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Applications of high power lasers

The use of computer generated, reflection holograms in conjunction with high power lasers for precision machining of metals and ceramics was investigated. The Reflection holograms which were developed and made to work at both optical wavelength (He-Ne, 6328 A) and infrared (CO2, 10.6) meet the primary practical requirement of ruggedness and are relatively economical and simple to fabricate. The technology is sufficiently advanced now so that reflection holography could indeed be used as a practical manufacturing device in certain applications requiring low power densities. However, the present holograms are energy inefficient and much of the laser power is lost in the zero order spot and higher diffraction orders. Improvements of laser machining over conventional methods are discussed and addition applications are listed. Possible uses in the electronics industry include drilling holes in printed circuit boards making soldered connections, and resistor trimming.

Angus, J. C.↗

Science and Technology Review January/February 2011

This month's issue has the following articles: (1) World's Most Intense X-Ray Laser Focuses on Livermore Science - Commentary by William H. Goldstein; (2) Groundbreaking Science with the World's Brightest X Rays - Experiments with x rays of unparalleled brightness and extremely short duration aim to reveal new information about atoms and molecules in motion; (3) From Data to Discovery - Ongoing control system enhancements at the National Ignition Facility bolster the understanding of experimental data and keep the system performing at its peak; (4) The Sun in All Its Splendor - Onboard the Solar Dynamics Observatory, Livermore-developed multilayer mirrors are enabling unprecedented full-disk, high-resolution images of the Sun; and (5) Drilling Deep into Plant Veins - A novel combination of imaging techniques is being used to understand the three-dimensional architecture of plant cell walls.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

Decommissioning Experience at Rokkasho; Standing Type Manipulator: A1000S for Dismantling Tasks - 16434

Decommissioning is a technical process which includes various steps and processes from the clean-up of radioactive materials to the progressive demolition of the plant. One of these steps is the cutting of subassemblies, like tanks, pipes or walls in small pieces suitable for the sorting and disposal. Different solutions are offered for this cutting work and can be grouped as following: - Chip forming - sawing, drilling, milling, turning etc. - Shearing - punching, stamping, scissoring. - Abrading - Grinding, lapping, polishing; water-jet. - Heat - flame cutting, plasma cutting, laser cutting. - Electro-Chemical - Etching, Electrical discharge machining (EDM). Each method has its limitations in accuracy, cost, and effect on the material. In 2013, Waelischmiller Engineering won a contract for two remote handling systems dedicated to the dismantling cell at Rokkasho Nuclear Fuel Reprocessing Facility in Japan. For this project, Inconel and other metals needed to be cut. One of the main cutting methods was decided to use of an angle grinder handled by a robotic arm. Because the use of the overhead systems (bridges and cranes) was difficult for this installation, it was determined, that the best alternative was a power manipulator A1000 installed on the floor with a pre-positioning system. The project proceeded to go forward with the adaptation of the standard A1000 with integration of a control system in a Cartesian coordinate frame; resulting in a heavy duty arm; A1000S with 6 degrees of freedom. The heavy duty power arm A1000S was developed and designed for mechanical cutting with an angle grinder, especially for thick and hard material for example stainless steel and Inconel. Cutting a thick material with an angle grinder requires repeatable precise linear motion, in order not to damage the disc. The angle grinder should be handled with a manipulator which can cut in all directions in a linear motion, since the objects which should be cut are usually very large and fixed in any direction For these requirements, the Cartesian control function was added to our standard power manipulator type A1000. In some cases, the decommissioning work includes repeated access routes or fixed access points that the manipulator arm has to pass repeatedly. For example a fixed point where the waste materials are collected, or repeated transport route that the arm has to go along for each step. For this requirement, the A1000S has been equipped with the 'Go To-Mode'. It is a 'teach and playback mode' which has been developed especially for remote operating manipulators. Quick direct teach, quick play function and an intuitive touch-panel layout are some of the features. With the Go To-Mode high working efficiency was achieved. After rigorous testing at Waelischmiller premises; the manipulator was delivered to JNFL in Rokkasho. It was found that the obtained functionality and precision can be applicable not only for the cutting with a disc grinder, but also the laser cutting method, which requires precise trajectory control. This paper will provide: - A project description, - Presentation of solution process, - Technical description of the A1000S, - Future Applications of the robotic Arm A1000S. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Inertial confinement fusion based on the ion-bubble trigger

Triggering the ion-bubble in an inertial confinement fusion, we have developed a novel scheme for the fast ignition. This scheme relies on the plasma cavitation by the wake of an intense laser pulse to generate an ion-bubble. The bubble acts both as an intense electron accelerator and as an electron wiggler. Consequently, the accelerated electrons trapped in the bubble can emit an intense tunable laser light. This light can be absorbed by an ablation layer on the outside surface of the ignition capsule, which subsequently drills it and thereby produces a guide channel in the pellet. Finally, the relativistic electron beam created in the bubble is guided through the channel to the high density core igniting the fusion fuel. The normalized beam intensity and beam energy required for triggering the ignition have been calculated when core is heated by the e-beam. In addition, through solving the momentum transfer, continuity and wave equations, a dispersion relation for the electromagnetic and space-charge waves has been analytically derived. The variations of growth rate with the ion-bubble density and electron beam energy have been illustrated. It is found that the growth rates of instability are significantly controlled by the ions concentration and the e-beam energy in the bubble.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

NDLGS project update

Recent results for laser and ESD processing for the NDLGS project will be reviewed. Conclusions are: (1) Short mix passes have profound effect on window T; (2) Multiple drill and re-weld at single location has been shown to be feasible and successful; (3) Kapton beam profiling method has been successfully developed. Comparison of 100 mm and 120 mm lenses gives reasonable and consistent results; (4) Manifold pumpdown data has been presented; (5) ESO results can be accurately predicted once a repeatable efficiency has been established; and (6) The electrode-workpiece geometry may play an important on ESO efficiency. Experiments are planned to investigate these effects.

36 MATERIALS SCIENCE↗

Photonic Doppler Velocimetry Probe Designed with Stereo Imaging

The velocity distribution of an imploding curved surface is measured with a miniature fiber-optic probe. The probe uses fiber matrix arrays that are focused onto different regions of this curved surface. A pyramid reflector deflects the interrogation onto specific regions of this curved surface. The fiber arrays record velocity along several hundred lines of sight with sub-nanosecond resolution. Reflected light from each spot on the moving surface is Doppler shifted with a small portion of this light propagating backwards through the launching fiber. The reflected light is mixed with a reference laser in a technique called Photonic Doppler velocimetry, providing continuous time records. Within the probe, seven groups of miniature optical relay lenses are grouped into a close-packed array, allowing the interrogation of seven regions of interest. A six-faceted pyramid reflector with a conical hole drilled into its center is used to direct the light beams onto different regions. To minimize back reflections, the fiber matrix arrays are index matched onto the first relay lens made of fused silica. The optical lens design minimizes the laser beam diameters and also provides excellent imaging capabilities. Therefore, two of the fiber matrix arrays are replaced by coherent bundles for stereo imaging recorded by a high-speed framing camera. This requires additional cutouts of the pyramid reflector to allow imaging overlap. Six additional 1.5 mm diameter incoherent bundles are attached to the edges of the pyramid reflector and are used for illumination. Precision metrology on the direction cosines of the trajectories is measured to satisfy environmental requirements for vibration and temperature.

photonic doppler velocimetry, PDV, pyramid reflect↗

SIMS microanalysis of the Strelley Pool Formation cherts and the implications for the secular-temporal oxygen-isotope trend of cherts

The significance of oxygen isotope ratios in Archean chert has long been debated. Cherts from the c. 3.4 Ga Strelley Pool Formation (SPF) (Pilbara Craton, Western Australia) host some of the oldest stromatolite and microfossil evidence for life, but the genesis and timing of silica cements has been unclear. Field relations, petrography and a combination of laser fluorination and in-situ SIMS measurements of δ 18 O in quartz show that bedded cherts of the SPF were originally precipitated as carbonates and were later widely replaced by quartz. Three localities were studied and analyzed for δ 18 O(Qz) in chert: 1) Camel Creek: foliated, metamorphosed, bedded cherts and meter-scale black chert veins; 2) Unconformity Ridge and ABDP8 drill core: stromatolitic and bedded chert overlying basal detrital quartz sandstone; and 3) the Trendall locality: “bedded” stromatolitic chert replacing original dolomite, low temperature hydrothermal quartz, and mm- to decimeter-scale chert-quartz veins. Laser fluorination (mm-scale) values of δ18O(Qz) range from: 14.2 to 18.2‰ VSMOW at Camel Creek; 9.3 to 18.9‰ at Unconformity Ridge; and 13.7 to 25.7‰ at Trendall. Values of δ 18 O(Qz) in cm to decimeter-scale hydrothermal chert veins cutting bedded carbonates at Trendall range from ca. 15 to 16‰, whereas “bedded cherts” are 17 to 26‰. These laser data include the highest δ 18 O values reported for cherts in Paleoarchean sediments and are up to 4‰ higher than the upper limit of ~22‰ reported in other studies, in apparent contrast to the long-standing secular-temporal trend which shows such high δ 18 O only in younger chert. However, analysis by laser fluorination at the 1-mm scale cannot resolve microtextures seen petrographically. In contrast, in-situ SIMS analyses can resolve petrographic microtextures and show δ 18 O(Qz) at 10-μm scale have an even greater range of 7–31‰ in “bedded” cherts at the Trendall locality, up to 9‰ above the secular-temporal trend. Textures observed optically at the Trendall locality were classified as: microquartz, mesoquartz, chalcedony, megaquartz veins, and cavity megaquartz. SEM-CL imaging shows two generations of meso- and megaquartz; bright CL with well-developed growth zoning, and dark CL with massive or mottled texture. Microquartz is the earliest textural generation of quartz and has a maximum δ 18 O(Qz) of ~22‰ by SIMS. Dark-CL mesoquartz has similar δ 18 O to microquartz and is interpreted to also be early. Bright-zoned-CL mesoquartz, which formed post-Archean, has even higher δ 18 O, up to 29‰. Vein megaquartz crosscuts most quartz generations and has a restricted range of δ 18 O, mostly from 16 to 19‰. Chalcedony pseudomorphs rhombic cavities and fractures, lines the edges of veins, and has similar δ 18 O to veins (16–19‰). Late cavity megaquartz is bright and zoned by CL, grows into late open cavities, and has the highest δ 18 O(Qz) values reported from the Pilbara, up to 31.3‰. Thus, the highest-δ 18 O quartz cements at the Trendall locality are the youngest and may be related to weathering. Early silicification and the formation of microquartz, chalcedony and low δ 18 O mesoquartz occurred during low temperature hydrothermal activity in the Archean. None of the SPF quartz examined is interpreted to have formed as a direct precipitate from Paleoarchean seawater. Thus, values of δ 18 O(Qz) do not record either water chemistry or temperature of Archean oceans. In-situ SIMS analysis shows that high-δ 18 O(Qz) values above 22‰ are only found in late-forming cavity megaquartz and bright-zoned-CL mesoquartz at the Trendall locality. The SPF results from our sample suite demonstrate the ability to resolve complex history using detailed petrography and SIMS analysis. Similar studies may show equal complexity of δ 18 O(Qz) data for other localities that are interpreted to show secular-temporal trends for chert. The apparent increase of δ 18 O(Qz) through time may reflect differences in diagenesis, and/or an inherent and previously unrecognized sampling bias that compares fundamentally different populations of quartz, such as Archean hydrothermal chert from volcanic greenstone belts, with unrelated Phanerozoic biogenic quartz.

59 BASIC BIOLOGICAL SCIENCES↗

Lunar Science

Lunar Laser Ranging will provide critical data to determine the initial composition of the Moon and the Earth-­Moon system. Specifically, LLR uniquely measures the properties of the lunar core via librations. LUNAR is advancing LLR: APOLLO recovery of Lunokhod 1, thus dramatically improving measurements of librations; Technology development of next generation retroreflectors; New drilling techniques. Dual-­use Low Frequency Radio arrays will constrain: Lunar ionosphere density via riometry; Nano-­size interplanetary dust particles responsible for surface weathering.

lunar laser ranging↗

Slopes To Prevent Trapping of Bubbles in Microfluidic Channels

The idea of designing a microfluidic channel to slope upward along the direction of flow of the liquid in the channel has been conceived to help prevent trapping of gas bubbles in the channel. In the original application that gave rise to this idea, the microfluidic channels are parts of micro-capillary electrophoresis (microCE) devices undergoing development for use on Mars in detecting compounds indicative of life. It is necessary to prevent trapping of gas bubbles in these devices because uninterrupted liquid pathways are essential for sustaining the electrical conduction and flows that are essential for CE. The idea is also applicable to microfluidic devices that may be developed for similar terrestrial microCE biotechnological applications or other terrestrial applications in which trapping of bubbles in microfluidic channels cannot be tolerated. A typical microCE device in the original application includes, among other things, multiple layers of borosilicate float glass wafers. Microfluidic channels are formed in the wafers, typically by use of wet chemical etching. The figure presents a simplified cross section of part of such a device in which the CE channel is formed in the lowermost wafer (denoted the channel wafer) and, according to the present innovation, slopes upward into a via hole in another wafer (denoted the manifold wafer) lying immediately above the channel wafer. Another feature of the present innovation is that the via hole in the manifold wafer is made to taper to a wider opening at the top to further reduce the tendency to trap bubbles. At the time of reporting the information for this article, an effort to identify an optimum technique for forming the slope and the taper was in progress. Of the techniques considered thus far, the one considered to be most promising is precision milling by use of femtosecond laser pulses. Other similar techniques that may work equally well are precision milling using a focused ion beam, or a small diamond-tipped drill bit.

Greer, Harold E.↗

Organic Molecules in the Sheepbed Mudstone, Gale Crater, Mars

The Sample Analysis at Mars (SAM) instrument on the Curiosity rover is designed to determine the inventory of organic and inorganic volatiles thermally released from solid samples using a combination of evolved gas analysis (EGA), gas chromatography mass spectrometry (GCMS), and tunable laser spectroscopy. Here we report on various chlorinated hydrocarbons (chloromethanes, chlorobenzene and dichloroalkanes) detected at elevated levels above instrument background at the Cumberland (CB) drill site, and discuss their possible sources.

Freissinet, C.↗

The ARADS Project as an Astrobiological Survey Mission Prototype

An astrobiological survey prior to human arrival will be important for preservation of signs of any existing or past evidence of Martian life, to reduce the risk of unintentional forward contamination of Martian environments in which terrestrial microbes might be able to gain a foothold (e.g., [1]), and to potentially protect the health of any human crews and enable their safe return to Earth. Evaluating for the presence of life and biosignatures may become a critical-path Mars exploration precursor in the not-so-far future, circa 2030-35. The near-subsurface, with its potential combination of volatiles, vapor exchange with the surface, and shelter from surface radiation, will be a primary initial target for in-situ astrobiological investigation. Sample acquisition, drilling and sample handling are key elements of robotic missions that target the subsurface [2], as well as near-surface ground ice deposits. In the mid 2000s, the Mars Astrobiology Field Laboratory (AFL) was proposed as a follow-on mission concept to the Mars Science Laboratory (MSL)/Curiosity rover mission [3]. The AFL would have included precision drilling to 2m, automated sample handling and remote processing of cores. However, the AFL concept needed further development and maturation. The Atacama Rover Astrobiology Drilling Studies (ARADS) project concept [4] was in part AFL-inspired. The 2014 ARADS concept included a medium sized rover, with habitability instruments, including the Phoenix Wet Chemistry Laboratory (WCL) [5], and an enhanced version of the ExoMars Mars Organic Molecule Analyzer (MOMA) Laser Desorption-Linear Ion Trap Mass Spectrometer (LITMS) [6]. ARADS likewise included two biosignature detection instruments -- the Signs of Life Detector (SOLID) immunoassay instrument [7,8] and the Chemical Laptop-derived [9] Planetary In-Situ Capillary Electrophoresis System (PISCES), while mitigating Planetary Protection-relevant contamination issues [10]. ARADS project objectives were to demonstrate the potential science return for such a mission in the context of the search for evidence of life, and technically to demonstrate the feasibility of roving with drilling missions to Mars. ARADS technology goals targeted analog-site demonstrations of automated drilling and sampling, integrated with its mobile habitability and biosignature detection instruments. And ARADS science operations goals developed remote science, contamination mitigation, and communications methods to enable simulating AFL-like science operations with time delays, directed by a remote science team[11]. Five subsequent Mars analog site field demonstrations (in Chile’s hyperarid Atacama Desert, 2016-19) provided a step-by-step development pathway for the ARADS platform’s science capabilities and systems integration, culminating in an integrated remote roving mission simulation in the final ARADS year (2019).

biosignatures↗

The Icebreaker Mission to Search for Life on Mars

The search for evidence of life on Mars is the ultimate motivation for its scientific exploration. The results from the Phoenix mission indicate that the high N. latitude ice-rich regolith at low elevations is likely to be a recently habitable place on Mars [Stoker et al., 2010]. The near-surface ice likely provided adequate water activity during periods of high obliquity, 3 to 10 Myr ago. Carbon dioxide and nitrogen are present in the atmosphere, and nitrates may be present in the soil. Together with iron in basaltic rocks and perchlorate in the soil they provide carbon and energy sources, and oxidative power to drive metabolism. Furthermore, the presence of organics is possible, as thermally reactive perchlorate would have prevented their detection by Viking and Phoenix. The Mars Icebreaker Life mission [McKay et al., 2013] focuses on the following science goals: (1) Search for biomolecular evidence of life; (2) Search for organic matter from either exogeneous or endogeneous sources using methods that are not effected by the presence of perchlorate; (3) Characterize oxidative species that produced reactivity of soils seen by Viking; and 4) Assess the habitability of the ice bearing soils. The Icebreaker Life payload (Figure 1) includes a 1-m rotary percussive drill that brings cuttings samples to the surface where they are delivered to three instruments (Fig. 1), the Signs of Life Detector (SOLID) [Parro et al., 2011] for biomolecular analysis, Laser Desorption Mass Spectrometer (LDMS) [??? 2015]) for broad spectrum organic analysis, and Wet Chemistry Laboratory (WCL) [Hecht et al., 2009] for detecting soluble species of nutrients and reactive oxidants. The Icebreaker payload fits on the Phoenix spacecraft and can land at the well-characterized Phoe-nix landing site in 2020 in a Discovery-class mission.

Carbon dioxide and nitrogen↗

Crustal Magnetic Fields

Cosmos 49, Polar Orbit Geophysical Observatory (POGO) (Orbiting Geophysical Observatory (OGO-2, 4 and 6)) and Magsat have been the only low-earth orbiting satellites to measure the crustal magnetic field on a global scale. These missions revealed the presence of long- wavelength (> 500 km) crustal anomalies predominantly located over continents. Ground based methods were, for the most part, unable to record these very large-scale features; no doubt due to the problems of assembling continental scale maps from numerous smaller surveys acquired over many years. Questions arose as to the source and nature of these long-wave length anomalies. As a result there was a great stimulant given to the study of the magnetic properties of the lower crust and upper mantle. Some indication as to the nature of these deep sources has been provided by the recent results from the deep crustal drilling programs. In addition, the mechanism of magnetization, induced or remanent, was largely unknown. For computational ease these anomalies were considered to result solely from induced magnetization. However, recent results from Mars Orbiter Laser Altimeter (MOLA), a magnetometer-bearing mission to Mars, have revealed crustal anomalies with dimensions similar to the largest anomalies on Earth. These Martian features could only have been produced by remanent magnetization, since Mars lacks an inducing field. The origin of long-wavelength crustal anomalies, however, has not been completely determined. Several large crustal magnetic anomalies (e.g., Bangui, Kursk, Kiruna and Central Europe) will be discussed and the role of future satellite magnetometer missions (Orsted, SUNSAT and Champ) in their interpretation evaluated.

Taylor, Patrick T.↗

Molecular Analyzer for Complex Refractory Organic-Rich Surfaces (MACROS)

The Molecular Analyzer for Complex Refractory Organic-rich Surfaces, MACROS, is a novel instrument package being developed at NASA Goddard Space Flight Center. MACROS enables the in situ characterization of a sample's composition by coupling two powerful techniques into one compact instrument package: (1) laser desorption/ionization time-of-flight mass spectrometry (LDMS) for broad detection of inorganic mineral composition and non-volatile organics, and (2) liquid-phase extraction methods to gently isolate the soluble organic and inorganic fraction of a planetary powder for enrichment and detailed analysis by liquid chromatographic separation coupled to LDMS. The LDMS is capable of positive and negative ion detection, precision mass selection, and fragment analysis. Two modes are included for LDMS: single laser LDMS as the broad survey mode and two step laser mass spectrometry (L2MS). The liquid-phase extraction will be done in a newly designed extraction module (EM) prototype, providing selectivity in the analysis of a complex sample. For the sample collection, a diamond drill front end will be used to collect rock/icy powder. With all these components and capabilities together, MACROS offers a versatile analytical instrument for a mission targeting an icy moon, carbonaceous asteroid, or comet, to fully characterize the surface composition and advance our understanding of the chemical inventory present on that body.

Getty, Stephanie A.↗

Laser Scanning System for Pressure and Temperature Paints

Acquiring pressure maps of aerodynamic surfaces is very important for improving and validating the performance of aerospace vehicles. Traditional pressure measurements are taken with pressure taps embedded in the model surface that are connected to transducers. While pressure taps allow highly accurate measurements to be acquired, they do have several drawbacks. Pressure taps do not give good spatial resolution due to the need for individual pressure tubes, compounded by limited space available inside models. Also, building a model proves very costly if taps are needed because of the large amount of labor necessary to drill, connect and test each one. The typical cost to install one tap is about $200. Recently, a new method for measuring pressure on aerodynamic surfaces has been developed utilizing a technology known as pressure sensitive paints (PSP). Using PSP, pressure distributions can be acquired optically with high spatial resolution and simple model preparation. Flow structures can be easily visualized using PSP, but are missed using low spatial resolution arrays of pressure taps. PSP even allows pressure distributions to be found on rotating machinery where previously this has been extremely difficult or even impossible. The goal of this research is to develop a laser scanning system for use with pressure sensitive paints that allows accurate pressure measurements to be obtained on various aerodynamic surfaces ranging from wind tunnel models to high speed jet engine compressor blades.

Sullivan, John↗

Laser Scanning System for Pressure and Temperature Paints

Acquiring pressure maps of aerodynamic surfaces is very important for improving and validating the performance of aerospace vehicles. Traditional pressure measurements are taken with pressure taps embedded in the model surface that are connected to transducers. While pressure taps allow highly accurate measurements to be acquired, they do have several drawbacks. Pressure taps do not give good spatial resolution due to the need for individual pressure tubes, compounded by limited space available inside models. Also, building a model proves very costly if taps are needed because of the large amount of labor necessary to drill, connect and test each one. The typical cost to install one tap is about $200. Recently, a new method for measuring pressure on aerodynamic surfaces has been developed utilizing a technology known as pressure sensitive paints (PSP). Using PSP, pressure distributions can be acquired optically with high spatial resolution and simple model preparation. Flow structures can be easily visualized using PSP, but are missed using low spatial resolution arrays of pressure taps. PSP even allows pressure distributions to be found on rotating machinery where previously this has been extremely difficult or even impossible. The goal of this research is to develop a laser scanning system for use with pressure sensitive paints that allows accurate pressure measurements to be obtained on various aerodynamic surfaces ranging from wind tunnel models to high speed jet engine compressor blades.

Sullivan, John↗