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At least 127 records · Page 7

Ultrashort Pulse Laser Surface Processing Techniques for Sterilization of Metal Surfaces for Planetary Protection

To prevent forward contamination from microbes aboard spacecraft intended to search for extraterrestrial life, there is a need for effective sterilization methods. However, current techniques are both time-consuming and expensive. For example, dry heat sterilization requires removal from the assembly site and several days of treatment. Furthermore, some components such as optics and electronics are not compatible with current sterilization techniques. Here, we report the latest results in our development of a novel femtosecond laser processing technique for the rapid sterilization of spacecraft hardware. Femtosecond lasers produce extremely high photon fluxes (10^29 photons/sec*cm^2, ~0.03 J/cm^2) in extremely short pulses, which can inactivate even stress-tolerant microbial spores with minimal damage to the spacecraft surface. Aluminum coupons were inoculated with specific densities of Bacillus subtilis bacterial endospores. These coupons were treated with various laser illumination parameters. Afterward, metal coupon samples were assayed for viable spores using a polyvinyl alcohol (PVA) peel, serial dilution, and plating for colony-forming units (CFU). Results indicate that with high enough energy density and pulse counts, most bacterial spores are inactivated with minimal damage to the metal. The sterilization is dependent on both the fluence and pulse count. In addition, femtosecond pulses are more effective than longer pulses for inactivation. These experiments have consistently achieved 4-log reduction in viable spores. Sterilization has been achieved on both flat metal coupons and non-flat surfaces with microchannels, with a slight reduction in sterilization efficiency on the uneven surface. The application of air flow during laser processing was also investigated as a way to remove spores that are dislodged from the surface by the laser illumination, which would contribute to the reduction of spacecraft bioburden. With laser processing technology rapidly evolving, our results support the possibility of an extremely rapid, in-situ surface sterilization method for use in spacecraft assembly clean rooms.

Kaleb McQuillan↗

Dual laser diode array emission coherently summed in an external cavity

The output power from two ten-element laser diodes arrays has been efficiently summed in an external cavity to obtain a coherent, continuous wave beam. In this technique, laser emission from each front surface antireflection coated diode array is stimulated by injection of emission from a second such array. This method was also applied to single-element diode lasers. The output beam characteristics such as spectral distribution, far-field and near-field beam patterns, and overall efficiency have been measured.

Hemmati, Hamid↗

Optical detection of pulsed surface particle displacements

The detection of acoustic surface wave pulses by a wideband differential interferometric laser technique which is insensitive to low frequency noise is described. System bandwidth is determined by the relationship between acoustic wavelength and the variable spacing between two laser probe beams focused on the solid surface which supports the waves. Theoretical sensitivity to surface displacement amplitude is equal to, or better than, that of other electrooptical techniques. Response to an ideal step function displacement is analyzed and experimental measurements of gated 2.5 MHz pulses generated on an aluminized pyrex plate are discussed. Potential application in the characterization of acoustic emission in composites is described.

Zerwekh, P. S.↗

Resonant Doppler velocimetry in supersonic nitrogen flow

The development of the Resonant Doppler Velocimeter (RDV) is discussed. It is a new nonintrusive laser technique for flow diagnosis. The RDV technique is applied to supersonic nitrogen flow with sodium atoms as tracer particles. The measurements are achieved by shining a tunable single frequency laser beam into the flow. The resonant absorption spectrum of the seeded species is determined by observing the fluorescence signal intensity as a function of excitation wavelength. By comparing the peak absorption wavelength with a reference frequency marker, the flow velocity along the excitation beam can be obtained through the Doppler shift relation. By fitting the spectrum with a theoretical line profile, the static temperature and pressure of the flow an be determined.

Cheng, S. W. S.↗

Comparison of experimental and computational techniques for plane mixing layers

In this paper, results from two experimental and two computational investigations of plane turbulent mixing layers are presented and compared. The experimental results include flow visualization data using the smoke laser technique and mean flow and turbulence measurements obtained with hot X-wires and a two-component LDV. Reasonably good agreement is found among these techniques, at least for turbulence quantities up to second order. Reynolds-averaged computations are successful at capturing the complete evolution of the mixing layer, including wake effects in the near field and approach to self-preservation in the far field. The two-dimensional vortex method shows excellent qualitative and quantitative agreement with measured data for the forced mixing layer. For the unforced layer, the results seem to indicate that a three-dimensional computation may be necessary.

Mehta, R. D.↗

Surface and subsurface characterization of laser-interference structured Ti6Al4V

Ti6Al4V specimens were exposed to high-energy laser pulses of 1.24 J/cm 2 fluences per pulse using a two-beam optical configuration to attain laser-interference. In addition to the formation of periodic surface textures by laser-interference, scanning electron microscope (SEM) images demonstrated several microstructural changes on the surface processed. Moreover, the surface and subsurface of Ti6Al4V specimens were characterized for the as-received and laser-interference processed conditions using x-ray photoelectron spectroscopy (XPS) and electron energy dispersive spectroscopy (EDS). The XPS data showed that this laser technique is effective at removal of surface contaminants for Ti6Al4V. The XPS analysis also revealed the formation of an oxy-nitride layer on the laser treated material. Finally, the microstructure analysis indicates that grain refinement, dendrite and twin structures were found near the surface due to laser processing.

36 MATERIALS SCIENCE↗

Optical detection of pulsed surface particle displacements

The detection of acoustic surface wave pulses by a wideband differential interferometric laser technique which is insensitive to low frequency noise is described. System bandwidth is determined by the relationship between acoustic wavelength and the variable spacing between two laser probe beams focused on the solid surface which supports the waves. Response to an ideal step function displacement is analyzed and experimental measurements of gated 2.5 MHz pulses generated on an aluminized pyrex plate are discussed.

Zewekh, P. S.↗

A survey of laser lightning rod techniques

The work done to create a laser lightning rod (LLR) is discussed. Some ongoing research which has the potential for achieving an operational laser lightning rod for use in the protection of missile launch sites, launch vehicles, and other property is discussed. Because of the ease with which a laser beam can be steered into any cloud overhead, an LLR could be used to ascertain if there exists enough charge in the clouds to discharge to the ground as triggered lightning. This leads to the possibility of using LLRs to test clouds prior to launching missiles through the clouds or prior to flying aircraft through the clouds. LLRs could also be used to probe and discharge clouds before or during any hazardous ground operations. Thus, an operational LLR may be able to both detect such sub-critical electrical fields and effectively neutralize them.

Barnes, Arnold A., Jr.↗

An airborne lidar instrument for detection of OH using the technique of laser-induced fluorescence

Under suitable laboratory conditions, it has been demonstrated that the laser-induced fluorescence (LIF) measurement technique is sensitive enough to detect single atoms and molecules. This potential sensitivity has provided motivation for the development of this technique for ambient OH measurements. The present paper is concerned with an airborne lidar instrument for measuring OH concentration as used for the NASA GTE/CITE (Global Tropospheric Experiment/Chemical Instrumentation Test and Evaluation) intercomparison experiments during the fall of 1983 and the spring of 1984. A description is given of a working airborne instrument for measurements of OH in ambient air. The detection sensitivity demonstrated in the experiments should be sufficient for routine measurements in areas in which the OH concentration is in the range of high 1,000,000 molecule per cu cm or higher.

Davis, L. I., Jr.↗

Non-Intrusive Laser-Induced Imaging for Speciation and Patternation in High Pressure Gas Turbine Combustors

The next generation of was turbine combustors for aerospace applications will be required to meet increasingly stringent constraints on fuel efficiency, noise abatement, and emissions. The power plants being designed to meet these constraints will operate at extreme conditions of temperature and pressure, thereby generating unique challenges to the previously employed diagnostic methodologies. Current efforts at NASA Glenn Research Center (GRC) utilize optically accessible, high pressure flametubes and sector combustor rigs to probe, via advanced nonintrusive laser techniques, the complex flowfields encountered in advanced combustor designs. The fuel-air mixing process is of particular concern for lowering NO(x) emissions generated in lean, premixed engine concepts. Using planar laser-induced fluorescence (PLIF) we have obtained real-time, detailed imaging of the fuel spray distribution for a number of fuel injector over a wide range of operational conditions that closely match those expected in the proposed propulsion systems. Using a novel combination of planar imaging, of fuel fluorescence and computational analysis that allows an examination of the flowfield from any perspective, we have produced spatially and temporally resolved fuel-air distribution maps. These maps provide detailed insight into the fuel injection at actual conditions never before possible, thereby greatly enhancing the evaluation of fuel injector performance and combustion phenomena.

Locke, Randy J.↗

A DFT-based kinetic Monte Carlo simulation of multiphase oxide-metal thin film growth

Functional thin films of nanoscale metal pillars in oxide or nitride matrices known as vertically aligned nanocomposite (VAN) have gained much interest owing to their unique strain-coupled and highly anisotropic properties. So far, the deposition of these films has been explored mostly experimentally. In this work, a density functional theory (DFT)-based kinetic Monte Carlo simulation model using Bortz–Kalos–Lebowitz algorithm was developed to understand the growth of VAN films deposited by pulsed laser technique on mismatching substrates. The model has been parameterized and applied to understand the kinetics of growth thin films consisting of Au pillars in CeO2 matrix deposited on SrTiO3 substrates. The effects of pulsed laser deposition (PLD) conditions including the pulse frequency, deposition flux, and substrate temperature were explored. The simulations indicate that the Au pillar size and shape exhibit significant dependence on the PLD conditions. Namely, increasing the temperature increases the average pillar size and lowers the pillar density, and vice versa. In addition, the simulations revealed that increasing the deposition rate results in lowering the average pillar size and increasing the density. Particularly, the DFT results suggest that Au pillar size can be tuned during the initial growth of the first monolayer due to the significantly low activation barrier. Our analysis showed that the relationship between the average pillar size and pillar density is influenced by the kinetics. Furthermore, autocorrelation analysis showed that pillars self-organize in quasi-ordered patterns at certain windows of the deposition conditions, which is attributed to the complex nature of the chemical interactions in the system, the kinetics, and the deposition parameters.

Physics↗

Shot noise limited detection of OH using the technique of laser-induced fluorescence

Nearly shot-noise limited detection of OH using the technique of laser-induced fluorescence is reported. A LIDAR configuration is used to excite fluoresence in a large volume and a narrow-bandwidth interference filter provides spectral discrimination. This arrangement alleviates the effect of ozone interference and facilitates image processing at relatively close distances. The detection limit is determined mainly by the short-noise of the solar background. Ground-based measurements in Dearborn indicate a detection limit of better than 1 x 10 to the 6th power OH/cubic cm over a forty-minute acquisition period. Under favorable conditions, a comparable detection limit was also observed for airborne measurements.

Bakalyar, D. M.↗

Laser prospects for SPS and restoration of the ozone layer

Large-scale applications of high-power lasers are considered (special experiments are described to confirm the feasibility of these applications) to achieve also large-scale environmental advantages. The possibility of producing electric energy by Laser-Solar Power Satellites in the near future is discussed. A full-scale experimental L-SPS satellite is suggested as a module of a global space energy network. Electric power of about 10 MW at the surface of the Earth is achievable as a result of energy conversion of laser radiation. L-SPS is based on the greatest advantages of present optics and laser techniques. Specialized-scale experiments are carried out and described. L-SPS project could provide real electricity for consumers not later than by highly developed fusion techniques, and the environmental aftereffects are quite favorable. A new method of power supply for satellites is suggested, based on the connection of an on-board electric circuit directly with the ground-based power grid by means of laser beams.

Kruzhilin, Yuri↗

High resolution spectral measurement of the HNO3 11.3-micron band using tunable diode lasers

High resolution spectra in the region of the 2-nu9 band of nitric acid have been obtained for selected portions of the HNO3 spectrum using tunable diode laser techniques. Continuous spectra are presented from 891.25/cm to 898.77/cm, with a spectral resolution less than or equal to 0.001/cm (30 MHz). Absolute line intensities and line positions are presented. Absolute wavelength calibration was obtained by frequency mixing the diode laser with a C(13)O2(16) isotope laser. Self and foreign gas (N2) broadening coefficients were iteratively calculated from the experimental data and were determined.

Brockman, P.↗

Intrusive and nonintrusive measurements of flow properties in arc jets

While numerous diagnostic techniques are available for determining the flow properties of arc jets, these have to be used complementarily in order to cover all the requisite information. Although intrusive techniques disturb the flow, they yield much information. The determination of total enthalpy remains a major challenge, and accurate heat-flux measurements entail knowledge of atom recombination and chemical energy recombination coefficients. Such state-specific methods as the spectroscopic and laser techniques are useful in understanding the chemistry and nonequilibrium reaction and excitation rates of the flow.

Scott, Carl D.↗