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NASA NTRS1972

Preparation, verification, and operational control of a large space-environment-simulation chamber for contamination sensitive tests

A 2-year program to prepare chamber A at the NASA Manned Spacecraft Center for Apollo telescope mount thermal-vacuum tests is discussed. This program covers modification to existing chamber systems, the development of facility and chamber operating procedures, the selection of chamber cleaning and control methods, and the development and evaluation of diagnostic instrumentation. Extensive efforts to ensure a minimum contamination environment for the Apollo telescope mount test series are illustrated. Recent thermal-vacuum tests of this chamber at progressive stages of cleanliness have demonstrated the success achieved in reducing the particulate and molecular contamination levels of the basic chamber interior.

Visentine, J. T.↗

NASA NTRS1998

Calibration Results for the AXAF Flux Contamination Monitor

The AXAF Flux Contamination Monitor (FCM) serves the purposes of transferring the absolute flux calibration from the ground calibration at the X-Ray Calibration Facility (XRCF) to operation on orbit and of detecting any changes in molecular contamination of the High-Resolution Mirror Assembly (HRMA) between ground calibration and the post-launch activation. We describe the design, construction, and characterization of the FCM radioactive sources, and their placement on the Forward Contamination Cover (FCC). We present results from FCM measurements with the AXAF focal-plane instruments, particularly the AXAF CCD Imaging Spectrometer (ACIS), during the ground calibration phase at the XRCF in 1997. Finally, we describe the plans for FCM on-orbit measurements during observatory activation and for the subsequent analysis.

Elsner, R. F.↗

NASA NTRS2015

NASA Applications of Molecular Adsorber Coatings

The Molecular Adsorber Coating (MAC) is a new, innovative technology that was developed to reduce the risk of molecular contamination on spaceflight applications. Outgassing from materials, such as plastics, adhesives, lubricants, silicones, epoxies, and potting compounds, pose a significant threat to the spacecraft and the lifetime of missions. As a coating made of highly porous inorganic materials, MAC offers impressive adsorptive capabilities that help capture and trap contaminants. Past research efforts have demonstrated the coating's promising adhesion performance, optical properties, acoustic durability, and thermal stability. These results advocate its use near or on surfaces that are targeted by outgassed materials, such as internal optics, electronics, detectors, baffles, sensitive instruments, thermal control coatings, and vacuum chamber test environments. The MAC technology has significantly progressed in development over the recent years. This presentation summarizes the many NASA spaceflight applications of MAC and how the coatings technology has been integrated as a mitigation tool for outgassed contaminants. For example, this sprayable paint technology has been beneficial for use in various vacuum chambers for contamination control and hardware bake-outs. The coating has also been used in small instrument cavities within spaceflight instrument for NASA missions.

molecular contaimination↗

NASA NTRS1993

Contamination design of a Scientific Instrument Protective Enclosure for the Hubble Space Telescope Servicing Mission

A Scientific Instrument Protective Enclosure (SIPE) was designed to accommodate second generation science instruments (SIs) for the Hubble Space Telescope (HST) First Servicing Mission (FSM). One of the main design drivers for the SIPE is to provide a protective environment for the SIs against particulate and molecular contaminants that pose a viable threat to the SI performance. The focus of this paper will detail the methodology incorporated in the design of the SIPE to provide a controlled environment for SI protection at the launch site, during pre-launch/launch activities, and during on-orbit operations in the Shuttle bay.

Hedgeland, Randy J.↗

NASA NTRS1998

Calibration Results for the AXAF Flux Contamination Monitor

The Flux Contamination Monitor (FCM) on the Advanced X-ray Astrophysics Facility (AXAF) serves the purposes of transfering the absolute flux calibration from the ground calibration at the X-Ray Calibration Facility (XRCF) at Marshall Space Flight Center to operation on orbit and of detecting any changes in molecular contamination of the High Resolution Mirror Assembly (HRMA) between ground calibration and the post-launch activation phase. we describe the design, construction, and characterization of the FCM radioactive sources, and their placement on the Forward Contamination Cover (FCC). We present results from FCM measurements with the AXAF focal plane instruments, particularly the AXAF CCD Imaging Spectrometer (ACIS), during the ground calibration phase at XRCF in 1997. Finally, we describe the plans for FCM on-orbit measurements during observatory activation and the subsequent analysis.

Elsner, Ronald F.↗

NASA NTRS2022

Clean Air Shower Curtain for Protection of Contamination Sensitive Telescopes on the Ariane 5 Launcher

The launch of the James Webb Space Telescope (JWST) was successfully performed by Ariane 5 from French Guiana on December 25th 2021. The unique nature of the JWST mission led to various adaptations of the Ariane 5 launch system to fulfill stringent cleanliness and hygrometry requirements all along the launch preparation. JWST integration and test activities in the Final Assembly Building (BAF) had to be performed in ISO Class 7 equivalent conditions under Volatile Organic Compounds (VOC) protection and monitoring. For this purpose, a dedicated air supply system equipped with Airborne Molecular Contamination (AMC) filters was installed in the umbilical mast. The fairing itself was specially sealed to protect the inner environment, and to, guarantee ISO Class 7, the BAF Composite Hall (BAF-HC) facilities were upgraded with a removable “Air Shower Curtain” (AShC) containment enclosure between the mobile platforms around JWST. The preparation of these Ariane 5 launch system adaptations started several years before the launch campaign with close cooperation and coordination between Arianespace, ArianeGroup, the European Space Agency (ESA) and the National Aeronautics and Space Administration (NASA). This paper describes their specificities and addresses the challenges experienced to achieve the successful mission preparation.

Contamination Control, James Webb Space Telescope,↗

NASA NTRS2022

Clean Air Shower Curtain for Protection of Contamination Sensitive Telescopes on the Ariane 5 Launcher

Contamination Control, James Webb Space Telescope,↗

NASA NTRS2000

Measurements with the Chandra Flight Contamination Monitor

NASA's Chandra X-ray Observatory includes a Flight Contamination Monitor (FCM), a system of 16 radioactive calibration sources mounted to the inside of the Observatory's forward contamination cover. The purpose of the FCM is to verify the ground-to-orbit transfer of the Chandra flux scale, through comparison of data acquired during the ground calibration with those obtained in orbit, immediately prior to opening the Observatory's sun-shade door. Here we report results of these measurements, which place limits on the change in mirror-detector system response and, hence, on any accumulation of molecular contamination on the mirrors' iridium-coated surfaces.

Elsner, R. E.↗

NASA NTRS2000

Measurements with the Chandra X-ray Observatory's Flight Contamination Monitor

NASA's Chandra X-ray Observatory includes a Flight Contamination Monitor (FCM), a system of 16 radioactive calibration sources mounted to the inside of the Observatory's forward contamination cover. The purpose of the FCM is to verify the ground-to-orbit transfer of the Chandra flux scale, through comparison of data acquired during the ground calibration with those obtained in orbit, immediately prior to opening the Observatory's sun-shade door. Here we report results of these measurements., which place limits on the change in the mirror-detector system response and, hence, on any accumulation of molecular contamination on the mirrors' iridium-coated surfaces between the two sets of measurements.

Elsner, R. F.↗

NASA NTRS1992

The LDEF experience. Materials

An overview is provided of the LDEF (Long Duration Exposure Facility) mission and the preliminary findings, focusing on the materials related disciplines. These findings are based on observations of low-earth orbit environmental effects on materials made in space during LDEF retrieval and during LDEF tray deintegration, and on initial findings of laboratory analyses of LDEF materials. Included are effects of individual environmental parameters: atomic oxygen, ultraviolet radiation, meteoroid and debris impacts, thermal cycling, vacuum, and contamination, plus combined effects of these parameters. Materials considered include thermal control coatings and surface treatments, ceramics and glasses, metals, polymers, and polymer matrix composites. In general, preliminary LDEF data are remarkably consistent; LDEF will provide a benchmark for materials design data bases for satellites in low earth orbit. Some materials were identified to be encouragingly resistant to low earth orbit space environmental effects for 5.8 years; other space qualified materials displayed significant environmental degradation. Molecular contamination was widespread.

Stein, Bland A.↗

NASA NTRS2012

Contamination Control Assessment of the World's Largest Space Environment Simulation Chamber

The Space Power Facility s thermal vacuum test chamber is the largest chamber in the world capable of providing an environment for space simulation. To improve performance and meet stringent requirements of a wide customer base, significant modifications were made to the vacuum chamber. These include major changes to the vacuum system and numerous enhancements to the chamber s unique polar crane, with a goal of providing high cleanliness levels. The significance of these changes and modifications are discussed in this paper. In addition, the composition and arrangement of the pumping system and its impact on molecular back-streaming are discussed in detail. Molecular contamination measurements obtained with a TQCM and witness wafers during two recent integrated system tests of the chamber are presented and discussed. Finally, a concluding remarks section is presented.

Snyder, Aaron↗

NASA NTRS2018

Preventing Premature Death in the M&S Lifecycle: Lessons Learned from Resurrection and Modernization of a Space System Contamination Model

Models and simulations (M&S) are often developed to meet specific needs and unique requirements for a particular situation. Once the M&S is implemented for a specific case and questions are answered, the M&S may go dormant until a similar need arises again at a later time, perhaps months to years later. Possible modification of the M&S may be required, and issues may arise if the M&S is not well documented, captured, or available. This can severely limit the useful life of the M&S and hinder future development or enhancements. This situation occurred with an M&S tool that had been developed to determine the impact to space system performance due to the presence of molecular contaminant films accumulating on key spacecraft surfaces. The challenges and issues encountered when resurrecting, executing, and modernizing the tool will be presented as a case study. To stay ahead of tomorrow’s challenges, resources to create M&S tools must be utilized efficiently. Lessons learned from this case study will aid M&S developers and users in planning for proper maintenance, transfer, and capture of key M&S tools and knowledge to avoid increased cost, increased development time, and wasted resources for projects relying on M&S.

Seasly, Elaine↗

NASA NTRS1983

Modeling correlation with flight data

The molecular contamination flow model (space 2 program) predicts the induced environment of the space shuttle orbiter/payload on orbit as well as the induced gas flow between the orbiter and payload surfaces. This computer program relates the input parameters which characterize the time dependent status of the orbiter/payload to the required output parameters. An application of the model to data from space transportation system flights 1, 2, and 3 shows that the model correlates well for direct flow and for return flux (STS-2/H2O). Correlation for return flux from other molecular sources/species appears to be within expectations but more analysis is required. The space 2 model seems to be an adequate predictive tool.

Ehlers, H. K. F.↗

NASA NTRS2010

Field Analysis of Microbial Contamination Using Three Molecular Methods in Parallel

Advanced technologies with the capability of detecting microbial contamination remain an integral tool for the next stage of space agency proposed exploration missions. To maintain a clean, operational spacecraft environment with minimal potential for forward contamination, such technology is a necessity, particularly, the ability to analyze samples near the point of collection and in real-time both for conducting biological scientific experiments and for performing routine monitoring operations. Multiple molecular methods for detecting microbial contamination are available, but many are either too large or not validated for use on spacecraft. Two methods, the adenosine- triphosphate (ATP) and Limulus Amebocyte Lysate (LAL) assays have been approved by the NASA Planetary Protection Office for the assessment of microbial contamination on spacecraft surfaces. We present the first parallel field analysis of microbial contamination pre- and post-cleaning using these two methods as well as universal primer-based polymerase chain reaction (PCR).

Morris, H.↗

NASA NTRS1990

An outgassing model of non-metallic materials for the ascent of a Titan 4 launch vehicle

Outgassing of nonmetallic materials and components inside Titan IV's 2A compartment during ascent may present a problem to the payload community in relation to molecular deposition and degradation of sensitive payload surfaces. The procedure currently being developed to model the amounts, transport, and deposition of outgassed molecular contaminants onto a payload's sensitive surface consists of three phases. The first phase involves the development of a thermogravimetric method that recreates the increasing temperature and decreasing pressure profiles expected in the 2A compartment of the TIV launch vehicle during ascent. The second phase involves the determination of deposition rates of outgassed materials onto a payload surface, and the subsequent evaporation rate as a function of temperature of deposited material. The third phase takes the temperature and pressure profiles from phase one, the deposition and evaporation rates and kinetic coefficients determined in phase two, and incorporates them into the SPACE II computer program to determine which payload surfaces are most susceptible to molecular deposition from TIV's outgassing sources, and the level of permanent deposition expected on those surfaces.

Barrows, R. D.↗

NASA NTRS1992

LDEF materials: An overview of the interim findings

The flight and retrieval of the National Aeronautics and Space Administration's Long Duration Exposure Facility (LDEF) provided an opportunity for the study of the low-Earth orbit (LEO) environment and long-duration space environmental effect (SEE) on materials that are unparalleled in the history of the U.S. space program. The 5.8-year flight of LDEF greatly enhanced the potential value of materials data from LDEF to the international SEE community, compared to that of the original 1-year flight plan. The remarkable flight attitude stability of LDEF enables specific analyses of various individual and combined effects of LEO environmental parameters on identical materials of the same space vehicle. NASA recognized the potential by forming the LDEF Space Environmental Effects on Materials Special Investigation Group (MSIG) to address the greatly expanded materials and LEO space environment parameter analysis opportunities available in the LDEF structure, experiment trays, and corollary measurements, so that the combined value of all LDEF materials data to current and future space missions will be assessed and documented. This paper provides an overview of the interim LDEF materials findings of the Principal Investigators and the Materials Special Investigation Group. These revelations are based on observations of LEO environmental effects on materials made in-space during LDEF retrieval and during LDEF tray deintegration at the Kennedy Space Center, and on findings of approximately 1.5 years of laboratory analyses of LDEF materials by the LDEF materials scientists. These findings were extensively reviewed and discussed at the MSIG-sponsored LDEF Materials Workshop '91. The results are presented in a format which categorizes the revelations as 'clear findings' or 'confusing/unexplained findings' and resultant needs for new space materials developments and ground simulation testing/analytical modeling in seven categories: environmental parameters and data bases; LDEF contamination; thermal control coatings and protective treatments; polymers and films; polymer-matrix composites; metals, ceramics, and optical materials; and systems-related materials. General outlines of findings of the other LDEF Special Investigation Groups (Ionizing Radiation, Meteoroid and Debris, and Systems) are also included. The utilization of LDEF materials data for future low-earth orbit missions is also discussed, concentrating on Space Station Freedom. Some directions for continuing studies of LDEF materials are outlined. In general, the LDEF data is remarkable consistent; LDEF will provide a 'benchmark' for materials design data bases for satellites in low-Earth orbit. Some materials were identified to be encouragingly resistant to LEO SEE for 5.8-years; other 'space qualified' materials displayed significant environmental degradation. Molecular contamination was widespread; LDEF offers an unprecedented opportunity to provide a unified perspective of unmanned LEO spacecraft contamination mechanisms. New material development requirements for long-term LEO missions have been identified and current ground simulation testing methods/data for new, durable materials concepts can be validated with LDEF results. LDEF findings are already being integrated into the design of Space Station Freedom.

Stein, Bland A.↗

NASA NTRS2024

Contamination Results of MISSE 8 Wake and Nadir Samples After 2 Years of Space Exposure on the International Space Station

Spacecraft in low Earth orbit (LEO) are subjected to harsh environmental conditions, including radiation (cosmic rays, ultraviolet, x-ray and charged particle radiation), micrometeoroids and orbital debris, temperature extremes, thermal cycling, and atomic oxygen. In addition, on-orbit spacecraft contamination is a serious spaceflight issue, with silicone contamination being a particular concern. In an effort to understand on-orbit contamination of Materials International Space Station Experiment 8 (MISSE 8) flight samples and other International Space Station (ISS) payloads, contamination studies were conducted post-flight on retrieved Teflon fluorinated ethylene propylene (FEP) samples flown in the wake and nadir orientations on MISSE 8. The wake sample was Teflon FEP (M8-W11) flown as part of the Glenn MISSE 8 Polymers Experiment on the Optical Reflector Materials Experiment-III Ram/Wake (ORMatE-III R/W) tray and exposed to the LEO wake environment for 2.0 years. The nadir samples were silver-Teflon FEP radiator pieces taken from the MISSE 8 Single Events Upset Xilinx-Sandia Experiment II (SEUXSE II) Power Box and exposed to the LEO nadir environment for 2.14 years. The Teflon FEP flight materials were analyzed for changes in surface morphology and chemistry as compared to pristine control samples. The wake samples were also analyzed for changes in optical properties. There was no evidence of a molecular contamination layer present on the surface of the MISSE 8 wake or nadir facing Teflon FEP flight samples, although both the wake and nadir flight samples contained particulate contamination in some regions. The analyzed nadir particles were primarily zinc rich. The majority of analyzed wake particles were comprised of oxidized aluminum with small amounts of zinc and magnesium. The wake particles appear to have arrived early in the mission (or pre-flight) during a single event. This paper provides details of the MISSE 8 sample contamination analyses.

Erosion↗

NASA NTRS1970

Molecular sieves control contamination and and insulate in thermal regenerators - A concept

Zeolitic molecular sieves prolong the lives of cryogenic engines by preventing contamination of the thermal regenerators on the cold ends of closed-cycle engines. Sieves also serve as thermal insulators by preventing conduction of heat along regenerators through contiguous disks of mesh.

Gasser, M. G.↗