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Fabrication and characterization of net-shaped iron nitride-amine-epoxy soft magnetic composites
Soft magnetic composites (SMCs) offer a promising alternative to electrical steels and soft ferrites in high performance motors and power electronics. They are ideal for incorporation into passive electronic components such as inductors and transformers, which require a non-permanent magnetic core to rapidly switch magnetization. As a result, there is a need for materials with the right combination of low coercivity, low magnetic remanence, high relative permeability, and high saturation magnetization to achieve these goals. Iron nitride is an attractive soft magnetic material for incorporation into an amine/epoxy resin matrix. This permits the synthesis of net-shaped SMCs using a “bottom-up” approach for overcoming the limitations of current state-of-the-art SMCs made via conventional powder metal processing techniques. In this work we present the fabrication of various net-shaped, iron nitride-based SMCs using two different amine/epoxy resin systems and their magnetic characterization. The maximum volume loading of iron nitride reached was ~77% via hot pressing, which produced SMCs with a saturation magnetic polarization (J s ) of ~0.9 T, roughly 2–3 times the J s of soft ferrites.
The Phase Diagram and Exotic Magnetostrictive Behaviors in Spinel Oxide Co(Fe1−xAlx)2O4 System
We report the magnetic and magnetostrictive behaviors of the pseudobinary ferrimagnetic spinel oxide system (1−x)CoFe2O4–xCoAl2O4 [Co(Fe1−xAlx)2O4], with one end-member being the ferrimagnetic CoFe2O4 and the other end-member being CoAl2O4 that is paramagnetic above 9.8 K. The temperature spectra of magnetization and magnetic susceptibility were employed to detect the magnetic transition temperatures and to determine the phase diagram of this system. Composition dependent and temperature dependent magnetostrictive behaviors reveal an exotic phase boundary that separates two ferrimagnetic states: At room temperature and under small magnetic fields (∼500 Oe), Fe-rich compositions exhibit negative magnetostriction while the Al-rich compositions exhibit positive magnetostriction though the values are small (<10 ppm). Moreover, the compositions around this phase boundary at room temperature (x = 0.35, 0.4, 0.45, 0.5) exhibit near-zero magnetostriction and enhanced magnetic susceptibility, which may be promising in the applications for magnetic cores, current sensors, or magnetic shielding materials.
Improved process of fabricating ferrite cores for magnetic logic circuits
Method of processing magnetic ferrite structures enhances their partially set-state properties, so that the threshold magnetomotive force required to produce a specified change of flux is increased.
Core Losses In Three Alloys
Report describes experimental investigation of core losses and dynamic magnetic flux densities as functions of magnetomotive force of three soft magnetic materials under sine-wave voltage excitation at frequencies from 1 to 50 kHz and at temperatures from 23 to 300 degrees C. Prompted by need for data to design magnetic cores for efficient, lightweight power supplies operating in harsh environments.
CORE: Frustrated Magnets, Charge Fractionalization and QCD
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A Uniform-Field Air-Core Bending Magnet "The Electron Pipe"
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SYNTHETIC OBSERVATIONS OF MAGNETIC FIELDS IN PROTOSTELLAR CORES
The role of magnetic fields in the early stages of star formation is not well constrained. In order to discriminate between different star formation models, we analyze 3D magnetohydrodynamic simulations of low-mass cores and explore the correlation between magnetic field orientation and outflow orientation over time. We produce synthetic observations of dust polarization at resolutions comparable to millimeter-wave dust polarization maps observed by the Combined Array for Research in Millimeter-wave Astronomy and compare these with 2D visualizations of projected magnetic field and column density. Cumulative distribution functions of the projected angle between the magnetic field and outflow show different degrees of alignment in simulations with differing mass-to-flux ratios. The distribution function for the less magnetized core agrees with observations finding random alignment between outflow and field orientations, while the more magnetized core exhibits stronger alignment. We find that fractional polarization increases when the system is viewed such that the magnetic field is close to the plane of the sky, and the values of fractional polarization are consistent with observational measurements. The simulation outflow, which reflects the underlying angular momentum of the accreted gas, changes direction significantly over over the first ∼0.1 Myr of evolution. This movement could lead to the observed random alignment between outflows and the magnetic fields in protostellar cores.
Magnetic core/shell-type composites composed of coarse FePt particles coated with finely powdered iron nitride
Highlights: • Magnetic core/shell-type composites were prepared on α″-Fe{sub 16}N{sub 2}-like compound with FePt core. • α″-Fe{sub 16}N{sub 2}-like compound grew epitaxially on the FePt core. • Magnetic coupling increased the magnetic coercivity of α″-Fe{sub 16}N{sub 2}-like compound. - Abstract: Although α″-Fe{sub 16}N{sub 2}-like compounds exhibit enhanced magnetization compared to α-Fe, it is important to increase their magnetic coercivity to obtain new hard magnetic materials for electric vehicle application. In the present work, coarse FePt particles were coated with finely powdered Fe{sub 3}O{sub 4} produced by the hydrolysis of Fe(acac){sub 3} in benzyl alcohol. This Fe{sub 3}O{sub 4} coating layer was subsequently reduced under hydrogen and then nitrided by ammonolysis at 150 °C to obtain a dual-phase mixture of an α″-Fe{sub 16}N{sub 2}-like compound (referred to herein as “α″-Fe{sub 16}N{sub 2}”) and residual α-Fe. The (“α″-Fe{sub 16}N{sub 2}” + α-Fe){sub 1-x}/(FePt){sub x} composite particles for which x = 0.2, 0.4 or 0.6 generated smooth magnetization hysteresis curves, and the magnetic coercivity of these materials increased with increases in the proportion of FePt. Magnetic coupling was clearly evident between the core and shell regions in the composite powder for which x = 0.6, as demonstrated by a plot of the Wohlfarth interaction against the magnetic field. Transmission electron microscopy images confirmed magnetic coupling between the coarse FePt particles (several hundred nm in diameter) and the coating of fine mixed particles (several tens of nm in diameter) of “α″-Fe{sub 16}N{sub 2}” and α-Fe. The “α″-Fe{sub 16}N{sub 2}” crystals forming the particle shell were found to grow epitaxially, aligning their c-axes parallel to that of the tetragonal FePt.
Gapless core reactor
A gapless core reactor includes a saturable magnetic core having reactor legs without air gaps and multiple windings. The windings are each wound around a common leg, spaced apart from each other and connected in counter series. The windings are configured such that a magnetic flux generated from an alternating current flowing through the windings generates a plurality of substantially equal and counter magnetic fluxes flowing through two or more separate magnetic circuits.
Performance of the NASA Digitizing Core-Loss Instrumentation
The standard method of magnetic core loss measurement was implemented on a high frequency digitizing oscilloscope in order to explore the limits to accuracy when characterizing high Q cores at frequencies up to 1 MHz. This method computes core loss from the cycle mean of the product of the exciting current in a primary winding and induced voltage in a separate flux sensing winding. It is pointed out that just 20 percent accuracy for a Q of 100 core material requires a phase angle accuracy of 0.1 between the voltage and current measurements. Experiment shows that at 1 MHz, even high quality, high frequency current sensing transformers can introduce phase errors of a degree or more. Due to the fact that the Q of some quasilinear core materials can exceed 300 at frequencies below 100 kHz, phase angle errors can be a problem even at 50 kHz. Hence great care is necessary with current sensing and ground loops when measuring high Q cores. Best high frequency current sensing accuracy was obtained from a fabricated 0.1-ohm coaxial resistor, differentially sensed. Sample high frequency core loss data taken with the setup for a permeability-14 MPP core is presented.
Verification of 5D continuum gyrokinetic code COGENT: Studies of kinetic drift wave instability
COGENT (Continuum Gyrokinetic Edge New Technology) is a kinetic plasma simulation code that is being developed by the edge simulation laboratory (ESL) collaboration. The original version of the code has been developed in a 4D phase space (2D configuration space and 2D velocity space) to address kinetic plasma phenomena in a complex magnetic field geometry including the core, magnetic separatrix, and scrape-off layer regions. This paper is focused on extending the original 4D phase space to a 5D phase space (3D2V) to address full kinetic turbulences in a tokamak edge region. Here, we report on the current status of 5D COGENT, which presently operates in a shear-less, simple slab geometry. As a verification study, we use the problems of collision-less drift wave instability (universal instability) including its modification in the presence of collisional effects. The simulation model includes the gyrokinetic equations for ion and electron species coupled to the long-wavelength limit of the gyro-Poisson equation. Collisional effects are represented by the Krook collision model. Linear analytical results for the drift mode growth rate and real frequency are recovered, and the non-linear stage is modelled and analysed as well. In addition, extensive 5D runs have been performed to address the effects of the drift wave instability on blob/filamentary structures characteristic of a tokamak edge. Finally, a helical-shaped potential perturbation is observed to grow exponentially in time while spinning around the filament axis with electron drift frequency.
The orbital record in stratigraphy
Orbital signals are being discovered in pre-Pleistocene sediments. Due to their hierarchical nature these cycle patterns are complex, and the imprecision of geochronology generally makes the assignment of stratigraphic cycles to specific orbital cycles uncertain, but in sequences such as the limnic Newark Group under study by Olsen and pelagic Cretaceous sequence worked on by our Italo-American group the relative frequencies yield a definitive match to the Milankovitch hierarchy. Due to the multiple ways in which climate impinges on depositional systems, the orbital signals are recorded in a multiplicity of parameters, and affect different sedimentary facies in different ways. In platform carbonates, for example, the chief effect is via sea-level variations (possibly tied to fluctuating ice volume), resulting in cycles of emergence and submergence. In limnic systems it finds its most dramatic expression in alternations of lake and playa conditions. Biogenic pelagic oozes such as chalks and the limestones derived from them display variations in the carbonate supplied by planktonic organisms such as coccolithophores and foraminifera, and also record variations in the aeration of bottom waters. Whereas early studies of stratigraphic cyclicity relied mainly on bedding variations visible in the field, present studies are supplementing these with instrumental scans of geochemical, paleontological, and geophysical parameters which yield quantitative curves amenable to time-series analysis; such analysis is, however, limited by problems of distorted time-scales. My own work has been largely concentrated on pelagic systems. In these, the sensitivity of pelagic organisms to climatic-oceanic changes, combined with the sensitivity of botton life to changes in oxygen availability (commonly much more restricted in the Past than now) has left cyclic patterns related to orbital forcing. These systems are further attractive because (1) they tend to offer depositional continuity, and (2) presence of abundant microfossils yields close ties to geochronology. A tantalizing possibility that stratigraphy may yield a record of orbital signals unrelated to climate has turned up in magnetic studies of our Cretaceous core. Magnetic secular variations here carry a strong 39 ka periodicity, corresponding to the theoretical obliquity period of that time - Does the obliquity cycle perhaps have some direct influence on the magnetic field?
Materials for efficient high-flux magnetic bearing actuators
Magnetic bearings have demonstrated the capability for achieving positioning accuracies at the nanometer level in precision motion control stages. This makes possible the positioning of a wafer in six degrees of freedom with the precision necessary for photolithography. To control the position of an object at the nanometer level, a model of the magnetic bearing actuator force-current-airgap relationship must be accurately obtained. Additionally, to reduce thermal effects the design of the actuator should be optimized to achieve maximum power efficiency and flux density. Optimization of the actuator is accomplished by proper pole face sizing and utilizing a magnetic core material which can be magnetized to the highest flux density with low magnetic loss properties. This paper describes the construction of a magnetic bearing calibration fixture designed for experimental measurement of the actuator force characteristics. The results of a material study that review the force properties of nickel-steel, silicon-steel, and cobalt-vanadium-iron, as they apply to magnetic bearing applications are also presented.
FNAL PIP-II Accumulator Ring
The FNAL accelerator complex is poised to reach MW neutrino beams on target for the exploration of the dark sector physics and rare physics program spaces. Future operations of the complex will include CW linac operations at beam intensities that have not been seen before \cite{PIP2,RCS_LOI}. The ambitious beam program relies on multi-turn H$^{-}$ injection into the FNAL Booster and then extracted into delivery rings or the Booster Neutrino Beam (BNB) 8 GeV HEP program. A new rapid-cycling synchrotron (RCS) will be required to reach the LBNF goal of 2.4 MW because of intense space-charge limitations. There are many accelerator engineering challenges that are already known and many that will be discovered. This proposal calls for an intermediate step that will both facilitate the operation of Booster in the PIP-II era and gain operational experience associated with high power injection rings. This step includes the design, construction and installation of a 0.8 GeV accumulator ring (upgradeable to 1+ GeV) to be located in the PIP-II Booster Transfer Line (BTL). The PIP-II accumulator ring (PAR) may be primarily designed around permanent magnets or use standard iron core magnet technology with an aperture selected to accommodate the desired high intensity protons at 0.8 GeV.
A versatile and sensitive balanced magnetic comparator.
Basic circuit, sensitivity and mode of operation of balanced magnetic core comparator
Feasibility and electromagnetic analysis of a REBCO superconducting undulator
Recent advances in second-generation (2G) high temperature superconducting (HTS) coated conductors (CCs) have made them very attractive for new applications such as undulators. In this study, we have, for the first time, experimentally evaluated a design to validate applicability of 2G-HTS tapes for next generation undulator magnetic structures. A two-period undulator magnetic core was fabricated and 2G-HTS CCs were successfully wound onto the undulator core. The performance of the undulator magnetic structure was investigated and the highest engineering current density, J e , in such configuration reported yet was obtained. A new U-slit tape configuration was used to reduce the number of resistive joints and it was shown that with this new technique affordable levels of resistance values can be achieved for short length undulators. The ferromagnetic core was designed such as to accommodate winding the U-slit tapes. Finally, test results indicated that the winding and the soldering procedures are successful and do not deteriorate the performance of the 2G-HTS tapes.