Radioisotope and radiation techniques for terrestrial and planetary gas and solid measurements.
Radioisotope and radiation techniques for terrestrial and planetary gas and solid measurements
RADIATION MEASUREMENT↗
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The UHURU X-ray instrument.
On Dec. 12, 1970, the UHURU X-ray observatory was launched into equatorial orbit with the prime mission of conducting an all-sky survey of astronomical X-ray sources with intensities of 0.00005 Sco-X1 or greater. The X-ray detection system contains 12 gas-filled proportional counters, 6 behind each collimator. The aspect system is discussed together with the structure, the pulse height analyzer, the command system, the calibration system, and the power distribution system. Pulse shape discrimination circuits used on UHURU use the same technique that was used on the system originally developed for large area proportional counters described by Gorenstein and Mickiewicz (1968).
Jagoda, N.↗
Apollo 6, Anomaly Report No. 6: Abnormal Structural Performance During Launch Phase
Approximately 2 minutes 13 seconds after lift-off of the Apollo 6 mission, abrupt changes of strain, vibration, and acceleration measurements were indicated in the S-IVB, instrument unit, adapter, lunar module, and command and service modules; photographs showed objects coming from the area of the adapter. The adapter, however, continued to sustain the required loads with no impairment of the mission. The investigation was first focused upon the understanding of the coupled vibration modes and characteristics of the launch vehicle and spacecraft.' Extensive test programs were conducted. It was eventually concluded that the adapter failure was not caused by vibration. Extensive study of the airborne photography and other evidence indicated that a large area of the adapter had lost inner facesheet from the honeycomb sandwich panels. Loads and stresses resulting from vibration were determined to be insufficient to initiate such a failure. The investigation was then directed toward determining the range of pressures that could have been trapped in the Apollo 6 adapter sandwich panels, and toward determining the tolerance of the panels to withstand pressure with various degrees of flaws such as adhesive voids and facesheet dents. The degradation effects of moisture and heat exposure on the adhesive strength were also studied and tested. These tests and analyses led to the conclusion that pressure internal to the sandwich panels could have caused the failure, if a large flaw existed. The pressure buildup would have been caused by aerodynamic heating effects on air and moisture trapped in the panel. The probable cause of the failure was found in the original ultrasonic inspection scan record of the affected adapter panel. In the center of the region where the adapter failed, horizontally along the station 709 panel splice, the record contained two thick anomalous lines extending several feet. Without an X-ray record of this region, the significance of this particular scan record cannot be fully understood. However, since all other evidence had indicated that the adhesive had to be weakened in a rather large area to initiate the failure, the investigation was focused intently upon the station 709 splices of other adapters. Sufficient information was developed to verify that deficient assembly techniques have consistently resulted in abnormalities in the structure at this station. These abnormalities were identified in adapters 12, 13, 14, 15, and 16. Before the splice abnormalities were pinpointed, corrective action was taken to reduce pressure "buildup in the honeycomb panels and to reduce heat degrading effects on the adhesive. This was done by drilling vent holes in the inner facesheet and covering the outer facesheet with cork. The adapters having identified abnormalities in the station 709 splice are being repaired, and the contractor is investigating ways of avoiding these -abnormalities in panels yet to be bonded.
Source record↗
Quantitative simultaneous multi-element microprobe analysis using combined wavelength and energy dispersive systems
A combined WDS-EDS system obviates the severe X-ray peak overlap problems encountered with Na, Mg, Al and Si common to pure EDS systems. By application of easily measured empirical correction factors for pulse pile-up and peak overlaps which are normally observed in the analysis of silicate minerals, the accuracy of analysis is comparable with that expected for WDS electron microprobe analyses. The continuum backgrounds are subtracted for the spectra by a spline fitting technique based on integrated intensities between the peaks. The preprocessed data are then reduced to chemical analyses by existing data reduction programs.
Walter, L. S.↗
Quantitative X-ray diffraction analysis of oxides formed on superalloys
Methods were developed for quantitative analysis by X-ray diffraction of the oxides Al2O3, NiO, Cr2O3, CoO, and CoCr2O4 within a standard deviation of about 10 percent of the weight fraction reported or within 1 percent absolute. These error limits assume that the sample oxides are well characterized and that the physiochemical structure of the oxides in the samples are identical with those in the synthesized standards. Results are given for the use of one of the techniques in the analysis of spalls from a series of oxidation tests of the cobalt base alloy WI-52.
Garlick, R. G.↗
Investigation of solidification in zero-gravity environment; M553 sphere forming experiment. Phase C: Evaluation of Skylab specimens
Results on specimen evaluation and discussion of solidification behavior in each case are reported in the following order: (1) specimen SL-1.6, (2) specimen SL-2.8, (3) specimen SL-2.4, (4) specimen SL-1.10 and (5) specimen SL-1.11. Comparison is made with ground-processed specimens of similar composition, whenever pertinent and meaningful. Among the nondestructive evaluation methods the measurement of sphericity was conducted by micrometric and shadowgraphic techniques. The intricate shape of specimens in some cases appeared difficult to define. In measuring the density, liquid penetration inside cavities that outcrop on the surface was avoided by sealing off these cavities. Among the destructive evaluation methods the use of the Quantimet 720 required particular attention, because of the small difference in contrast between second phases and micropores. With regard to microporosity microvoids in the core of some specimens were so fine that X-ray microradiography had to be used.
Kattamis, T. Z.↗
Thermal Inspection for the Assessment of Adhesively Bonded Metal Adherends
Certification of adhesively bonded structures is currently a challenge for aircraft manufacturers. The ability to certify bonds in primary structure can reduce dependence on fasteners and this will enable more efficient manufacturing. For example, drilling holes and installing fasteners in bonded joints can be a potentially significant bottleneck in airframe manufacturing. In addition, fasteners increase the airframe weight and can add stress concentration areas. Reducing fastener count can accelerate manufacturing and improve aircraft performance. NASA is currently investigating nondestructive evaluation (NDE) techniques to assess bond integrity. For example, bond thickness influences bond strength and therefore NDE techniques are being investigated to determine bond thickness. For bonded metal structures, there is a large difference in the thermal diffusivity between the 7075 aluminum alloy metal adherends and aircraft grade adhesive. Multi-layered thermal models show a large variation in the thermal response for bondline adhesive thicknesses that vary from 100 to 300 microns for adherend thicknesses of 0.163 cm. Experimental through-transmission thermal measurements reveal promise to quantitatively characterize the bondline thickness. Results were validated with X-ray computed tomography and optical microscopy measurements, and influence of porosity on the thermal model and measurements are investigated.
X-ray computed tomography↗
Thermal Inspection for the Assessment of Adhesively Bonded Metal Adherents
Certification of adhesively bonded structures is currently a challenge for aircraft manufacturers. The ability to certify bonds in primary structure can reduce dependence on fasteners and this will enable more efficient manufacturing. For example, drilling holes and installing fasteners in bonded joints can be a potentially significant bottleneck in airframe manufacturing. In addition, fasteners increase the airframe weight and can add stress concentration areas. Reducing fastener count can accelerate manufacturing and improve aircraft performance. NASA is currently investigating nondestructive evaluation (NDE) techniques to assess bond integrity. For example, bond thickness influences bond strength and therefore NDE techniques are being investigated to determine bond thickness. For bonded metal structures, there is a large difference in the thermal diffusivity between the 7075 aluminum alloy metal adherends and aircraft grade adhesive. Multi-layered thermal models show a large variation in the thermal response for bondline adhesive thicknesses that vary from 100 to 300 microns for adherend thicknesses of 0.163 cm. Experimental through-transmission thermal measurements reveal promise to quantitatively characterize the bondline thickness. Results were validated with X-ray computed tomography and optical microscopy measurements, and influence of porosity on the thermal model and measurements are investigated.
bondline thickness↗
Evaluation and optimization of the advanced signal counting techniques on weldments
The signal counting technique with the Delta ultrasonic method is evaluated and optimized for flaw detection in aluminum welds. A comparison is made between the counting and conventional amplitude-gate methods to detect flaws. No conclusion is drawn on the sensitivity of these two methods to detect flaws when the mismatch at the welds is small (25 mils or less). When the mismatch is 25 mils or more, the signal counting method is more sensitive. Of the 24 welded specimens, 50 flaws were found by X-ray inspection and 59 by the Delta method. On 1/4-inch thick welds, X-ray is equal to or slightly more sensitive than Delta method, but on the 1/2-inch thick welds Delta ultrasonic appears more sensitive in flaw detection.
Yee, B. G. W.↗
Catalysis study for space shuttle vehicle thermal protection systems
Experimental results on the problem of reducing aerodynamic heating on space shuttle orbiter surfaces are presented. Data include: (1) development of a laboratory flow reactor technique for measuring gamma sub O and gamma sub N on candidate materials at surfaces, T sub w, in the nominal range 1000 to 2000, (2) measurements of gamma sub O and gamma sub N above 1000 K for both the glass coating of a reusable surface insulation material and the siliconized surface of a reinforced pyrolyzed plastic material, (3) measurement of the ablation behavior of the coated RPP material at T sub w is greater than or equal to 2150 K, (4) X-ray photoelectron spectral studies of the chemical constituents on these surfaces before and after dissociated gas exposure, (5) scanning electron micrograph examination of as-received and reacted specimens, and (6) development and exploitation of a method of predicting the aerodynamic heating consquences of these gamma sub O(T sub w) and gamma sub N(T sub w) measurements for critical locations on a radiation cooled orbiter vehicle.
Breen, J.↗
X-ray analysis of fatigue damage in copper
A Warren-Averbach x-ray line profile analysis was applied to, broadened x-ray diffraction peaks from copper deformed in fatigue. The copper specimens were fatigued by four point bending at various strain amplitudes, and measurements were made at various fractions of the total fatigue life. The analysis results in an estimation of 1) an average coherently diffracting domain size in a direction normal to the diffracting planes; and 2) a strain distribution function. The strain distribution function is in terms of the root mean square strain, <ϵ^(2)> where ϵ is averaged over a given distance at all points in the diffracting crystals. This rms strain is expressed as a function of averaging distance for a direction normal to the diffracting planes. The rms strains were found to be a function of the fatigue strain amplitude level, increasing with amplitude and reaching a maximum limiting value during the first 2% of the fatigue life. The strains were normally larger in the 4lO0 direction compared to the <111> direction and the absolute values were quite small. These results may be explained by assuming the dislocations are present in the form of dipoles because the lattice strain around a dipole is much less than around single dislocations. Conclusions arrived at in this analysis are in agreement with current theories of fatigue damage in metals. The result that maximum hardening is achieved during the initial few percent of the fatigue life is confirmed by many other investigators using entirely different analytical techniques. It is felt that the structure of the material is changing during this initial hardening stage to an eventual steady state characteristic of the testing conditions. A unique substructure is developed which thereafter persists, and the remainder of the fatigue test is taken up by crack propagation through this substructure until ultimate failure occurs by fracture. The formation of this steady state structure is dependent on the maximum fatigue strain amplitude and on the frequency and temperature of cycling for a particular material.
COPPER↗
Residual Stress Analysis of Overspeeded Disk with Central Hole by X-ray Diffraction
An X-ray - diffraction analysis of residual surface stresses after plastic strain was introduced in a parallel-sided 3S-O aluminum disk with a central hole by two types of centrifugal overspeed is reported. Both tangential and radial stresses were generally tensile with large local variations near the hole where surface stresses may have been partly superficial. These stresses were both tensile and compressive dependent on the distance from the disk center when mass compression was effected near the hole.
ALUMINUM↗
X-ray film holder permits single continuous picture of tubing joint
X ray technique produces a clear continuous picture of a welded brazed tubing joint on a single film with one exposure. A stationary X ray source located in the plane of the joint to be inspected, a means of rotating the tube, and a unique internal film holder and positioning fixture are used.
Diamond, J. W.↗
Some observational aspects of X-ray astronomy.
X ray astronomy observation techniques and apparatus noting detectors, data analysis problems for rocket observations and Crab Nebula, galactic and background radiation
Clark, G.↗
Grazing-incidence telescopes for X-ray astronomy.
Grazing incidence telescopes for X ray astronomy, describing mirrors, detection systems and dispersion techniques
Giacconi, R.↗
Electron paramagnetic resonance study of chromium/+3/ in X-ray irradiated ruby
Increase of chromium/+3/ concentration in X ray irradiated ruby during isothermal annealings measured by EPR technique
Liu, D. C.↗
Measurement of the degree of anisotropy of the cosmic radiation using the IMP space vehicle
The detector and data reduction techniques used in connection with the cosmic ray experiments designed for and flown on Explorer 34 and 41 satellites are described. A history of the program development and the present status of data processing are briefly summarized. The instrument to measure the anisotropy and energy spectra of cosmic ray electrons and protons, and X-rays of solar and galactic origin is discussed. The main characteristics of the detectors and the stability during 23 months of operation are described. The method of analysis of the angular distribution of solar cosmic ray particles in the ecliptic plane is given. It is shown that the anisotropy of low energy particles of solar origin decreases sharply to a very small value when the satellite penetrates the magnetosphere.
Palmeira, R. A. R.↗
The use of magnetometers on balloon-borne X-ray astronomy experiments.
The use of magnetometers for azimuth determination of balloon-borne X-ray astronomy payloads is examined, with special emphasis placed on the experiments of the University of Adelaide Cosmic Ray Group. A critical evaluation is made of the effectiveness of the magnetometers, including discussion of effects due to geomagnetic field variations, magnetometer misorientation and spurious contaminant magnetic fields. Calibration techniques and details of in-flight performance are also presented.
Thomas, R. M.↗