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NASA NTRS2007

Catalytic Ignition and Upstream Reaction Propagation in Monolith Reactors

Using numerical simulations, this work demonstrates a concept called back-end ignition for lighting-off and pre-heating a catalytic monolith in a power generation system. In this concept, a downstream heat source (e.g. a flame) or resistive heating in the downstream portion of the monolith initiates a localized catalytic reaction which subsequently propagates upstream and heats the entire monolith. The simulations used a transient numerical model of a single catalytic channel which characterizes the behavior of the entire monolith. The model treats both the gas and solid phases and includes detailed homogeneous and heterogeneous reactions. An important parameter in the model for back-end ignition is upstream heat conduction along the solid. The simulations used both dry and wet CO chemistry as a model fuel for the proof-of-concept calculations; the presence of water vapor can trigger homogenous reactions, provided that gas-phase temperatures are adequately high and there is sufficient fuel remaining after surface reactions. With sufficiently high inlet equivalence ratio, back-end ignition occurs using the thermophysical properties of both a ceramic and metal monolith (coated with platinum in both cases), with the heat-up times significantly faster for the metal monolith. For lower equivalence ratios, back-end ignition occurs without upstream propagation. Once light-off and propagation occur, the inlet equivalence ratio could be reduced significantly while still maintaining an ignited monolith as demonstrated by calculations using complete monolith heating.

Struk, Peter M.↗

NASA NTRS2019

Investigating Diurnal Changes in the Normal Albedo of the Lunar Surface at 1064 nm: A New Analysis with the Lunar Orbiter Laser Altimeter

The thermal environment of the lunar surface is extreme. At the equator, temperatures drop ~300 K between local noon and night. Laboratory studies demonstrate that minerals common to the lunar surface (e.g.,pyroxene, olivine) show spectral changes with respect to temperature in near infrared wavelengths. Over temperature changes equivalent to the lunar thermal environment (ΔT ≈ 300K), the reflectance of pure pyroxene samples can vary by a factor of two.

Deutsch, Ariel N.↗

NASA NTRS1985

Method for measuring surface activity of silicon nitride powder

Amorphous, alpha-, and beta-Si3N4 powders were activated by vibration ball milling in purified MeOH, and the surface activity of ground powders was determined by the temperature programmed desorption (TPD) method using NH3 gas. The concentration of active sites with a potential energy equivalent to the peak temperature in the spectrum increased was markedly by ball milling the amorphous Si3N4. The alpha- and beta-Si3N4 also had active sites produced by ball milling. The concentration of active site increased with increased ball milling time. A method for measuring surface activity of ceramic raw materials by TPD is proposed.

Kanno, Y.↗

NASA NTRS1990

Stratocumulus cloud height variations determined from surface and satellite observations

Determination of cloud-top heights from satellite-inferred cloud-top temperatures is a relatively straightforward procedure for a well-behaved troposphere. The assumption of a monotonically decreasing temperature with increasing altitude is commonly used to assign a height to a given cloud-top temperature. In the hybrid bispectral threshold method, or HBTM, Minnis et al. (1987) assume that the lapse rate for the troposphere is -6.5/Kkm and that the surface temperature which calibrated this lapse rate is the 24 hour mean of the observed or modeled clear-sky, equivalent blackbody temperature. The International Satellite Cloud Climatology Project (ISCCP) algorithm (Rossow et al., 1988) attempts a more realistic assignment of height by utilizing interpolations of analyzed temperature fields from the National Meteorological Center (NMC) to determine the temperature at a given level over the region of interest. Neither these nor other techniques have been tested to any useful extent. The First ISCCP Regional Experiment (FIRE) Intensive Field Observations (IFO) provide an excellent opportunity to assess satellite-derived cloud height results because of the availability of both direct and indirect cloud-top altitude data of known accuracy. The variations of cloud-top altitude during the Marine Stratocumulus IFO (MSIFO, June 29 to July 19, 1987) derived from surface, aircraft, and satellite data are examined.

Minnis, Patrick↗

NASA NTRS1994

Simulation of Tip-Sample Interaction in the Atomic Force Microscope

Recent simulations of the interaction between planar surfaces and model Atomic Force Microscope (AFM) tips have suggested that there are conditions under which the tip may become unstable and 'avalanche' toward the sample surface. Here we investigate via computer simulation the stability of a variety of model AFM tip configurations with respect to the avalanche transition for a number of fcc metals. We perform Monte-Carlo simulations at room temperature using the Equivalent Crystal Theory (ECT) of Smith and Banerjea. Results are compared with recent experimental results as well as with our earlier work on the avalanche of parallel planar surfaces. Our results on a model single-atom tip are in excellent agreement with recent experiments on tunneling through mechanically-controlled break junctions.

Good, Brian S.↗

NASA NTRS1983

Zenith angle effects in multichannel infrared sea surface remote sensing

Several approaches to infrared multichannel sea surface temperature retrievals propose using a universal set of constants. It is shown that the single-channel multiangle technique (i.e., GOES and NOAA) and the multichannel single-angle technique (NOAA-n) are similar concepts with a common derivation from radiative transfer theory. It is also shown that the linear correlation factor between surface temperature minus satellite temperature in one channel versus the difference in satellite temperatures in two channels is not independent of the difference in satellite sensed equivalent blackbody temperature. The 3.7-micron, 11-micron, and 12-micron channels on the NOAA-n AVHRR can be used in combination to compute atmospheric transmissivity and average atmospheric temperature, but a better combination would be substituting three 0.5-micron-wide channels centered on 11.25 micron, 11.75 micron, and 12.25 micron. A triple window multispectral scanner in the 11-12.5 micron region allows determination of diffuse surface reflectance which can bias sea surface temperatures - 0.4 K + or - 0.3 K.

Maul, G. A.↗

NASA NTRS1989

Surface composition of solid-rocket exhausted aluminum oxide particles

Particulate samples of aluminum oxide were collected on Teflon filters from the exhaust plume of the Space Shuttle (STS-61A, October 30, 1985) over the altitude interval 4.6-7.6 km immediately after launch. These particles were analyzed using SEM, energy-dispersive X-ray analysis, electron spectroscopy for chemical analysis, X-ray fluorescent spectroscopy, and conventional wet-chemical techniques. The samples were 0.6-1.0 percent surface-chlorided (chlorided meaning predominantly aluminum chlorides and oxychlorides, possibly including other adsorbed forms of chloride) by weight. This level of chloriding is about one-third of the amount determined previously from laboratory-prepared alumina and surface site samples of solid-rocket-produced alumina (SRPA) after both had been exposed to moist HCl vapor at temperatures down to ambient. This level is equivalent to previous laboratory results with samples exposed to moist HCl at temperatures above the boiling point of water. It is suggested that the present lower chloriding levels, determined for samples from a 'dry' Shuttle exhaust cloud, underscore the importance of a liquid water/hydrochloric acid phase in governing the extent of surface chloriding of SRPA. The reduced chloriding is not trivial with respect to potential physical/chemical modification of the SRPA particle surfaces and their corresponding interaction with the atmosphere.

Cofer, Wesley R., III↗

NASA NTRS2000

Galactic Noise and Passive Microwave Remote Sensing from Space at L-Band

The spectral window at L-band (1.4 GHz) is important for passive remote sensing of parameters such as soil moisture and ocean salinity best measured at long wavelengths. At L-band, radiation from extraterrestrial (galactic) sources is strong enough to warrant inclusion in calibration and retrieval algorithms and unlike the constant cosmic background is spatially variable. Previous estimates of the magnitude and distribution of this background radiation have been rather coarse, However, recent surveys of the radio sky at 1.4 GHz have made it possible to produce maps with sufficient spatial and radiometric accuracy to be relevant to remote sensing applications. This is of particular concern for remote sensing of sea surface salinity because the surface (water) is a good reflector and the salinity signal is relatively small. This paper presents a modem map of the radiometric sky at L-band and a solution to the problem of determining the portion of the sky seen by a radiometer in orbit. The data is derived from recent radio astronomy surveys and is presented as equivalent brightness temperature suitable for remote sensing applications. Examples using orbits and antennas representative of those contemplated for remote sensing of soil moisture and sea surface salinity from space are presented to illustrate the signal levels to be expected. Radiation near the galactic plane can exceed several kelvin.

LeVine, D. M.↗

NASA NTRS2019

Analyzing Machine Learning Predictions of Passive Microwave Brightness Temperature Spectral Difference Over Snow-Covered Terrain in High Mountain Asia

Snow is an important component of the terrestrial freshwater budget in high mountainAsia (HMA) and contributes to the runoff in Himalayan rivers through snowmelt. Despitethe importance of snow in HMA, considerable spatiotemporal uncertainty exists across the different estimates of snow water equivalent for this region. In order to better estimate snow water equivalent, radiative transfer models are often used in conjunction with microwave brightness temperature measurements. In this study, the efficacy of support vector machines (SVMs), a machine learning technique, to predict passive microwave brightness temperature spectral difference (1Tb) as a function of geophysical variables (snow water equivalent, snow depth, snow temperature, and snow density) is explored through a sensitivity analysis. The use of machine learning (as opposed to radiative transfer models) is a relatively new and novel approach for improving snow water equivalent estimates. The Noah-MP land surface model within the NASALand Information System framework is used to simulate the hydrologic cycle over HMA and model geophysical variables that are then used for SVM training. The SVMsserve as a nonlinear map between the geophysical space (modeled in Noah-MP) andthe observation space (1Tb as measured by the radiometer). Advanced MicrowaveScanning Radiometer-Earth Observing System measured passive microwave brightness temperatures over snow-covered locations in the HMA region are used as training data during the SVM training phase. Sensitivity of well-trained SVMs to each Noah-MP modeled state variable is assessed by computing normalized sensitivity coefficients. Sensitivity analysis results generally conform with the known first-order physics. Input states that increase volume scattering of microwave radiation, such as snow density and snow water equivalent, exhibit a plurality of positive normalized sensitivity coefficients. In general, snow temperature was the most sensitive input to the SVM predictions. The sensitivity of each state is location and time dependent. The signs of normalized sensitivity coefficients that indicate physical irrationality are ascribed to significant cross-correlation between Noah-MP simulated states and decreased SVM prediction capability at specific locations due to insufficient training data. SVM prediction pitfalls do exist that serve to highlight the limitations of this particular machine learning algorithm.

high mountain Asia↗

NASA NTRS1980

Microwave remote sensing of snowpacks

The interaction mechanisms responsible for the microwave backscattering and emission behavior of snow were investigated, and models were developed relating the backscattering coefficient (sigma) and apparent temperature (T) to the physical parameters of the snowpack. The microwave responses to snow wetness, snow water equivalent, snow surface roughness, and to diurnal variations were investigated. Snow wetness was shown to have an increasing effect with increasing frequency and angle of incidence for both active and passive cases. Increasing snow wetness was observed to decrease the magnitude sigma and increase T. Snow water equivalent was also observed to exhibit a significant influence sigma and T. Snow surface configuration (roughness) was observed to be significant only for wet snow surface conditions. Diurnal variations were as large as 15 dB for sigma at 35 GHz and 120 K for T at 37 GHz. Simple models for sigma and T of a snowpack scene were developed in terms of the most significant ground-truth parameters. The coefficients for these models were then evaluated; the fits to the sigma and T measurements were generally good. Finally, areas of needed additional observations were outlined and experiments were specified to further the understanding of the microwave-snowpack interaction mechanisms.

Stiles, W. H.↗

NASA NTRS1987

An analysis of the vertical structure equation for arbitrary thermal profiles

The vertical structure equation is a singular Sturm-Liouville problem whose eigenfunctions describe the vertical dependence of the normal modes of the primitive equations linearized about a given thermal profile. The eigenvalues give the equivalent depths of the modes. The spectrum of the vertical structure equation and the appropriateness of various upper boundary conditions, both for arbitrary thermal profiles were studied. The results depend critically upon whether or not the thermal profile is such that the basic state atmosphere is bounded. In the case of a bounded atmosphere it is shown that the spectrum is always totally discrete, regardless of details of the thermal profile. For the barotropic equivalent depth, which corresponds to the lowest eigen value, upper and lower bounds which depend only on the surface temperature and the atmosphere height were obtained. All eigenfunctions are bounded, but always have unbounded first derivatives. It was proved that the commonly invoked upper boundary condition that vertical velocity must vanish as pressure tends to zero, as well as a number of alternative conditions, is well posed. It was concluded that the vertical structure equation always has a totally discrete spectrum under the assumptions implicit in the primitive equations.

Cohn, Stephen E.↗

NASA NTRS1989

An analysis of the vertical structure equation for arbitrary thermal profiles

Cohn, Stephen E.↗

DOE OSTI2022

The miniJPAS survey: White dwarf science with 56 optical filters

We analyze the white dwarf population in miniJPAS, the first square degree observed with 56 medium-band, 145 Å in width optical filters by the Javalambre Physics of the accelerating Universe Astrophysical Survey (J-PAS), to provide a data-based forecast for the white dwarf science with low-resolution ($R$ ~ 50) photo-spectra. We define the sample of the bluest point-like sources in miniJPAS with $r$ < 21.5 mag, a point-like probability larger than 0.5, ($u$ - $r$)< 0.80 mag, and ($g$ - $i$)< 0.25 mag. This sample comprises 33 sources with spectroscopic information: 11 white dwarfs and 22 quasi-stellar objects (QSOs). We estimate the effective temperature ($T$ eff ), the surface gravity, and the composition of the white dwarf population by a Bayesian fitting to the observed photo-spectra. The miniJPAS data are sensitive to the Balmer series and the presence of polluting metals. Our results, combined with those from the Javalambre Photometric Local Universe Survey (J-PLUS) which has a lower spectral resolution but has already observed thousands of white dwarfs, suggest that J-PAS photometry would permit – down to $r$ ~ 21.5 mag and at least for sources with 7000 < $T$ eff < 22 000 K – both the classification of the observed white dwarfs into H-dominated and He-dominated with 99% confidence and the detection of calcium absorption for equivalent widths larger than 15 Å. The effective temperature is estimated with a 2% uncertainty, which is close to the 1% from spectroscopy. A precise estimation of the surface gravity depends on the available parallax information. In addition, the white dwarf population at $T$ eff > 7000 K can be segregated from the bluest extragalactic QSOs, providing a clean sample based on optical photometry alone. The J-PAS low-resolution photo-spectra would produce precise effective temperatures and atmospheric compositions for white dwarfs, complementing the data from Gaia. J-PAS will also detect and characterize new white dwarfs beyond the Gaia magnitude limit, providing faint candidates for spectroscopic follow-up.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2020

Millikelvin-resolved ambient thermography

Thermography detects surface temperature and subsurface thermal activity of an object based on the Stefan-Boltzmann law. Impacts of the technology would be more far-reaching with finer thermal sensitivity, called noise-equivalent differential temperature (NEDT). Existing efforts to advance NEDT are all focused on improving registration of radiation signals with better cameras, driving the number close to the end of the roadmap at 20 to 40 mK. In this work, we take a distinct approach of sensitizing surface radiation against minute temperature variation of the object. The emissivity of the thermal imaging sensitizer (TIS) rises abruptly at a preprogrammed temperature, driven by a metal-insulator transition in cooperation with photonic resonance in the structure. The NEDT is refined by over 15 times with the TIS to achieve single-digit millikelvin resolution near room temperature, empowering ambient thermography for a broad range of applications such as in operando electronics analysis and early cancer screening.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

NASA NTRS1995

Ames Research Center Mars/Pathfinder Heat Shield Design Verification ARC-JET Test

Design verification tests were performed on samples representing the aerobrake of the Mars/Pathfinder vehicle. The test specimens consisted of the SLA-561V ablator bonded to the honeycomb structure. The primary objective was to evaluate the ablation materials performance and to measure temperatures within the ablator, at the structural bondline and at the back sheet of the honeycomb structure. Other objectives were to evaluate the effect of ablative repair plug material treatment and voids in the heat shield. A total of 29 models were provided for testing in the Ames 60MW arc-jet facility. Of these, 23 models were flat-faced and six remaining models were curved edge ones, intended to simulate the conditions on the curved rim of the forebody where the maximum shear occurred. Eight sets of test conditions were used. The stagnation point heating rates varied from 47 to 240 W/cm2 and the stagnation pressures from 0.15 to 0.27 atm. (The maximum flight values are 132 W/cm2 and 0.25 atm) The majority of these runs were made at a nominal stagnation pressure of 0.25 atm. Two higher pressure runs were made to check the current (denser) ablation material for spallation, or other forms of thermal stress failure. Over 60% of the flatfaced models yielded good thermocouple data and all produced useful surface recession information. Of the five curved-edge models that were tested, only one gave good data; the remaining ones experienced model-holder failure. The test results can be summarized by noting that no failure of the ablative material was observed on any model. Also, the bondline temperature design limit of 250 C was never reached within an equivalent flight time despite a stagnation point heat load that exceeded the maximum flight value by up to 130%. At heating rates of over 200W/cm2 and stagnation pressures of 0.25 atm, or greater, the average surface recessions exceeded 0.5 cm on some models. The surface roughness increased dramatically at pressures above 0.25 atm and was four times greater at 0.27 atm than at 0.25 atm. Procured repair plug material performed much better than room-temperature cured plugs, as observed in the previous tests. Voids in the ablator did not increase local temperatures and gaps did not grow during testing.

Tran, Huy K.↗

DOE OSTI2023

Improving Performance of III-V Solar Cells Grown on Spalled Germanium with Ex Situ Substrate Planarization

Controlled spalling allows removal of devices and provides an opportunity for cost reduction through substrate reuse. However, the fracture-based process can leave behind morphological surface features, notably river lines, that can disrupt epitaxial growth and degrade device performance. We investigate the viability of various wet etch chemistries to planarize river lines to ensure high-quality device growth and performance without mechanical repolishing, and so maintain a route towards cost-effective reuse. Etching in a HF: HNO 3 :CH 3 COOH solution effectively planarizes river lines and produces a surface that yields devices with equivalent performance to those grown on epi-ready Ge wafer surfaces. Further studies will focus on optimizing etch composition, temperature, and time to minimize material removal while maintaining a suitable surface for high-quality epitaxy.

germanium↗

NASA NTRS1976

Accelerated test techniques for micro-circuits: Evaluation of high temperature (473 k - 573 K) accelerated life test techniques as effective microcircuit screening methods

The application of high temperature accelerated test techniques was shown to be an effective method of microcircuit defect screening. Comprehensive microcircuit evaluations and a series of high temperature (473 K to 573 K) life tests demonstrated that a freak or early failure population of surface contaminated devices could be completely screened in thirty two hours of test at an ambient temperature of 523 K. Equivalent screening at 398 K, as prescribed by current Military and NASA specifications, would have required in excess of 1,500 hours of test. All testing was accomplished with a Texas Instruments' 54L10, low power triple-3 input NAND gate manufactured with a titanium- tungsten (Ti-W), Gold (Au) metallization system. A number of design and/or manufacturing anomalies were also noted with the Ti-W, Au metallization system. Further study of the exact nature and cause(s) of these anomalies is recommended prior to the use of microcircuits with Ti-W, Au metallization in long life/high reliability applications. Photomicrographs of tested circuits are included.

Johnson, G. M.↗

NASA NTRS1976

Acceleration of fatigue tests for built-up titanium components

A study was made of the feasibility of a room-temperature scheme of accelerating fatigue tests for Mach 3 advanced supersonic transport aircraft. The test scheme used equivalent room-temperature cycles calculated for supersonic flight conditions. Verification tests were conducted using specimens representing titanium wing lower surface structure. Test-acceleration parameters were developed for the test with an auxiliary test set. Five specimens were tested with a flight-by-flight load and temperature spectrum to simulate typical Mach 3 operation. Two additional sets of five specimens were tested at room temperature to evaluate the test-acceleration scheme. The fatigue behavior of the specimens generally correlated well with the proposed correction method.

Watanabe, R. T.↗