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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,189 records · Page 66
All sourcesNASA NTRSDOE OSTI
DOE OSTI2021

Integrated sample-handling and mounting system for fixed-target serial synchrotron crystallography

Serial synchrotron crystallography (SSX) is enabling the efficient use of small crystals for structure–function studies of biomolecules and for drug discovery. An integrated SSX system has been developed comprising ultralow background-scatter sample holders suitable for room and cryogenic temperature crystallographic data collection, a sample-loading station and a humid `gloveless' glovebox. The sample holders incorporate thin-film supports with a variety of designs optimized for different crystal-loading challenges. These holders facilitate the dispersion of crystals and the removal of excess liquid, can be cooled at extremely high rates, generate little background scatter, allow data collection over >90° of oscillation without obstruction or the risk of generating saturating Bragg peaks, are compatible with existing infrastructure for high-throughput cryocrystallography and are reusable. The sample-loading station allows sample preparation and loading onto the support film, the application of time-varying suction for optimal removal of excess liquid, crystal repositioning and cryoprotection, and the application of sealing films for room-temperature data collection, all in a controlled-humidity environment. The humid glovebox allows microscope observation of the sample-loading station and crystallization trays while maintaining near-saturating humidities that further minimize the risks of sample dehydration and damage, and maximize working times. This integrated system addresses common problems in obtaining properly dispersed, properly hydrated and isomorphous microcrystals for fixed-orientation and oscillation data collection. Its ease of use, flexibility and optimized performance make it attractive not just for SSX but also for single-crystal and few-crystal data collection. Fundamental concepts that are important in achieving desired crystal distributions on a sample holder via time-varying suction-induced liquid flows are also discussed.

47 OTHER INSTRUMENTATION↗
NASA NTRS1993

Flow visualization study in high aspect ratio cooling channels for rocket engines

The structural integrity of high pressure liquid propellant rocket engine thrust chambers is typically maintained through regenerative cooling. The coolant flows through passages formed either by constructing the chamber liner from tubes or by milling channels in a solid liner. Recently, Carlile and Quentmeyer showed life extending advantages (by lowering hot gas wall temperatures) of milling channels with larger height to width aspect ratios (AR is greater than 4) than the traditional, approximately square cross section, passages. Further, the total coolant pressure drop in the thrust chamber could also be reduced, resulting in lower turbomachinery power requirements. High aspect ratio cooling channels could offer many benefits to designers developing new high performance engines, such as the European Vulcain engine (which uses an aspect ratio up to 9). With platelet manufacturing technology, channel aspect ratios up to 15 could be formed offering potentially greater benefits. Some issues still exist with the high aspect ratio coolant channels. In a coolant passage of circular or square cross section, strong secondary vortices develop as the fluid passes through the curved throat region. These vortices mix the fluid and bring lower temperature coolant to the hot wall. Typically, the circulation enhances the heat transfer at the hot gas wall by about 40 percent over a straight channel. The effect that increasing channel aspect ratio has on the curvature heat transfer enhancement has not been sufficiently studied. If the increase in aspect ratio degrades the secondary flow, the fluid mixing will be reduced. Analysis has shown that reduced coolant mixing will result in significantly higher wall temperatures, due to thermal stratification in the coolant, thus decreasing the benefits of the high aspect ratio geometry. A better understanding of the fundamental flow phenomena in high aspect ratio channels with curvature is needed to fully evaluate the benefits of this geometry. The fluid dynamic and conjugate heat transfer problem of high aspect ratio rocket engine coolant channels are being investigated numerically, but these efforts have been hampered by a lack of validating data. Wall temperature data is available for the conjugate problem for channels without curvature and aspect ratio = 5.0, and unheated fluid dynamic data are available for square and circular cross section channels with curvature at Reynold's numbers up to 40,000. But the effects of aspect ratio on secondary flow development have not been experimentally studied. To provide some insight into the effects of channel aspect ratio on secondary flow and to qualitatively provide anchoring for the numerical codes, a flow visualization experiment was initiated at the NASA Lewis Research Center.

Meyer, Michael L.↗
DOE OSTI2014

Primordial power spectrum from Planck

Using modified Richardson-Lucy algorithm we reconstruct the primordial power spectrum (PPS) from Planck Cosmic Microwave Background (CMB) temperature anisotropy data. In our analysis we use different combinations of angular power spectra from Planck to reconstruct the shape of the primordial power spectrum and locate possible features. Performing an extensive error analysis we found the dip near ℓ ∼ 750–850 represents the most prominent feature in the data. Feature near ℓ ∼ 1800–2000 is detectable with high confidence only in 217 GHz spectrum and is apparently consequence of a small systematic as described in the revised Planck 2013 papers. Fixing the background cosmological parameters and the foreground nuisance parameters to their best fit baseline values, we report that the best fit power law primordial power spectrum is consistent with the reconstructed form of the PPS at 2σ C.L. of the estimated errors (apart from the local features mentioned above). As a consistency test, we found the reconstructed primordial power spectrum from Planck temperature data can also substantially improve the fit to WMAP-9 angular power spectrum data (with respect to power-law form of the PPS) allowing an overall amplitude shift of ∼ 2.5%. In this context low-ℓ and 100 GHz spectrum from Planck which have proper overlap in the multipole range with WMAP data found to be completely consistent with WMAP-9 (allowing amplitude shift). As another important result of our analysis we do report the evidence of gravitational lensing through the reconstruction analysis. Finally we present two smooth form of the PPS containing only the important features. These smooth forms of PPS can provide significant improvements in fitting the data (with respect to the power law PPS) and can be helpful to give hints for inflationary model building.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2025

Predictive modeling of Néel temperature in austenitic alloys using CALPHAD and data analytics

The Néel temperature is a crucial yet often overlooked parameter in calculating the stacking fault energy (SFE) of austenitic alloys. Several empirical equations have been proposed to estimate the Néel temperature of austenitic alloys, which are then used to calculate the SFE and explain deformation mechanisms. However, these empirical equations, typically derived using linear regression algorithms, are often simplistic and may fail to capture the complex interactions among multiple alloying elements that influence the Néel temperature. Moreover, their applicability is usually limited to specific compositional ranges. In this study, we propose a CALPHAD based approach and develop a surrogate decision tree based regression model capable of capturing the interactions among multiple alloying elements to predict the Néel temperature. Predictions from both the CALPHAD approach and the regression model show close agreement with experimental measurements reported in the literature. In conclusion, the implications of accurate Néel temperature predictions on the calculated SFE and deformation mechanisms are also discussed.

36 MATERIALS SCIENCE↗
NASA NTRS2003

Determination of Net Martian Polar Dust Flux from MGS-TES Observations

Using atmospheric dust abundance and atmospheric temperature observation data from the Thermal Emission Spectrometer (TES) on board the Mars Global Surveyor (MGS), the net flux of dust into and out of the Martian polar regions will be examined. Mars polar regions possess layered terrain , believed to be comprised of a mixture of ice and dust, with the different layers possibly representing different past climate regimes. These changes in climate may reflect changes in the deposition of dust and volatiles through impacts, volcanism, changes in resources of ice and dust, and response to Milankovitch type cycles (changes in eccentricity of orbit, obliquity and precession of axis). Understanding how rapidly such layers can be generated is an important element to understanding Mars climate history. This study uses the observed vertical temperature data and dust content measurements from TES to analyze the sign (gain or loss) of dust at high latitudes.

M A Blackmon↗
NASA NTRS1984

Intercomparisons of temperature, density and wind measurements from in situ and satellite techniques

Atmospheric temperature, density, and wind data retrieved by various means are intercompared, covering the 1980-1984 period. The study encompasses such data sources as radiosonde, rocketsonde, in situ measurements, remote measurements, satellites, and NOAA-6 and 7 TOVS data. Larger temperature differences (up to 7-8 K) are noted for the rocketsonde/satellite comparison than for the radiosonde/satellite comparison (less than 1 K). The rocketsonde measurements were found to be internally consistent to less than 1 K up to 50 km and to less than 3 K up to 60 km. A general agreement of the density data obtained from small rocketsondes and large sounding rocket systems is suggested to be within 15 percent up to 85 km of altitude. The usefulness of intermixing the measurements of the various atmospheric parameters obtained from different instruments is emphasized, and some suggestions are made concerning the approaches to such intermixing.

Schmidlin, F. J.↗
NASA NTRS2011

Stability of a Crystal Oscillator, Type Si530, Inside and Beyond its Specified Operating Temperature Range

Data acquisition and control systems depend on timing signals for proper operation and required accuracy. These clocked signals are typically provided by some form of an oscillator set to produce a repetitive, defined signal at a given frequency. Crystal oscillators are commonly used because they are less expensive, smaller, and more reliable than other types of oscillators. Because of the inherent characteristics of the crystal, the oscillators exhibit excellent frequency stability within the specified range of operational temperature. In some cases, however, some compensation techniques are adopted to further improve the thermal stability of a crystal oscillator. Very limited data exist on the performance and reliability of commercial-off-the-shelf (COTS) crystal oscillators at temperatures beyond the manufacturer's specified operating temperature range. This information is very crucial if any of these parts were to be used in circuits designed for use in space exploration missions where extreme temperature swings and thermal cycling are encountered. This report presents the results of the work obtained on the operation of Silicon Laboratories crystal oscillator, type Si530, under specified and extreme ambient temperatures.

Patterson, Richard L.↗
NASA NTRS1995

Observation of local cloud and moisture feedbacks over high ocean and desert surface temperatures

New data on clouds and moisture, made possible by reanalysis of weather satellite observations, show that the atmosphere reacts to warm clusters of very high sea surface temperatures in the western Pacific Ocean with increased moisture, cloudiness, and convection, suggesting a negative feedback limiting the sea surface temperature rise. The reverse was observed over dry and hot deserts where both moisture and cloudiness decrease, suggesting a positive feedback perpetuating existing desert conditions. In addition, the observations show a common critical surface temperature for both oceans and land; the distribution of atmospheric moisture is observed to reach a maximum value when the daily surface temperatures approach 304 +/- 1 K. These observations reveal complex dynamic-radiative interactions where multiple processes act simultaneously at the surface as well as in the atmosphere to regulate the feedback processes.

Chahine, Moustafa T.↗
NASA NTRS1975

Parametric evaluation of a dual-layer dynamic hyperfiltration membrane for recovery of spacecraft wash water at elevated temperature

Performance data consisting of solute rejections and product flux have been measured, as dependent on the operational parameters. These parameters were pressure, 5,000,000 N/sq m (750 psia) to 7,000,000 N/sq m (1040 psia); temperature, 347 K (165 F) to 368 K (200 F); velocity, 1.6 m/s to 10 m/s; and concentration (up to 14x). Tests were carried out on analog wash water. Data taken include rejections of organic materials (TOC), ammonia, urea, and an assortment of ions. The membrane used was a dual-layer, polyacrylic acid over zirconium oxide, deposited in situ on a porcelain ceramic substrate.

Brandon, C. A.↗
NASA NTRS1987

The calculation of high-temperature equilibrium and nonequilibrium specific heat data for N2, O2 and NO

Specific heat data for high-temperature air species are needed to compute the temperature and enthalpy of gas mixtures in aerothermodynamics flowfield calculations. Accurate data are known only for temperatures under 6000 K, but are required for temperatures exceeding 25,000 K. In the present study, CP data are computed for N2, O2 and NO. The calculations are based on summations over all the vibration-rotation energy levels for all known bound electronic states. Estimates are made for the error introduced by the neglect of possible additional high-lying electronic states. In addition, a scheme for the partitioning of the internal energy into vibrational, rotational and electronic contributions is presented which consistently accounts for the nonseparable nature of the various energy modes. The multitemperature specific heat data are recommended for use in nonequilibrium flowfield models.

Jaffe, Richard L.↗
DOE OSTI2018

Low-Temperature Ionic Conductivity Enhanced by Disrupted Ice Formation in Polyampholyte Hydrogels

Here, the phase behavior of water in hydrogels has a broad impact on many health and energy applications. Our previous study showed that polyampholyte hydrogel has the potential to be used as an aqueous gel electrolyte in electrochemical storage devices at -30 °C due to enhanced low-temperature conductivity. In this study, we detail the impact polymer structure has on this enhanced conductivity, explaining this finding with a model charge-balanced polyampholyte, poly(4-vinylbenzenesulfonate- co -[3-(methacryloylam ino)propyl] trimethylammonium chloride), a hydrogel whose polymer and water structures are probed by variable-temperature SAXS, WAXS, and solid-state NMR spectroscopy. SAXS results at room temperature indicate a networked globule structure in the charge-balanced polyampholyte hydrogels. The globular radius of gyration is ~ 2.5 nm, whereas the globular size and its clustering structure are dependent on synthesis parameters. Variable-temperature SAXS data reveal a temperature-dependent structure evolution of the polyampholyte hydrogel. An interconnected globular network structure of polymer-rich phase at low temperature, observed by electron microscopy, is suggested to preserve ion-conducting channels of nonfrozen water molecules at low temperatures. This hypothesis is further supported by solid-state NMR spectroscopy. Together these findings provide macromolecular- and molecular-level insight that may be used to design gel electrolytes for enhanced low-temperature performance.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2026

Deriving reliable nucleation rates from metadynamics simulations: Application to Yukawa fluids

In order to solidify the usefulness of metadynamics in studying nucleation of crystals from supercooled liquids, this work provides a specific procedure to calculate nucleation free energy barriers. After a pedagogical review of the important elements of classical nucleation theory and how metadynamics is used to find nucleation free energy barriers, we explain the benefits of local collective variables over more common global collective variables. We show how a metadynamics free energy barrier must be carefully post-processed so that classical nucleation theory can be applied to calculate nucleation rates. We apply our procedure to a Yukawa plasma and show that a particular physically motivated fit to metadynamics data reproduces low-temperature reference data, justifying the usefulness of metadynamics to predict nucleation rates.

42 ENGINEERING↗
DOE OSTI2019

Quasiparticle relaxation dynamics in URu 2 - x Fe x Si 2 single crystals

We investigate quasiparticle relaxation dynamics in URu 2–x Fe x Si 2 single crystals using ultrafast optical-pump optical-probe (OPOP) spectroscopy as a function of temperature and Fe substitution (x), crossing from the hidden-order (HO) phase (x = 0) to the large-moment antiferromagnet (LMAFM) phase (x = 0 .12). Here, at low temperature, the dynamics for x = 0 and x = 0 .12 are consistent with the low-energy electronic structure of the HO and LMAFM phases that emerge from the high-temperature paramagnetic (PM) phase. In contrast, near the bicritical point separating HO and LMAFM (x = 0 .1), two transitions occur over a narrow temperature range (from 15.5–17.5 K). A PM to HO transition occurs at an intermediate temperature followed by a transition to the LMAFM phase at lower temperature. While the data at low temperatures are consistent with the expected coexistence of LMAFM and HO, the data in the intermediate temperature phase are not, and instead suggest the possibility of an unexpected coexistence of HO and PM. Additionally, the dynamics in the PM phase reflect the presence of a hybridization gap as well as strongly interacting spin and charge degrees of freedom. OPOP yields insights into meV-scale electrodynamics with sub-Kelvin temperature resolution, providing a complementary approach to study low-energy electronic structure in quantum materials.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
NASA NTRS1975

Aerial thermal scanner data for monitoring rooftop temperatures

Four Nebraska communities and one South Dakota community were surveyed. Thermal scanner data were converted to a film format and the resultant imagery was successfully employed to monitor rooftop temperatures. The program places emphasis on heat losses resulting from inadequate home insulation, offers CENGAS customers the opportunity to observe a thermogram of their rooftop, and assists homeowners in evaluating insulation needs.

Bjorkland, J.↗
DOE OSTI2023

DTS data from TRACER TBS

Distributed temperature-sensing data collected using a Silixa-XT DTS and 50/125 MM fiber. Data are calibrated using two water baths at the surface and an iMet aloft at the end of the fiber and tether. The data are then assigned an altitude for the TBS flight.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2015

Neutron and high-resolution room-temperature X-ray data collection from crystallized lytic polysaccharide monooxygenase

Bacteria and fungi express lytic polysaccharide monooxgyenase (LPMO) enzymes that act in conjunction with canonical hydrolytic sugar-processing enzymes to rapidly convert polysaccharides such as chitin, cellulose and starch to single monosaccharide products. In order to gain a better understanding of the structure and oxidative mechanism of these enzymes, large crystals (1–3 mm 3 ) of a chitin-processing LPMO from the Gram-positive soil bacterium Jonesia denitrificans were grown and screened for their ability to diffract neutrons. In addition to the collection of neutron diffraction data, which were processed to 2.1 Å resolution, a high-resolution room-temperature X-ray diffraction data set was collected and processed to 1.1 Å resolution in space group P 2 1 2 1 2 1 . To our knowledge, this work marks the first successful neutron crystallographic experiment on an LPMO. As a result, joint X-ray/neutron refinement of the resulting data will reveal new details of the structure and mechanism of this recently discovered class of enzymes.

59 BASIC BIOLOGICAL SCIENCES↗
NASA NTRS1990

Analysis of stratospheric ozone, temperature, and minor constituent data

The objective of this research is to use available satellite measurements of temperature and constituent concentrations to test the conceptual picture of stratospheric chemistry and transport. This was originally broken down into two sub-goals: first, to use the constituent data to search for critical tests of our understanding of stratospheric chemistry and second, to examine constituent transport processes emphasizing interactions with chemistry on various time scales. A third important goal which has evolved is to use the available solar backscattered ultraviolet (SBUV) and Total Ozone Mapping Spectrometer (TOMS) data from Nimbus 7 to describe the morphology of recent changes in Antarctic and global ozone with emphasis on searching for constraints to theories. The major effort now being pursued relative to the two original goals is our effort as a theoretical team for the Arctic Airborne Stratospheric Expedition (AASE). Our effort for the AASE is based on the 3D transport and chemistry model at Goddard. Our goal is to use this model to place the results from the mission data in a regional and global context. Specifically, we set out to make model runs starting in late December and running through March of 1989, both with and without heterogeneous chemistry. The transport is to be carried out using dynamical fields from a 4D data assimilation model being developed under separate funding from this task. We have successfully carried out a series of single constituent transport experiments. One of the things demonstrated by these runs was the difficulty in obtaining observed low N2O abundances in the vortex without simultaneously obtaining very high ozone values. Because the runs start in late December, this difficulty arises in the attempt to define consistent initial conditions for the 3D model. To accomplish a consistent set of initial conditions, we are using the 2D photochemistry-transport model of Jackman and Douglass and mapping in potential temperature, potential vorticity space as developed by Schoeberl and coworkers.

Stolarski, Richard S.↗