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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,207 records · Page 67

Effects of method of loading and specimen configuration on compressive strength of graphite/epoxy composite materials

Three test schemes were examined for testing graphite/epoxy (Narmco T300/5208) composite material specimens to failure in compression, including an adaptation of the IITRI "wedge grip" compression fixture, a face-supported-compression fixture, and an end-loaded-coupon fixture. The effects of specimen size, specimen support arrangement and method of load transfer on compressive behavior of graphite/epoxy were investigated. Compressive stress strain, strength, and modulus data obtained with the three fixtures are presented with evaluations showing the effects of all test parameters, including fiber orientation. The IITRI fixture has the potential to provide good stress/strain data to failure for unidirectional and quasi-isotropic laminates. The face supported fixture was found to be the most desirable for testing + or - 45 s laminates.

Clark, R. K.↗

Wiring test program insulation material related properties

This viewgraph presentation provides an overview of activities at DASA-RI concerning the testing of wires for manned spacecraft, including test facilities, arc-tracking tests, flammability tests, microgravity tests, and standardization, and outlines future activities.

Reher, Heinz-Josef↗

Electrostatic testing of thin plastic materials

Ten thin plastic materials (Velostat, RCAS 1200, Llumalloy, Herculite 80, RCAS 2400, Wrightlon 7000, PVC, Aclar 22A, Mylar, and Polyethylene) were tested for electrostatic properties by four different devices: (1) The static decay meter, (2) the manual triboelectric testing device, (3) the robotic triboelectric testing device, and (4) the resistivity measurement adapter device. The static decay meter measured the electrostatic decay rates in accordance with the Federal Test Method Standard 101B, Method 4046. The manual and the robotic triboelectric devices measured the triboelectric generated peak voltages and the five-second decay voltages in accordance with the criteria for acceptance standards at Kennedy Space Center. The resistivity measurement adapter measured the surface resistivity of each material. An analysis was made to correlate the data among the four testing devices. For the material tested the pass/fail results were compared for the 4046 method and the triboelectric testing devices. For the limited number of materials tested, the relationship between decay rate and surface resistivity was investigated as well as the relationship between triboelectric peak voltage and surface resistivity.

Skinner, S. Ballou↗

Materials, Manufacturing, and Test Development of a Composite Fan Blade Leading Edge Subcomponent for Improved Impact Resistance

Application of polymer matrix composite materials for jet engine fan blades is becoming attractive as an alternative to metallic blades; particularly for large engines where significant weight savings are recognized on moving to a composite structure. However, the weight benefit of the composite is offset by a reduction of aerodynamic efficiency resulting from a necessary increase in blade thickness; relative to the titanium blades. Blade dimensions are largely driven by resistance to damage on bird strike. Further development of the composite material is necessary to allow composite blade designs to approximate the dimensions of a metallic fan blade. The reduction in thickness over the state of the art composite blades is expected to translate into structural weight reduction, improved aerodynamic efficiency, and therefore reduced fuel consumption. This paper presents test article design, subcomponent blade leading edge fabrication, test method development, and initial results from ballistic impact of a gelatin projectile on the leading edge of composite fan blades. The simplified test article geometry was developed to realistically simulate a blade leading edge while decreasing fabrication complexity. Impact data is presented on baseline composite blades and toughened blades; where a considerable improvement to impact resistance was recorded.

Materials↗

Materials, Manufacturing and Test Development of a Composite Fan Blade Leading Edge Subcomponent for Improved Impact Resistance

Application of polymer matrix composite materials for jet engine fan blades is becoming attractive as an alternative to metallic blades; particularly for large engines where significant weight savings are recognized on moving to a composite structure. However, the weight benefit of the composite of is offset by a reduction of aerodynamic efficiency resulting from a necessary increase in blade thickness; relative to the titanium blades. Blade dimensions are largely driven by resistance to damage on bird strike. Further development of the composite material is necessary to allow composite blade designs to approximate the dimensions of a metallic fan blade. The reduction in thickness over the state of the art composite blades is expected to translate into structural weight reduction, improved aerodynamic efficiency, and therefore reduced fuel consumption. This paper presents test article design, subcomponent blade leading edge fabrication, test method development, and initial results from ballistic impact of a gelatin projectile on the leading edge of composite fan blades. The simplified test article geometry was developed to realistically simulate a blade leading edge while decreasing fabrication complexity. Impact data is presented on baseline composite blades and toughened blades; where a considerable improvement to impact resistance was recorded.

Ballistic Impact↗

Sub-sized specimen testing and its relationship with Gen IV Materials Qualification

Renewed interest in advanced reactor technologies which can produce inherently safe, reliable, low carbon, low cost energy requires the development of new materials which can operate in the extreme environments proposed by Gen IV reactor designs. The primary focus of the Nuclear Materials Discovery and Qualification Initiative (NMDQi) is to accelerate the process by which new materials can make their way into commercial use, enabling new technologies and innovations within the nuclear sector. Due to limitations in the production of neutron irradiated material for testing and qualification, the use of specimens far smaller than those traditionally called for in regulatory codes becomes a necessity. While the use of these sub-sized specimens is necessary to achieve materials qualification on a realistic timeline and budget, literature showing the efficacy of these samples as an appropriate surrogate for ASME/ASTM defined samples is limited. This poster will detail historical efforts to compare the mechanical behavior of small geometry samples with bulk material behavior and the potential of sub-sized specimen testing at INL for future materials qualification efforts.

36 MATERIALS SCIENCE↗

Issues related to testing of Space Station materials

Issues pertaining to the long life of Space Station materials and to the test methodology for the certification of these materials are presented. Consideration is given to atomic oxygen degradation, debris and micrometeoroid damage, and thermal cycling. It is noted that the integration of the combined effects of all of these phenomena is highly important as they cannot be viewed as separate isues.

Fowler, M.↗

Spark Plasma Sintering (SPS) Update for the Fuel Conversion Effort at the Transient Reactor Test Facility

Over the lifetime of the Transient Reactor Test Facility (TREAT) reactor from 1959 to 1994, a series of historical tests disclosed certain material specific requisites for irradiation testing variables resulted in negligible structural damage after exposure to the reactor and multiple experiments. Comparable fuel design, material testing, and qualifications needs to occur for the high-enriched uranium (HEU) to low enriched uranium (LEU) fuel conversion (<20% U235) of TREAT. This includes, retaining a uniform precipitate dispersion of fueled UO2 micron-size particles throughout a graphite-moderating matrix, where high-density graphite is in direct contact with the fuel and acts as a moderator. On that note, the design of future LEU reactor TREAT fuel core will consider the relative sizing and spacing of fuel as well as the retention of graphite in accordance with the expected thermal, neutron, and energy portfolio for future conversion. In light of the above, LEU conversion fuel blocks currently being manufactured must undergo critical materials testing, irradiation, and examination to determine effects on the manufactured replacement fuel blocks at the millimeter to sub-micron size scale. Herein, we will report and update the community on value-added studies focusing on spark plasma sintering as an alternative technique to fabricate high density graphite dispersion fuel.

36 MATERIALS SCIENCE↗

Flash and fire test: Evaluation of the behavior of nonmetallic materials in hydrogen

Tests conducted to evaluate the behavior of nonmetallic materials in hydrogen are described. The results of the flash and fire test are presented. The flash and fire test is used to evaluate the tendency of heated materials to ignite in a hydrogen atmosphere when subjected to an ignition source. The test represents a hydrogen parallel to a hazard condition known to exist in oxygen systems. Ten nonmetallic materials were evaluated to establish baseline data on the behavior of the materials and to characterize one mode of material failure considered to be a factor pertinent to the safe use of a material in hydrogen.

Source record↗

Tribological Tuft Testing Candidate Brush Seal Materials

This paper presents a tribological tuft test method of candidate brush seal materials in viewgraph form. The goals of the research are: 1) To develop test method to tribologically brush seal materials; 2) To evaluate materials to identify potential improvements and trends; and 3) Guide seal material development and selection.

DellaCorte, Chris↗

An investigation of the Iosipescu and Asymmetrical Four-Point Bend tests for composite materials

The results of an extensive analytical and experimental investigation of the Iosipescu and Asymmetrical Four-Point Bend (AFPB) test methods are summarized. Finite element analyses were used to assess the influence of notch parameters and load locations on the stress state in the specimens. The shear moduli and shear strengths were experimentally measured for quasi-isotropic graphite-epoxy laminates using both the Iosipescu and the AFPB test methods with various combinations of notch parameters and load locations. The test results indicate that changes in the notch geometry and load locations aimed at improving the stress distribution in the test section result in unexpected changes in the failure mode.

Spigel, B. S.↗

Transverse Tension Fatigue Life Characterization Through Flexure Testing of Composite Materials

The transverse tension fatigue life of S2/8552 glass-epoxy and IM7/8552 carbon-epoxy was characterized using flexure tests of 90-degree laminates loaded in 3-point and 4-point bending. The influence of specimen polishing and specimen configuration on transverse tension fatigue life was examined using the glass-epoxy laminates. Results showed that 90-degree bend specimens with polished machined edges and polished tension-side surfaces, where bending failures where observed, had lower fatigue lives than unpolished specimens when cyclically loaded at equal stress levels. The influence of specimen thickness and the utility of a Weibull scaling law was examined using the carbon-epoxy laminates. The influence of test frequency on fatigue results was also documented for the 4-point bending configuration. A Weibull scaling law was used to predict the 4-point bending fatigue lives from the 3-point bending curve fit and vice-versa. Scaling was performed based on maximum cyclic stress level as well as fatigue life. The scaling laws based on stress level shifted the curve fit S-N characterizations in the desired direction, however, the magnitude of the shift was not adequate to accurately predict the fatigue lives. Furthermore, the scaling law based on fatigue life shifted the curve fit S-N characterizations in the opposite direction from measured values. Therefore, these scaling laws were not adequate for obtaining accurate predictions of the transverse tension fatigue lives.

OBrien, T. Kevin↗

Using Isothermal Microcalorimetry to Determine Compatibility of Structural Materials with High Test Hydrogen Peroxide (HTP) Propellant

High-Test Hydrogen Peroxide (HTP) propellant (greater than or equal to 70%) offers many advantages in space launch applications; however, materials used in construction of propulsion systems must be shown to be compatible with HTP. Isothermal Microcalorimetry (IMC) was used to determine the compatibility of several metallic and non-metallic materials with 90% HTP. The results of these experiments agreed with those from immersion bath tests when the values were converted to %Active Oxygen Loss per week (%AOL/wk).

Gostowski, Rudy↗

An Approach to Evaluate Precision and Inter-Laboratory Variability of Flammability Test Methods for Aerospace Materials

Materials selection for spacecraft is based on conventional flammability or ignition sensitivity acceptance tests. Current procedures for determining the inter-laboratory repeatability and reproducibility of aerospace materials flammability tests are not considering the dependence of data variability on test conditions and consequently attempts to characterize the precision of these methods were not successful. The inter-laboratory data variability is determined with tests conducted under arbitrary conditions, which consequently may not provide sufficient information to enable adequate determination of a method's precision. For evaluating the precision of NASA's flammability test methods, the protocol recommended includes selecting critical parameters and determining the 50% failure point by considering the specific failure criteria of each method using the critical parameter as a variable. Upon performing inter-laboratory round robin testing using this approach, the laboratories' performance could be evaluated by comparing the repeatability of the 50% failure point and/or the repeatability of critical conditions where the probabilities of passing and failing are unity, i.e., the transition zone repeatability. When a sufficient amount of data has been acquired with this method, an adequate estimation of precision of aerospace materials flammability test methods will be possible.

Hirsch, David↗