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Subscale tests were extensively used to develop a data base on elastic properties of graphite-epoxy wound pressure vessels. Scaling phenomena were observed to influence biaxial strains. Causes for scaling are proposed and lamina models with scaling factors are presented.
In order to explain the results of the testing conducted in Part I and relate the subscale test specimen performance to case performance during prelaunch loading, a comprehensive analysis program was conducted. Finite element models of both full-scale case and subscale test coupons were made. Validated axisymmetric models were used for the case analyses. Modeling of coupons was accomplished using a generalized plane strain finite element model in most cases, although some three-dimensional finite element modeling was used to investigate the importance of three-dimensional effects on the coupon performance. The large number of plies and complexity of the test coupons used limited the finite element grids to a through-the-thickness discretization of one element per ply. Delaminations observed in the helical ply dropoff region were modeled using frictionless sliders. Comparisons of predicted strains and displacements were made with the test data from both cases and coupons to validate the finite element models. Based on observations of the test results and finite element predictions, a failure criterion for both coupons and cases was postulated and then validated by comparing performance predictions to test results. Finally, the validated failure criterion was used to predict the performance of the first two flight cases under prelaunch loads.
Chains produced by use of rotating mandrel. Mandrel and locating and driving disks assembled around first band. Mandrel and band then mounted in respective positions on filament-winding machine. Second band linked to first by winding filament around first band on rotating mandrel. Short chains made this way have variety of uses; example, thermal isolators, each consisting of two linked bands of insulating material, used to support two separated insulating sheilds surrounding container of liquid helium.
The data tape 8 data are presented in tabular form. Each page consists of six-component force and moment coefficients as they vary with angle of attack at a specific Mach number and roll angle. The angle of attack range is from 0 to 180 deg in 5 deg increments. The six coefficients are normal force, pitching moment, side force, yawing moment, axial force, and rolling moment. Each successive page is incremented for roll angle in 45 deg increments for a roll angle range from 0 to 360 deg. The cycle is then repeated for the next Mach number. The Mach numbers in the data base are 0.4, 0.5, 0.55, 0.6, 0.7, 0.8, 0.9, 0.95, 1.05, 1.1, 1.2, 1.4, 1.96, 2.5, 3.0, and 3.48.
A model for predicting the fracture strength of homogeneous materials is proposed. Impacted FWC samples were evaluated using ultrasonic testing and an X-ray dye penetration method. The ability of the model to measure fracture strength was also examined. The relation between attenuation and velocity measurements is studied. It is observed that the X-ray method is not useful for predicting fracture strength because the dye could not penetrate the matrix. It is noted that fracture strength predictions derived from the fracture mechanical model and the ultrasonic measurements correlate well with actual measured fracture strengths.
An epoxy and carbon fiber composite has been used to produce a light-weight rocket case for the Space Shuttle. A kinetic model is developed which can predict the extent of epoxy conversion during the winding and curing of the case. The model accounts for both chemical and physical kinetics. In the model, chemical kinetics occur exclusively up to the time the transition temperature equals the reaction temperature. At this point the resin begins to solidify and the rate of this process limits the rate of epoxy conversion. A comparison of predicted and actual epoxy conversion is presented for isothermal and temperature programmed cure schedules.
Acoustic emission in 51-cm diameter graphite/epoxy pressure vessels was monitored during pressurization (hydrotesting). Several vessels were subjected to impact by a blunt impactor, but only after the vessels had been proofed; that is, pressurized to 80 percent of nominal burst pressure as determined from control (unimpacted) vessels. AE activity was then monitored throughout a series of successively higher pressure cycles ranging from 10 to 60 percent of ultimate. Each cycle included a ramp up to pressure followed by a 4-min hold period and then pressure unload. The event rate was high, and especially modified AE analyzers had to be used to acquire the data. This paper presents the AE event count versus pressure history of these tests and demonstrates the ability of the AE technique to monitor the growth of damage and to estimate the effect on ultimate strength. The number of events that occurred during pressure holds proved to be a reasonable estimator of vessel performance.
Compression testing of 12-ply graphite/bismaleimide laminated plates with induced and natural defects is discussed, and emphasis is placed on resultant changes in strength and stiffness. Ply drops, ply cuts, and fiber crossovers are studied by comparison with a quasi-isotropic control group. It is observed that, as expected, failure initiates at the defects and progresses via delamination, sublaminate buckling, angle-ply cracking, and longitudinal ply failure. The ultimate stress is reduced by approximately 40 percent for all types of defects except the unsymmetrical cut-ply specimens which averages a 54-percent reduction. The average stiffness reduction of 10 percent is observed for specimens with induced defects. Fiber crossovers are found to reduce the laminate strength and stiffness significantly.
Graphite/epoxy composites are extensively used in the aerospace and sporting goods industries due to their superior engineering properties compared to those of metals. However, graphite/epoxy is extremely susceptible to impact damage which can cause considerable and sometimes undetected reduction in strength. An inelastic impact model was developed to predict damage due to low-velocity impact. A transient dynamic finite element formulation was used in conjunction with the 3D Tsai-Wu failure criterion to determine and incorporate failure in the materials during impact. Material degradation can be adjusted from no degradation to partial degradation to full degradation. The developed software is based on an object-oriented implementation framework called Extensible Implementation Framework for Finite Elements (EIFFE).
Multiple Fiber Bragg-gratings are embedded in carbon-epoxy laminates as well as in composite wound pressure vessel. Structural properties of such composites are investigated. The measurements include stress-strain relation in laminates and Poisson's ratio in several specimens with varying orientation of the optical fiber Bragg-sensor with respect to the carbon fiber in an epoxy matrix. Additionally, fiber Bragg gratings are bonded on the surface of these laminates and cylinders fabricated out of carbon-epoxy composites and multiple points are monitored and compared for strain measurements at several locations.
The design and fabrication of composite blades for the WTS-4, a four-megawatt horizontal-axis wind turbine, is discussed. The blade consists of a two-cell, monolithic structure of filament-wound, fiberglass/epoxy composite. Filament winding is a low-cost process which can produce a blade with an aerodynamically efficient airfoil and planform with nonlinear twist to achieve high performance in terms of energy capture. Its retention provides a redundant attachment for long, durable life and safety. Advanced tooling concepts and as sophisticated computer control is used to achieve the unique filament-wound shape.
Impacters of various masses were dropped from various heights onto thick graphite/epoxy filament-wound cylinders. The cylinders represented filament-wound cases made for the booster motors of the Space Shuttle. Tups of various shapes were affixed to the impacters. Some of the cylinders were filled with inert propellant, and some were empty. The cylinders were impacted numerous times around the circumference and then cut into tension coupons, each containing an impact site. The size of the damage and the residual tension strength were measured. For hemispherical tups, strength was reduced as much as 30 percent by nonvisible damage. The damage consisted of matrix cracking and broken fibers. Analytical methods were used to predict the damage and residual tension strength. A factor of safety to account for nonvisible damage was determined. For corner and rod shaped tups, any damage that resulted in strength loss was readily visible.
Studies were conducted to select a TRW A-type polyimide resin that would be suitable for fabrication of filament wound reinforced plastics structures. Several different formulations were evaluated after which the P105AC formulation was selected as the most promising. Procedures were developed for preparing P105AC/S-glass roving prepreg and for fabricating filament wound structural composites. Composites were fabricated and then tested in order to obtain tensile and shear strength information. Small, closed-end cylindrical pressure vessels then were fabricated using a stainless steel liner and end-fittings with a P105AC/S-glass polar-wound overwrap. These pressure vessels were cured in an air circulating oven without augmented pressure. It was concluded upon completion of this study that the P105AC resin system is suitable for filament winding; that low void content, high strength composites are obtained by the filament winding process; and that augmented pressure is not required to effect the fabrication of filament wound P105AC composites.
The work performed in selecting a TRW A-type polyimide resin that would be suitable for fabrication of filament wound reinforced plastic structures is described. Several different formulations were evaluated after which the P105AC formulation was selected as the most promising. Procedures then were developed for preparing P105AC/S-glass roving prepreg and for fabricating filament wound structural composites. Composites were fabricated and then tested in order to obtain tensile and shear strength information. Small, closed-end cylindrical pressure vessels then were fabricated using a stainless steel liner and end fittings with a P105AC/S-glass polar wound overwrap. These pressure vessels were cured in an air circulating oven without augmented pressure. It is concluded that the P105AC resin system is suitable for filament winding; that low void content, high strength composites are obtained by the filament winding process; and that augmented pressure is not required to effect the fabrication of filament wound P105AC composites.
A method has been devised to enable the fabrication of lightweight pressure vessels from multilayer composite materials. This method is related to, but not the same as, the method described in gMaking a Metal- Lined Composite-Overwrapped Pressure Vessel h (MFS-31814), NASA Tech Briefs, Vol. 29, No. 3 (March 2005), page 59. The method is flexible in that it poses no major impediment to changes in tank design and is applicable to a wide range of tank sizes. The figure depicts a finished tank fabricated by this method, showing layers added at various stages of the fabrication process. In the first step of the process, a mandrel that defines the size and shape of the interior of the tank is machined from a polyurethane foam or other suitable lightweight tooling material. The mandrel is outfitted with metallic end fittings on a shaft. Each end fitting includes an outer flange that has a small step to accommodate a thin layer of graphite/epoxy or other suitable composite material. The outer surface of the mandrel (but not the fittings) is covered with a suitable release material. The composite material is filament- wound so as to cover the entire surface of the mandrel from the step on one end fitting to the step on the other end fitting. The composite material is then cured in place. The entire workpiece is cut in half in a plane perpendicular to the axis of symmetry at its mid-length point, yielding two composite-material half shells, each containing half of the foam mandrel. The halves of the mandrel are removed from within the composite shells, then the shells are reassembled and bonded together with a belly band of cured composite material. The resulting composite shell becomes a mandrel for the subsequent steps of the fabrication process and remains inside the final tank. The outer surface of the composite shell is covered with a layer of material designed to be impermeable by the pressurized fluid to be contained in the tank. A second step on the outer flange of each end fitting accommodates this layer. Depending on the application, this layer could be, for example, a layer of rubber, a polymer film, or an electrodeposited layer of metal. If the fluid to be contained in the tank is a gas, then the best permeation barrier is electrodeposited metal (typically copper or nickel), which can be effective at a thickness of as little as 0.005 in (.0.13 mm). The electrodeposited metal becomes molecularly bonded to the second step on each metallic end fitting. The permeation-barrier layer is covered with many layers of filament-wound composite material, which could be the same as, or different from, the composite material of the inner shell. Finally, the filament-wound composite material is cured in an ov
The focus of this study is on the suitability in the application of classical laminate theory analysis tools for filament wound pressure vessels with adhesive laminated joints in particular: pressure vessel wall performance, joint stiffness and failure prediction. Two 18-inch diameter 12-ply filament wound pressure vessels were fabricated. One vessel was fabricated with a 24-ply pyramid laminated adhesive double strap butt joint. The second vessel was fabricated with the same number of plies in an inverted pyramid joint. Results from hydrostatic tests are presented. Experimental results were used as input to the computer programs GENLAM and Laminate, and the output compared to test. By using the axial stress resultant, the classical laminate theory results show a correlation within 1% to the experimental results in predicting the pressure vessel wall pressure performance. The prediction of joint stiffness for the two adhesive joints in the axial direction is within 1% of the experimental results. The calculated hoop direction joint stress resultant is 25% less than the measured resultant for both joint configurations. A correction factor is derived and used in the joint analysis. The correction factor is derived from the hoop stress resultant from the tank wall performance investigation. The vessel with the pyramid joint is determined to have failed in the joint area at a hydrostatic pressure 33% value below predicted failure. The vessel with the inverted pyramid joint failed in the wall acreage at a hydrostatic pressure within 10% of the actual failure pressure.
Method and apparatus for enhancing the durability as well as the strength and stiffness of prepreg fiber tows of the sort used in composite materials are disclosed. The method involves adhering electrospun fibers onto the surface of such composite materials as filament-wound composite objects and the surface of prepreg fiber tows of the sort that are subsequently used in the production of composite materials of the filament-wound, woven, and braided sorts. The apparatus performs the methods described herein.
Composite materials offer significant weight savings in many aerospace applications. The toughness of the interface of fibers crossing at different angles often determines failure of composite components. A method for toughening the interface in fabric and filament wound components using directly electrospun thermoplastic nanofiber on carbon fiber tow is presented. The method was first demonstrated with limited trials, and then was scaled up to a continuous lab scale process. Filament wound tubes were fabricated and tested using unmodified baseline towpreg material and nanofiber coated towpreg.