A portion of fundamental 1.06 micrometer laser radiation is converted into its second harmonic frequency, and the average power of the second harmonic frequency is detected by an integrating detector. The amount of the power of the second harmonic frequency depends on the match between the optical length of the laser cavity and the mode-lock frequency. The length is controlled by a feedback loop which phase compares the output of the second harmonic detector to the piezoelectric crystal dither signal.

Sigfred, J.↗

Multiframe X-ray diffraction on the OMEGA EP laser

A method of measuring multiple temporally resolved powder x-ray diffraction measurements during a single dynamic compression laser experiment has been demonstrated on the OMEGA EP laser. Up to four time-gated snapshots of the x-ray diffraction pattern are collected on an ultrafast x-ray framing camera with a 2θ scattering angle coverage of 48°–65° and 400-ps temporal resolution with the potential for 10°–160° and 200-ps resolution. X-ray diffraction snapshots capture the transformation to a high-pressure β phase in ramp-compressed Zr, constraining the atomic structure and pressure–density equation-of-state in a single shot. Here, this platform will be used to constrain transition pressures, understand the role of kinetics, and verify the existence of hysteresis and metastability on phase transformations at the lattice level under single-shot dynamic compression.

47 OTHER INSTRUMENTATION↗

A Scalable Solution Route to Porous Networks of Nanostructured Black Tungsten

This paper studied the feasibility of a new solution-processed method to manufacture black tungsten nanostructures by laser conversion of tungsten hexacarbonyl precursor on the Inconel 625 substrate under argon atmosphere at ambient pressure. The results show that sublimation of the precursor can be prevented if the decomposition temperature (>170 °C) is achieved using the laser heating method. Three different laser powers from 60–400 W were used to investigate the role of laser parameters on the conversion. It was found that lower laser power of 60 W resulted in a mixture of unconverted precursor and converted tungsten. Higher laser powers >200 W resulted in α-W (BCC) in one step without further heat treatment. Different oxygen concentrations from 0.5 ppm to 21 vol% were used in the laser canister to investigate the effect of oxygen concentration on the conversion. It was found that the hard vacuum (>10−4 torr) or hydrogen is not necessary to obtain α-W (BCC). The solar absorptance varied from 63–97%, depending on the amount of precursor deposited on the substrate and oxygen content in the laser canister. This solution-based laser conversion of tungsten precursor is a scalable method to manufacture tungsten coatings for high-temperature applications.

14 SOLAR ENERGY↗

Toward the Development of Molten Salt Reactor Diagnostics based on Resonantly Enhanced Laser Spectroscopy

One emerging concern within the safeguards community is how to best ensure compliance with nuclear security regulations within molten salt reactor (MSR) facilities. This problem is nontrivial as molten salts used for fuel or coolant are highly corrosive, chemically complex, and inherently require high operational temperatures. Laser spectroscopy methods such as laser-induced breakdown spectroscopy (LIBS) and laser-induced fluorescence (LIF) have previously been suggested for molten salt diagnostics due to their compatibility with liquid phase samples and potential for in-situ measurements [1]. In the former, the laser is used to ionize the sample, allowing for the characteristic light from electronic de-excitation as the resultant plasma cools to be used for material characterization. In the latter, a tunable light source is set be resonant with a specific transition, resulting in element specific excitation and the emission of fluorescence light. In our previous work [2], we demonstrated that LIF could be used for the detection of fission fragments such as Nd in solution through the separation of laser scatter and fluorescence within the time domain. Here, we present progress towards two alternate measurement schemes: LIF measurements based on spectroscopic discrimination of fluorescence emissions and resonant LIBS measurements that induce plasma using a light source set to the resonant frequency of a specific electronic transition. Both methods aim to exploit resonant excitation methods to enhance the emitted signal. The studies may provide routes for element-specific detection of constituents within complicated matrices and a means to better understand the chemical behavior of lanthanides and actinides relevant to MSRs.

98 - NUCLEAR DISARMAMENT, SAFEGUARDS, AND PHYSICAL↗

Method and circuit for shaping laser output pulses

The invention is a method and circuit for shaping laser output pulses from a laser resonator. A Q-switch and polarizer act in combination to control the loss to the resonator and provide the laser output representative of such loss. An optical diode senses the level of the output pulse and provides an output signal that when amplified is used to control voltage from a supply to provide a control signal which is applied to the Q-switch to control the shape of the output pulse by adjusting its length.

Barnes, Norman P.↗