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At least 127 records · Page 7

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NASA NTRS1979

Hydrogen chloride partitioning in a Titan III exhaust cloud diluted with ambient air

Measurements and analysis are presented of the partitioning of HCl between hydrochloric acid aerosol and gaseous HCl in a Titan III exhaust cloud, as the cloud is diluted with humid ambient air. Partitioning was determined by measuring the gaseous HCl concentration with a recently developed airborne Gas Filter Correlation detector and simultaneously with a chemiluminescence detector which measures total HCl. Although equilibrium predictions for HCl aerosol formation indicated that no HCl aerosol should exist in the exhaust cloud for the meteorological conditions of this launch, the measurements indicated significant HCl aerosol formation. These measurements will provide verification for advanced modeling programs now under development.

Sebacher, D. I.↗

NASA NTRS1999

The HERO Program: High-Energy Replicated Optics for a Hard-X-Ray Balloon Payload

We are developing high-energy replicated optics for a balloon-borne hard-x-ray telescope. When completed, the telescope will have around 150 square cm of effective collecting area up to 65 keV, and an angular resolution of around 30 arc seconds, half power diameter. When used in conjunction with an array of focal plane imaging detectors, for which Gas Scintillation Proportional Counters are under development, the payload will provide unprecedented sensitivity for pointed observations in the hard-x-ray band. We will present an overview of the High Energy Replicated Optics (HERO) program together with test data from the first mirror units. The overall sensitivity of the full payload, when flown on long- and ultra-long-duration balloon flights, will be compared with past and planned satellite-borne hard-x-ray missions.

Ramsey, B. D.↗

NASA NTRS1990

The atmosphere as particle detector

The possibility of using an inflatable, gas-filled balloon as a TeV gamma-ray detector on the moon is considered. By taking an atmosphere of Xenon gas there, or by extracting it on the moon, a layman's detector design is presented. In spite of its shortcomings, the exercise illustrates several of the novel features offered by particle physics on the moon.

Stanev, Todor↗

NASA NTRS1990

Discourse for slide presentation: An overview of chemical detection systems

A brief overview of some of the analytical techniques currently used in monitoring and analyzing permanent gases and selected volatile organic compound in air are presented. Some of the analytical considerations in developing a specific method are discussed. Four broad groups of hardware are discussed: compound class specific personal monitors, gas chromatographic systems, infrared spectroscopic systems, and mass spectrometric residual gas analyzer systems. Three types of detectors are also discussed: catalytic sensor based systems, photoionization detectors, and wet or dry chemical reagent systems. Under gas chromatograph based systems five detector systems used in combination with a GC are covered: thermal conductivity detectors, photoionization detectors, Fourier transform infrared spectrophotometric systems, quadrapole mass spectrometric systems, and a relatively recent development, a surface acoustic wave vapor detector.

Peters, Randy Alan↗

NASA NTRS1974

Three stage gas dilution system for calibration of air quality instrumentation

Tests were conducted on a three stage gas dilution system to evaluate the performance of the system for preparation of gas mixtures in the range of concentrations from 1 to 200 ppm. The test gas used in the evaluation was carbon monoxide. Mixtures of carbon monoxide and air were prepared in the gas dilution system and analyzed on stream with a commercially available infrared CO detector. Results showed the gas dilution system to be accurate to within 5, 3, and 2 percent in the respective ranges of 1-20 ppm, 20-50 ppm, and 50-200 ppm.

Gregory, G. L.↗

NASA NTRS2015

Color Changing Hydrogen Sensors

During the Space Shuttle Program, one of the most hazardous operation that occurred was the loading of liquid hydrogen (LH2) during fueling operations of the spacecraft. Due to hydrogen's low explosive limit, any amount leaked could lead to catastrophic event. Hydrogen's chemical properties make it ideal as a rocket fuel; however, the fuel is deemed unsafe for most commercial use because of the inability to easily detect the gas leaking. The increased use of hydrogen over traditional fossil fuels would reduce greenhouse gases and America's dependency on foreign oil. Therefore a technology that would improve safety at NASA and in the commercial sector while creating a new economic sector would have a huge impact to NASA's mission. The Chemochromic Detector for sensing hydrogen gas leakage is a color-changing detector that is useful in any application where it is important to know not only the presence but also the location of the hydrogen gas leak. This technology utilizes a chemochromicpigment and polymer matrix that can be molded or spun into rigid or pliable shapes useable in variable temperature environments including atmospheres of inert gas, hydrogen gas, or mixtures of gases. A change in color of the detector material indicates where gaseous hydrogen leaks are occurring. The irreversible sensor has a dramatic color change from beige to dark grey and remains dark grey after exposure. A reversible pigment changes from white to blue in the presence of hydrogen and reverts back to white in the presence of oxygen. Both versions of the sensor's pigments were comprised of a mixture of a metal oxide substrate and a hydro-chromic compound (i.e., the compound that changed color in the presence of hydrogen) and immediately notified the operator of the presence of low levels of hydrogen. The detector can be used in a variety of formats including paint, tape, caulking, injection molded parts, textiles and fabrics, composites, and films. This technology brings numerous benefits over the traditional hydrogen sensors: The technology has excellent temperature stability (4K to 373 K), it can be used in cryogenic fluid applications, it is easy to apply and remove; it requires no power to operate; it has a quick response time; the leak points can be detected visually or electronically; it is nonhazardous, thus environmentally friendly; it can be reversible or irreversible; it does not require on-site monitoring; has a long shelf life; the detector is very durable; and the technology is inexpensive to manufacture.

Chemochromic sensor↗

NASA NTRS2007

Implementation of Leak Test Methods for the International Space Station (ISS) Elements, Systems and Components

The International Space Station (ISS has Qualification and Acceptance Environmental Test Requirements document, SSP 41172 that includes many environmental tests such as Thermal vacuum & Cycling, Depress/Repress, Sinusoidal, Random, and Acoustic Vibration, Pyro Shock, Acceleration, Humidity, Pressure, Electromatic Interference (EMI)/Electromagnetic Compatibility (EMCO), etc. This document also includes (13) leak test methods for Pressure Integrity Verification of the ISS Elements, Systems, and Components. These leak test methods are well known, however, the test procedure for specific leak test method shall be written and implemented paying attention to the important procedural steps/details that, if omitted or deviated, could impact the quality of the final product and affect the crew safety. Such procedural steps/details for different methods include, but not limited to: - Sequence of testing, f or example, pressurization and submersion steps for Method I (Immersion); - Stabilization of the mass spectrometer leak detector outputs fo r Method II (vacuum Chamber or Bell jar); - Proper data processing an d taking a conservative approach while making predictions for on-orbit leakage rate for Method III(Pressure Change); - Proper Calibration o f the mass spectrometer leak detector for all the tracer gas (mostly Helium) Methods such as Method V (Detector Probe), Method VI (Hood), Method VII (Tracer Probe), Method VIII(Accumulation); - Usage of visibl ility aides for Method I (Immersion), Method IV (Chemical Indicator), Method XII (Foam/Liquid Application), and Method XIII (Hydrostatic/Visual Inspection); While some methods could be used for the total leaka ge (either internal-to-external or external-to-internal) rate requirement verification (Vacuum Chamber, Pressure Decay, Hood, Accumulation), other methods shall be used only as a pass/fail test for individual joints (e.g., welds, fittings, and plugs) or for troubleshooting purposes (Chemical Indicator, Detector Probe, Tracer Probe, Local Vacuum Chamber, Foam/Liquid Application, and Hydrostatic/Visual Inspection). Any isolation of SSP 41172 requirements have led to either retesting of hardware or accepting a risk associated with the potential system or component pressure integrity problem during flight.

Underwood, Steve↗

NASA NTRS1984

Helium ionization detection apparatus

In a gas chromatograph apparatus comprising a gas supply (He carrier gas), a sample injection apparatus, a chromatograph column, a He ion detector, and connecting tubes, a foreign gas (other than He) injection apparatus is installed between the sample injection apparatus and the detector. Mixing of the sample gas and foreign gas takes place readily, the sample gas is always maintained at a stable concentrator range, and accurate measurements are possible, especially at low sample gas concentrations.

Nagai, R.↗

NASA NTRS1972

Simple gas chromatographic system for analysis of microbial respiratory gases

Dual column ambient temperature system, consisting of pair of capillary columns, microbead thermistor detector and micro gas-sampling valve, is used in remote life-detection equipment for space experiments. Performance outweighs advantage gained by utilizing single-column systems to reduce weight, conserve carrier gas and operate at lower power levels.

Carle, G. C.↗

NASA NTRS1976

Ultraviolet corona detection sensor study

The feasibility of detecting electrical corona discharge phenomena in a space simulation chamber via emission of ultraviolet light was evaluated. A corona simulator, with a hemispherically capped point to plane electrode geometry, was used to generate corona glows over a wide range of pressure, voltage, current, electrode gap length and electrode point radius. Several ultraviolet detectors, including a copper cathode gas discharge tube and a UV enhanced silicon photodiode detector, were evaluated in the course of the spectral intensity measurements. The performance of both silicon target vidicons and silicon intensified target vidicons was evaluated analytically using the data generated by the spectroradiometer scans and the performance data supplied by the manufacturers.

Schmitt, R. J.↗

NASA NTRS1988

The Cosmic Ray Nuclei Experiment on the Spacelab-II mission

The Cosmic Ray Nuclei Experiment flown on the Spacelab-II mission was designed to measure the elemental composition of individual cosmic ray nuclei (Li to Ni) from 40 Gev/amu to several TeV/amu. The detector utilizes plastic scintillation counters for charge measurement, and gas Cerenkov and transition radiation detectors for energy measurements. The data analysis is in progress and results on the energy spectra are expected in the near future.

Grunsfeld, John Mace↗

NASA NTRS1991

Measurement of tropospheric carbon monoxide using gas filter radiometers

The measurement of tropospheric carbon monoxide with gas filter radiometers is examined on the basis of the MAPS experiment. The performance characteristics of an instrument that uses the MAPS detectors, broadband filters, and gas cells in a system similar to the GASCOFIL system described by Morrow and Nicholls (1985) is determined. The signal function for two carbon monoxide channels of the MAPS instrument as it was flown in 1981 is shown. The measurements of the lower pressure channel are weighted to a higher altitude. The signal function, when integrated over altitude and multiplied by the normalization constant, yields the value of the signal. Both signal functions approach zero at the top because the gas concentration approaches zero. The present data reduction technique assumes that there are no clouds in the field of view. If clouds are present, the inferred carbon monoxide mixing ratio is too high, and those points must be rejected from the data set.

Reichle, Henry G., Jr.↗

NASA NTRS1977

Evaluation of a hydrogen chloride detector for environmental monitoring

The paper describes a hydrogen chloride detector designed to monitor concentrations of hydrogen chloride gas in the ambient environment. The detector was developed for NASA for use in launch vehicle effluent monitoring. The detector operates on chemiluminescence principles with a lower detection limit of less than 5 x 10 to the -3rd ppm (by volume). The hydrogen chloride in the air sample reacts with a bromide-bromate coating in the inlet tube of the instrument producing bromine. Bromine is then quantitated by chemiluminescent oxidation of luminol. The visible light generated in the chemiluminescent reaction is proportional to the hydrogen chloride concentration of the sampled airstream. The detector is most suited to laboratory or field studies where hydrogen chloride is the dominant pollutant, as compared to the interfering species. Interferences include strong acids, acid-forming gases, and halogen gases. Of the interferences investigated the most serious in these groups are hydrochloric and sulfuric acid, sulfur dioxide, and chlorine, respectively. The detector has been in use since 1974 and has been found to be highly portable, rugged, and stable under extreme environmental conditions.

Gregory, G. L.↗

NASA NTRS2001

Buffer Gas Acquisition and Storage

The acquisition and storage of buffer gases (primarily argon and nitrogen) from the Mars atmosphere provides a valuable resource for blanketing and pressurizing fuel tanks and as a buffer gas for breathing air for manned missions. During the acquisition of carbon dioxide (CO2), whether by sorption bed or cryo-freezer, the accompanying buffer gases build up in the carbon dioxide acquisition system, reduce the flow of CO2 to the bed, and lower system efficiency. It is this build up of buffer gases that provide a convenient source, which must be removed, for efficient capture Of CO2 Removal of this buffer gas barrier greatly improves the charging rate of the CO2 acquisition bed and, thereby, maintains the fuel production rates required for a successful mission. Consequently, the acquisition, purification, and storage of these buffer gases are important goals of ISRU plans. Purity of the buffer gases is a concern e.g., if the CO, freezer operates at 140 K, the composition of the inert gas would be approximately 21 percent CO2, 50 percent nitrogen, and 29 percent argon. Although there are several approaches that could be used, this effort focused on a hollow-fiber membrane (HFM) separation method. This study measured the permeation rates of CO2, nitrogen (ND, and argon (Ar) through a multiple-membrane system and the individual membranes from room temperature to 193K and 10 kpa to 300 kPa. Concentrations were measured with a gas chromatograph that used a thermoconductivity (TCD) detector with helium (He) as the carrier gas. The general trend as the temperature was lowered was for the membranes to become more selective, In addition, the relative permeation rates between the three gases changed with temperature. The end result was to provide design parameters that could be used to separate CO2 from N2 and Ar.

Parrish, Clyde F.↗

NASA NTRS1991

Development of a miniaturized gas chromatograph-mass spectrometer with a microbore capillary column and an array detector

A review is presented of the demonstration of a miniaturized focal plane mass spectrograph using a microbore capillary column with an array detector to measure multiple mass spectra from narrow and closely eluted gas chromatograph peaks. It is shown that the system possesses high sensitivity and a high speed of spectral mass measurements. The combination of the capillary column with the miniaturized mass spectrograph is uniquely suited for the development of a field-portable, high-performance system.

Sinha, Mahadeva P.↗

NASA NTRS2004

Deployment of a Fast-GCMS System to Measure C2 to C5 Carbonyls, Methanol and Ethanol Aboard Aircraft

Through funding of this proposal, a fast response gas chromatograph/mass spectrometer (FGCMS) instrument to measure less than or equal to C4 carbonyl compounds and methanol was developed for the NASA GTE TRACE-P (Global Tropospheric Experiment, Transport And Chemical Evolution Over The Pacific) mission. The system consists of four major components: sample inlet, preconcentration system, gas chromatograph (GC), and detector. The preconcentration system is a custom-built cryogen-conservative system. The GC is a compact, custom-built unit that can be temperature programmed and rapidly cooled. Detection is accomplished with an Agilent Technologies 5973 mass spectrometer. The FGCMS instrument provides positive identification because the compounds are chromatographically separated and mass selected. During TRACE-P, a sample was analyzed every 5 minutes. The FGCMS limit of detection was between 5 and 75 pptv, depending on the compound. The entire instrument package is contained in a standard NASA instrument rack (106 cm x 61 cm x 135 cm), consumes less than 1200 watts and is fully automated with LabViEW 6i. Methods were developed or producing highly accurate gas phase standards for the target compounds and for testing the system in the presence of potential interferents. This report presents data on these tests and on the general overall performance of the system in the laboratory and aboard the DC-8 aircraft during the mission. Vertical profiles for acetaldehyde, methanol, acetone, propanal, methyl ethyl ketone, and butanal from FGCMS data collected over the entire mission are also presented.

Apel, Eric C.↗

NASA NTRS2021

The Imaging X-Ray Polarimetry Explorer (IXPE): Technical Overview IV

Scheduled to launch in late 2021,the Imaging X-ray Polarimetry Explorer (IXPE) is a Small Explorer Mission designed to open up a new window of investigation --X-ray polarimetry. The IXPE observatory features 3 identical telescopes each consisting of a mirror module assembly with a polarization-sensitive imaging x-ray detector at its focus. An extending boom, deployed on orbit, provides the necessary 4 m focal length. The payload sits atop a 3-axis stabilized spacecraft which, among other things, provides power, attitude determination and control, commanding, and telemetry to the ground. During its 2-year baseline mission, IXPE will conduct precise polarimetry for samples of multiple categories of x-ray sources, with follow-on observations of selected targets. IXPE is a partnership between NASA and the Italian Space Agency (ASI).

X-ray polarimetry↗

NASA NTRS1999

Survey of Fire Detection Technologies and System Evaluation/Certification Methodologies and Their Suitability for Aircraft Cargo Compartments

As part of the National Aeronautics and Space Administration (NASA) initiated program on global civil aviation, NIST is assisting Federal Aviation Administration in its research to improve fire detection in aircraft cargo compartments. Aircraft cargo compartment detection certification methods have been reviewed. The Fire Emulator-Detector Evaluator (FE/DE) has been designed to evaluate fire detection technologies such as new sensors, multi-element detectors, and detectors that employ complex algorithms. The FE/DE is a flow tunnel that can reproduce velocity, temperature, smoke, and Combustion gas levels to which a detector might be exposed during a fire. A scientific literature survey and patent search have been conducted relating to existing and emerging fire detection technologies, and the potential use of new fire detection strategies in cargo compartment areas has been assessed. In the near term, improved detector signal processing and multi-sensor detectors based on combinations of smoke measurements, combustion gases and temperature are envisioned as significantly impacting detector system performance.

Cleary, T.↗