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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,171 records · Page 65
All sourcesNASA NTRSDOE OSTI
NASA NTRSDate not supplied

On-chip Broadband Load Calibrators for Characterizing Transition-Edge Sensor Bolometers

We describe the design and fabrication of on-chip broadband load calibrators for element-by- element and full circuit characterization of transition-edge sensor (TES) bolometers for cosmic microwave background (CMB) polarimetry. Fabricated in a 4 X 4 grid on a 100 mm silicon wafer, the chips allow systematic testing of individual detector circuit elements without the need for an external blackbody source. This in-situ testing approach provides rapid and efficient characterization of various pixel designs in order to optimize the optical efficiency and control of systematic effects of the detectors. In this work, we demonstrate the on-chip calibrators on the Cosmology Large Angular Scale Surveyor (CLASS) W-band pixels. In particular, we investigate the loss on microstrip transmission lines and measure the performance of various designs of TESs, magic-tees, via-less crossovers, and signal terminations. We also test a filter-bank spectrometer with eight resonators spanning 80 – 105 GHz to characterize the spectral response of circuit elements across the detector bandwidth.

Sumit Dahal↗
NASA NTRS2023

New Mie Scattering Diffuse Targets Development and Characterization

Earth science remote sensing observations require the detection and measurement of light originating from bright targets, such as clouds, and darker targets, such as an open ocean. This requirement drives the need to design, develop, and characterize improved calibration targets in support of current and future NASA instruments. New diffuse targets to be used as spectral albedo calibration standards were developed and characterized. The new targets based on fused silica or/and pressed and sintered Polytetrafluoroethylene (PTFE) were developed to be Earth scene specific. The various reflectance levels are achieved by modifying the material parameters, thickness, and surface finish. The new targets were characterized in laboratory and simulated space environments. We acquired high accuracy reflectance and transmittance data using a precision optical scatterometer and spectrophotometer located in the NASA Goddard Space Flight Center (GSFC) Diffuser Calibration Lab. The Total hemispherical reflectance (THR) and Bidirectional Reflectance Distribution Function (BRDF) were measured over the range of solar incident and scattered elevation and azimuthal angles typically realized on orbit by remote sensing instruments. We intend to space certify the new calibration targets after concluding on-orbit testing on the International Space Stations (ISS) scheduled for the second half of 2023.

Georgi Georgiev↗
NASA NTRSDate not supplied

Characterization of Fluorescence Signals in Synthetic Anorthite

In-situ resource utilization (ISRU) is a key capability to enable a long term presence on the Moon and other planetary bodies. For example, efforts have been underway to develop processes to utilize the lunar regolith to produce building materials and extract useful resources. In processes that utilize the regolith directly to produce construction materials, such as in various sintering methods, characterizing the composition of the regolith is important as the composition can affect the optimal process parame-ters. In processes that involve extracting resources such as iron, oxygen, hydrogen, etc., identifying areas with higher abundance of a particular resource will be critical since different regions of the Moon exhibit differing regolith composition. To this end, Ra-man is one technique that can rapidly characterize the mineralogy of rock samples. This technique has al-ready been deployed on Mars to detect various miner-als including olivine, carbonates, phosphates, etc. Besides characterizing the mineralogy, Raman spectra often contain unwanted fluorescence signals that can mask Raman peaks. In some cases, the fluorescence signals are narrow enough to aid in the identification of specific elements in soils. In this work, we explore fluorescence peaks in a synthetic anorthite sample, which are at the same position as Ruby fluorescence peaks attributed to chromium. These fluorescence peaks, as well as similar fluorescence peaks attributed to other elements, could have important implications for ISRU and the mining of critical resources as has been previously described.

Raman Spectroscopy↗
NASA NTRSDate not supplied

Analysis of Crack Propagation Transients in Accelerated Fatigue Characterization of Adhesives

The characterization of the rates of crack propagation by means of a Paris law is intended for steady-state fatigue conditions. While rates of crack propagation are primarily driven by 𝐽𝐽𝑚𝑚𝑚𝑚𝑚𝑚, in the presence of evolving process zones and fiber bridging they also depend on the crack propagation length: cracks with fully formed process zones propagate more slowly. Analyses of the rates of crack propagation in laminates secondarily bonded with AF163-2K film adhesive were conducted to identify the rate transients that occur during the formation of the process zone in the adhesive and during the evolution of bridging of the adhesive’s carrier knit across the crack faces. Dávila's CF22 cohesive fatigue damage model was used in finite element analyses of the double cantilever beam test to explain discrepancies in experimental rates of propagation obtained from tests conducted with either increasing or decreasing 𝐽max. The results indicate that the analyses accurately reproduce transient and steady-state rates of propagation observed in the experimental results, as well as the threshold of propagation. Transient rates of propagation always exceed those in steady state, which underscores the need to understand transients and account for them in fatigue characterization. The results also highlight that a Paris curve for steady-state propagation can be obtained most quickly using a decreasing load function, but that this curve consists of an unconservative bound to the rates of propagation. A lateral shift in the Paris curve is proposed for a conservative characterization that removes the effect of bridging and other R-curve effects.

fracture mechanics; delamination; J-integral↗
NASA NTRS2024

Advanced Libya-4 radiometric and atmospheric characterization utilizing MODIS and VIIRS full-scan reflective solar band measurements

The NASA Clouds and the Earth's Radiant Energy System (CERES) project provides observed flux and cloud products to the climate science community. The CERES instruments, along with the MODIS and VIIRS imagers, are onboard the Terra, Aqua, NPP, and NOAA20 satellites. In order to produce seamless multi-platform integrated products, long-term sensor stability and inter-calibration are required. Inter-calibration between sensors within the same sun-synchronous orbit relies on Earth invariant targets because simultaneous nadir overpasses are not possible. To facilitate inter-calibration efforts, the CERES Imager and Geostationary Calibration Group (IGCG) has improved the Libya-4 target characterization. Improvements include full scan angle characterization to enable daily observations, clear-sky identification using individual scan angle dynamic spatial homogeneity thresholds, and atmospheric corrections. The water vapor correction was found to be effective across the full scan, whereas the ozone and aerosol corrections were less effective. The atmospheric-corrected normalized radiance temporal fluctuations are similar across scan angles, spectral bands, and between the MODIS and VIIRS imagers, suggesting that the fluctuations are a result of the natural variability of the Libya-4 surface reflectance. The Libya-4 surface variability is more than likely caused by changes in the prevailing winds that alter sand dune orientation and resulting shadows. The full-scan-imager atmosphere and angle corrected reflected solar band radiance trend standard errors are between 0.6% and 1.0%, and for near-nadir observations, are between 0.5% and 0.8%. The advanced characterization suggests that the Libya-4 short-term surface reflectance anomalies may need to be considered for imager stability monitoring and inter-calibration efforts.

Libya-4 Pseudo-invariant Calibration Site↗
NASA NTRSDate not supplied

Science Applications From NAST-I Measurements: PBL Thermodynamic Characterization and Variation

The National Airborne Sounder Testbed-Interferometer (NAST‑I) suborbital system serves as a spaceborne instrument simulator and pathfinder for future satellite capabilities and airborne science experiments. The NAST‑I measurements are made to advance understanding of science critical for weather, climate, chemistry, and radiation applications. NAST‑I provides high-spatial linear resolution equal to 13% of the aircraft altitude at nadir, and high-spectral resolution (0.25 cm -1 ) measurements within the spectral region of 645–2700 cm ‑1 . NAST-I measurements and corresponding geophysical retrievals and their potential benefits toward improved atmospheric state and composition characterizations needed for air quality, wildfire, and other science applications have been published in many Peer-reviewed papers. NAST-I capabilities could be of particular importance toward enhancing characterization and understanding of the Planetary Boundary Layer (PBL). Initial results of PBL thermodynamic characterization and variation with its time evolution from NAST-I measurements will also be presented.

PBL↗
NASA NTRSDate not supplied

Analysis of Crack Propagation Transients in Accelerated Fatigue Characterization of Adhesives

The characterization of the rates of crack propagation by means of a Paris law is intended for steady-state fatigue conditions. While rates of crack propagation are primarily driven by 𝐽𝐽𝑚𝑚𝑚𝑚𝑚𝑚, in the presence of evolving process zones and fiber bridging they also depend on the crack propagation length: cracks with fully formed process zones propagate more slowly. Analyses of the rates of crack propagation in laminates secondarily bonded with AF163-2K film adhesive were conducted to identify the rate transients that occur during the formation of the process zone in the adhesive and during the evolution of bridging of the adhesive’s carrier knit across the crack faces. Dávila's CF22 cohesive fatigue damage model was used in finite element analyses of the double cantilever beam test to explain discrepancies in experimental rates of propagation obtained from tests conducted with either increasing or decreasing 𝐽max. The results indicate that the analyses accurately reproduce transient and steady-state rates of propagation observed in the experimental results, as well as the threshold of propagation. Transient rates of propagation always exceed those in steady state, which underscores the need to understand transients and account for them in fatigue characterization. The results also highlight that a Paris curve for steady-state propagation can be obtained most quickly using a decreasing load function, but that this curve consists of an unconservative bound to the rates of propagation. A lateral shift in the Paris curve is proposed for a conservative characterization that removes the effect of bridging and other R-curve effects.

fracture mechanics; delamination; J-integral↗
NASA NTRSDate not supplied

PBL Thermodynamic Characterization and Its Variability From NAST-I During the Wh2yMSIE Field Campaign

The National Airborne Sounder Testbed-Interferometer (NAST‑I) suborbital system (<2.6 km IFOV; 0.25 cm-1 within 645–2700 cm‑1) serves as a spaceborne instrument simulator and pathfinder for future satellite capabilities and airborne science experiments. The NAST‑I measurements are made to advance understanding of science critical for weather, climate, chemistry, and radiation applications. Here we present some groundbreaking capabilities of NAST-I measurements and corresponding geophysical retrievals and their potential benefits toward improved atmospheric state and composition characterizations needed for science applications of particular importance toward enhancing characterization and understanding of the Planetary Boundary Layer (PBL). Initial results of PBL height estimation and thermodynamic characterization and their time evolution from NAST-I measurements during the WH2yMSIE field campaign are presented.

Daniel K Zhou↗
NASA NTRS2026

Polarized Resonant Soft X-ray Scattering (P-RSoXS) as a New Technique for Characterizing Amorphous Astromaterials

In the coming years, samples will be returned from several asteroids, the lunar surface, and the first material returned directly from the Martian surface. Previous in-situ and remote studies indicate these samples will contain abundant amorphous or weakly crystalline materials. However, detailed characterization and quantification of these amorphous materials remains challenging. Conventional techniques, including electron microscopy and X-ray diffraction, provide important information on material structure, but are generally limited to crystalline materials. Polarized resonant soft X-ray scattering (P-RSoXS) is a synchrotron-based X-ray scattering technique that has been used to characterize and quantify weakly crystalline systems, including soft materials. This research aims to translate this technique to geologic and extraterrestrial materials, building off the knowledge of using P-RSoXS to interrogate soft materials. P-RSoXS is well-suited to interrogate geologic materials, which are often multiphase, heterogeneous systems with crystalline and amorphous components, and domain sizes on the order of tens of nanometers. It is anticipated that future work will help reveal new chemical and structural information in geologic materials. Maturation of this preliminary work to develop P-RSoXS to characterize astromaterial-relevant samples will provide new understanding of the secondary processes responsible for the development of amorphous astromaterials and further elucidate our knowledge of the geologic history and past alteration processes.

Joshua H Litofsky↗
DOE OSTI2018

Support for Fuel Fabrication and Characterization

Oak Ridge National Laboratory (ORNL) has participated in the Advanced Gas Reactor (AGR) program for the Next Generation Nuclear Plant (NGNP) and the transition to the Idaho National Laboratory (INL) Advanced Reactor Technologies (ART) Technology Development Office (TDO) since the inception of the program. In this effort, ORNL has fabricated tristructural isotropic (TRISO) fuel and fuel compacts for AGR-1, AGR-2, and AGR-3/4 experiments, provided matrix only components for AGC-2, AGC-4, and AGR 3/4 experiments and for university studies, and provided characterization, coating, and compaction support for INL and BWX Technologies Nuclear Operations Group (BWXT). In fiscal year (FY) 2017, the activities for the INL ART TDO fuel development are focused on preparations for the AGR-5/6/7 experiments and technical support to the Generation-IV International Forum (GIF) pre-irradiation leach-burn-leach (LBL) round robin effort with China and South Korea. With the successful transfer of fuel fabrication technology to BWXT, ORNL’s involvement has shifted toward transferring fuel characterization methods, providing technical support, verification of BWXT laboratory results, and fabricating surrogate fuel materials for university collaborations. ORNL will also provide analytical support to BWXT and INL for uranium dispersion analysis and confirmatory fuel characterization analyses as needed.

+↗
DOE OSTI2018

Collab Fracture Characterization: Preliminary Results from the Modeling and Flow Testing of Experiment 1

The EGS Collab project is developing ~10-20 m-scale field sites where fracture stimulation and flow models can be validated against controlled, small-scale, in-situ experiments. At the first experimental site, a hydraulic fracture will be created in metamorphic rock at the 4850 level in the former Homestake Mine. The experimental concept is for fracturing to be initiated at an injection well and continue until it intersects a production well approximately 10 meters away. Initial step-pressure flow testing of the fracture are to be performed to describe pressure-aperture-flow relationships. The flow field between the injector and producer boreholes will be characterized using a series of forced gradient dipole tracer tests. A number of fracture characterization models have been used to assist in the design of the tracer tests. The tracer test program will use conservative, sorbing, and particulate tracers, as well as sampling for radon gas to describe the fracture surface area (i.e., potential heat transfer area), flow pathway distribution, and volume. Tracer concentration at the production well (i.e. break through curves) will be measured using a series of inline sensors, liquid sampling devices, filtering of the effluent, and the measuring of gas concentrations in the effluent. Tracer monitoring data will be compared against results from a collection of numerical simulators developed at U.S. national laboratories and universities for the purpose of validating these flow and transport models. Ultimately these same models will be used to predict the heat transfer characteristics of the fracture and will be compared to a thermal characterization field test where cold water will be injected at the injection well and the temperature will be measured at the production well. This paper discusses the early tracer transport model predictions and parameters sensitivity that affect the tracer breakthrough curves at the production well.

15 GEOTHERMAL ENERGY↗
DOE OSTI2019

Impedance Characterization of Utility-Scale Renewable Energy and Storage Systems: Preprint

This paper presents the impedance characterization of utility-scale wind turbines and PV/storage inverters using a multimegawatt grid simulator-based grid integration testbed. The paper describes testbed components including a 7 MVA grid simulator, 5 MW dynamometer, medium-voltage measurement system, and real-time control system used for automated impedance characterization of wind turbines and inverters. Different aspects of impedance measurement are discussed, including the selection of the magnitude and type of perturbation, measurement of frequency cross-coupling between sequence impedance responses, and the alignment of the reference frame for sequence impedance measurement. The paper also demonstrates high-fidelity validation of EMT simulation models and characterization of grid-forming inverters using impedance measurements.

17 WIND ENERGY↗
DOE OSTI2018

Support for Fuel Fabrication and Characterization

Oak Ridge National Laboratory (ORNL) has participated in the Advanced Gas Reactor (AGR) program for the Next Generation Nuclear Plant (NGNP) and the transition to the Idaho National Laboratory (INL) Advanced Reactor Technologies (ART) Technology Development Office (TDO) since the inception of the program. In this effort, ORNL has fabricated tristructural isotropic (TRISO) fuel and fuel compacts for AGR-1, AGR-2, and AGR-3/4 experiments, provided matrix only components for AGC-2, AGC-4, and AGR 3/4 experiments and for university studies, and provided characterization, coating, and compaction support for INL and BWX Technologies Nuclear Operations Group (BWXT). In fiscal year (FY) 2017, the activities for the INL ART TDO fuel development are focused on preparations for the AGR-5/6/7 experiments and technical support to the Generation IV (GenIV) pre-irradiation leach-burn-leach round robin effort with China and South Korea. With the successful transfer of fuel fabrication technology to BWXT, ORNL’s involvement has shifted toward transferring fuel characterization methods, providing technical support, verification of BWXT laboratory results, and fabricating surrogate fuel materials for university collaborations. ORNL will also provide analytical support to BWXT and INL for uranium dispersion analysis and confirmatory fuel characterization analyses as needed.

+↗
DOE OSTI2019

EGS Collab Project Electrical Resistivity Tomography Characterization and Monitoring

The EGS (Enhanced Geothermal Systems) Collab project is performing stimulation experiments in highly monitored and well-characterized intermediate-scale (~10-20 m) field test beds. The characterization and monitoring system includes an array of electrodes grouted in place within six monitoring wells, with 16 electrodes per well. The electrodes enable characterization of the 3D low-frequency electrical properties of the host rock, and changes in those properties during stimulation and tracer testing using both static and time-lapse Electrical Resistivity Tomography. In this talk we present: 1) ERT array design and installation, 2) baseline (pre-stimulation) imaging results, 3) time-lapse data collected during stimulation operations, and 4) real-time imaging during clean water injections intended to illuminate flow paths as a decrease in bulk electrical conductivity. We will also discuss aspects and lessons learned for conducting ERT imaging operations in the presence of high fluid pressure gradients during stimulation and flow operations. Results to date reveal a highly heterogeneous rock fabric, ranging over four orders of magnitude in bulk electrical conductivity, and high polarization capacity. Baseline imaging results are consistent with borehole logs and core studies. Time-lapse imaging results to identify major flow paths during tracer studies are forthcoming and will be discussed during this presentation. Ultimately the ERT imaging data sets provide useful information for validating and verifying model predictions in preparation for research at DOE’s Frontier Observatory for Research in Geothermal Energy (FORGE).

electrical resistivity tomography, geophysics, geo↗
DOE OSTI2017

Support for INL ART TDO Advanced Gas Reactor Fuel Fabrication and Characterization

Oak Ridge National Laboratory (ORNL) has participated in the Advanced Gas Reactor (AGR) program for the Next Generation Nuclear Plant (NGNP) since the inception of the program. In this effort, ORNL has fabricated tri-structural isotropic (TRISO) fuel and fuel compacts for AGR-1, AGR-2, and AGR-3/4 experiments, provided matrix only components for AGC-2 and AGR-3/4 experiments and for university studies, and provided characterization, coating, and compaction support for Babcock and Wilcox (B&W). In FY 2017, the activities for the Very-High Temperature Reactor (VHTR) Technology Development Office (TDO) fuel development are focused on preparations for the AGR-5/6/7 experiments. With the successful transfer of fuel fabrication technology to B&W, ORNL’s involvement has shifted toward transferring fuel characterization methods, providing support for fabricating surrogate fuel materials international collaborations. ORNL will also provide analytical support to B&W for uranium dispersion analysis and confirmatory fuel characterization analyses as needed.

+↗
DOE OSTI2019

Characterization of a Fast-Framing X-Ray Camera With Wide Dynamic Range for High-Energy Imaging

We present first characterization results, with a focus on high-flux measurements, of a fast-framing, wide-dynamic-range x-ray camera intended for high-energy imaging. The MM-PAD-2.1 uses an integrating pixel front-end with a charge removal architecture and in-pixel counter to extend the pixel well depth while maintaining low read noise across the full dynamic range. The charge-removal mechanism is dead-time-less (i.e., incoming signal continues to be integrated by the front-end while charge removal is taking place). The purpose of the highflux characterization was to determine the maximum sustained incident flux that could be measured while still exhibiting linear behavior. To this end, a 16 x 16 pixel prototype was tested at the Advanced Photon Source at Argonne National Laboratory using 10 keV photons generated by an undulator source. The intensity of the incident beam was varied over 3 orders of magnitude using a series of attenuators, and the signal integrated by the MM-PAD-2.1 prototype was compared to that measured by a He-filled ion chamber directly upstream. Initial results indicate linear performance up to ca. 10(10) ph/s in a spot spanning approximately 2 x 1.5 pixels (FWHM). The onset of transient radiation damage was observed during these measurements, characterized primarily by failure of digital readout from the detector ASIC. These effects were observed to reverse after annealing at 30 degrees C for several hours, with full recovery of the detector readout.

Shanks, Katherine S.↗
DOE OSTI2021

BETO 2021 Peer Review - Advanced Catalyst Synthesis and Characterization (ACSC) Project WBS 2.5.4.304; 303; 305

The Advanced Catalyst Synthesis and Characterization (ACSC) project, in close collaboration with the Chemical Catalysis for Bioenergy (ChemCatBio) Consortium enabling projects, CatCost, and the Engineering of Catalyst Scale-Up project, (1) provides fundamental insight into working catalysts leading to actionable recommendations for all of the ChemCatBio catalysis projects, (2) addresses overarching catalysis challenges central to the ChemCatBio Consortium, and (3) adapts and applies new synthesis methodologies and in situ/operando characterization capabilities to meet the evolving needs of the catalysis projects. The outcome is a transition from empirical catalyst development to rational design through the prediction of materials with targeted properties based on advanced characterization combined with computational modeling, and the synthesis of next generation catalysts with predicted structures that yield demonstrated improvements in catalytic performance. In FY18, the ACSC helped to demonstrate the utility of the complete catalyst and process development cycle for dimethyl ether to high-octane gasoline over metal-modified zeolite catalysts for the Upgrading of C1 Building Blocks project, and in FY21 will leverage capabilities, expertise, and computational models established for this effort to target next-generation catalysts for ethanol to distillates for the Upgrading of C2 Intermediates project with enhanced performance in half the time.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗
DOE OSTI2021

Commissioning & Characterization of Magnetized Gridded Thermionic Electron Source

Collaborative efforts to design and fabricate a magnetized gridded thermionic electron source have been conducted between Xelera and Jefferson Lab. Commissioning and characterization of an electron gun fabricated by Xelera was performed to benchmark the viability of future electron source designs and capabilities. The work involved simulation, installation, trouble-shooting, modifications of the design, commissioning, characterization, and magnetization of the electron beam produced. A specially designed cavity as well as novel diagnostic tools and methods were developed, implemented, and experimentally tested. Finally, the gun was used to demonstrate a previously unachieved current of magnetized electron beam from a gridded thermionic source of this uniquely compact size. This thesis addresses the following scientific and technological challenges: building a compact gridded thermionic electron source, producing high current magnetized electron beam, and demonstrating novel characterization measurements for magnetized beam.

Stefani, Mark↗