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At least 127 records · Page 7

Procedure for dispersing fiber bundles

Fiber bundles are dispersed and fibers are cleaned within enclosed container; therefore, safety clothing, masks, and eye protection are not required. Procedure also could be used wherever materials, such as fiberglass or insulation, require dispersion, fluffing, or cleaning. Process could be automated into continuous operation for handling large quantities of fiber.

Padilla, D.↗

SRB attach ring phenolic TPS fishtail seal evaluation tests

The SRB attach ring is thermally protected with layered phenolic cloth fairings that are fastened to the ring. The gap between the fairings and the motor case is closed off with a rubber seal of a fishtail cross sectional shape bonded to the phenolic. On both the STS-1 and STS-2 flights this gap was discovered to vary anywhere from an intended gap of 0.375 in. to an actual measured gap of 0.60 in. due to tolerances. Tests were conducted with and without a 0.25 in. thick cork shim placed under the seal with a 0.60 in. gap under the phenolic TPS to determine and compare the performance of the seal in the two different configurations. To alleviate the difficult and costly procedure of installing the cork shim under the seal, especially after phenolic TPS mounting on the attach ring, large fishtail seals of idential Elder gray silicon material and two different hardnesses were tested. A similar matrix of tests was conducted with this new large fishtail seal, and seals with both type hardnesses performed well regardless of whether or not the seal was bonded in the phenolic at the front of the seal groove. Similar results had been obtained with the original small fishtail seal which performed adequately with the 0.25 in. cork shim under it.

Karu, Z. S.↗

Analysis of International Space Station Vehicle Materials on MISSE 6

The International Space Station Materials and Processes team has multiple material samples on MISSE 6, 7 and 8 to observe Low Earth Orbit (LEO) environmental effects on Space Station materials. Optical properties, thickness/mass loss, surface elemental analysis, visual and microscopic analysis for surface change are some of the techniques employed in this investigation. Results for the following MISSE 6 samples materials will be presented: deionized water sealed anodized aluminum; Hyzod(tm) polycarbonate used to temporarily protect ISS windows; Russian quartz window material; Beta Cloth with Teflon(tm) reformulated without perfluorooctanoic acid (PFOA), and electroless nickel. Discussion for current and future MISSE materials experiments will be presented. MISSE 7 samples are: more deionized water sealed anodized aluminum, including Photofoil(tm); indium tin oxide (ITO) over-coated Kapton(tm) used as thermo-optical surfaces; mechanically scribed tin-plated beryllium-copper samples for "tin pest" growth (alpha/beta transformation); and beta cloth backed with a black coating rather than aluminization. MISSE 8 samples are: exposed "scrim cloth" (fiberglass weave) from the ISS solar array wing material, protective fiberglass tapes and sleeve materials, and optical witness samples to monitor contamination.

Finckenor, Miria↗

Environmental variables associated with vacationers' sun protection at warm weather resorts in North America

Background: Vacationing at sunny, warm weather locations is a risk factor for excessive solar ultraviolet (UV) radiation exposure and skin cancer. Objectives: This study examined the association of environmental variables related to UV levels with vacationers' sun protection. Methods: Vacationers at 41 summer resorts in 17 states and 1 Canadian Province were interviewed (n=3531) and observed (N=4347) during 2012 and 2013. Clothing coverage, sunglasses, and shade use were observed. Use of sunscreen and sunburns were self-reported. Environmental information was recorded by research staff or acquired from ground stations and the weather service. Results: Temperature was positively associated with sun protection behaviors; however clothing coverage was negatively associated with temperature. Cloud cover was negatively associated with sun protection, with the exception of clothing coverage which was positively associated with it. Elevation showed a mixed pattern of associations with vacationer's sun protection. Latitude of a resort was negatively associated with most sun protection behaviors, such that sun protection increased at more southerly resorts. Similarly, the farther south a vacationer traveled to the resort, the less sun protection they employed. The UV index showed a weak, positive relationship with some sun protection behaviors even when controlling for temperature. Conclusions: Vacationers appeared aware that UV is higher at southern latitudes and may learn UV is intense when living in southern regions. However, many used temperature, an unreliable cue, to judge UV intensity and seemed to adjust clothing for warmth not UV protection. Efforts are needed to help individuals make more accurate sun safety decisions. - Highlights: • Vacationers poorly monitor and protect against environmental ultraviolet radiation (UVR). • On cloudy days vacationers fail to protect against UVR. • Temperature is erroneously used by vacationers as a marker for UVR. • Clothing is used primarily by vacationers for warmth, not UVR protection. • The farther south a vacationer travels, the more likely they are to sunburn.

79 ASTRONOMY AND ASTROPHYSICS↗

Aerosol Filtration Efficiency of Common Fabrics Used in Respiratory Cloth Masks

The emergence of a pandemic affecting the respiratory system can result in a significant demand for face masks. This includes the use of cloth masks by large sections of the public, as can be seen during the current global spread of COVID-19. However, there is limited knowledge available on the performance of various commonly available fabrics used in cloth masks. Importantly, there is a need to evaluate filtration efficiencies as a function of aerosol particulate sizes in the 10 nm – 10 µm range, which is particularly relevant for respiratory virus transmission. We have carried out these studies for several common fabrics including cotton, silk, chiffon, flannel, various synthetics, and their combinations. While the filtration efficiencies for various fabrics when a single layer was used ranged from 5-80% and 15-95% for particle sizes <300 nm and >300 nm respectively, the efficiencies improved when multiple layers were used, and when using a specific combination of different fabrics. Filtration efficiencies of the hybrids (such as cotton-silk, cotton-chiffon, cotton-flannel) was >80 % (for particles <300 nm) and >90 % (for particles >300 nm). We speculate that the enhanced performance of the hybrids is likely due to the combined effect of mechanical and electrostatic-based filtration. Cotton, the most widely used material for cloth masks performs better at higher weave densities (i.e., threads per inch) and can make a significant difference in filtration efficiencies. Our studies also imply that gaps (as caused by an improper fit of the mask) can result in over a 60% decrease in the filtration efficiency, implying the need for future cloth mask design studies to take into account issues of “fit” and leakage, while allowing the exhaled air to vent efficiently. Overall, we find that combinations of various commonly available fabrics used in cloth masks can potentially provide significant protection against the transmission of aerosol particles.

36 MATERIALS SCIENCE↗

Structures and Mechanisms Design Concepts for Adaptive Deployable Entry Placement Technology

System studies have shown that large deployable aerodynamic decelerators such as the Adaptive Deployable Entry and Placement Technology (ADEPT) concept can revolutionize future robotic and human exploration missions involving atmospheric entry, descent and landing by significantly reducing the maximum heating rate, total heat load, and deceleration loads experienced by the spacecraft during entry [1-3]. ADEPT and the Hypersonic Inflatable Aerodynamic Decelerator (HIAD) [4] share the approach of stowing the entry system in the shroud of the launch vehicle and deploying it to a much larger diameter prior to entry. The ADEPT concept provides a low ballistic coefficient for planetary entry by employing an umbrella-like deployable structure consisting of ribs, struts and a fabric cover that form an aerodynamic decelerator capable of undergoing hypersonic flight. The ADEPT "skin" is a 3-D woven carbon cloth that serves as a thermal protection system (TPS) and as a structural surface that transfers aerodynamic forces to the underlying ribs [5]. This paper focuses on design activities associated with integrating ADEPT components (cloth, ribs, struts and mechanisms) into a system that can function across all configurations and environments of a typical mission concept: stowed during launch, in-space deployment, entry, descent, parachute deployment and separation from the landing payload. The baseline structures and mechanisms were selected via trade studies conducted during the summer and fall of 2012. They are now being incorporated into the design of a ground test article (GTA) that will be fabricated in 2013. It will be used to evaluate retention of the stowed configuration in a launch environment, mechanism operation for release, deployment and locking, and static strength of the deployed decelerator. Of particular interest are the carbon cloth interfaces, underlying hot structure, (Advanced Carbon- Carbon ribs) and other structural components (nose cap, struts, and main body) designed to withstand the pressure and extremely high heating experienced during planetary entry.

Yount, Bryan C.↗

Thermal stress in aviation.

Personnel comfort and protection from thermal stress, discussing clothing, environmental temperature, metabolic heat production, solar radiation, etc

VENTILATION↗

Thermal Analysis of an In-Space Heat Shield Exposed to a Rocket Plume During Stage Separation

Thermal analyses were conducted to evaluate the thermal response of various individual materials and multi-layer configurations for an in-space heat shield exposed to a rocket plume during stage separation. Frequently used, readily available thermal protection materials consisting of cork, carbon cloth phenolic (CCP), and silica cloth phenolic (SCP) were selected for an initial screening analysis. SCP was chosen as the primary material for further evaluation using an updated thermal environment calculated using computational fluid dynamics (CFD) results. A multi-layer configuration consisting of SCP providing erosion resistance and a Nomex honeycomb providing thermal protection was then evaluated as a solution for more mass-efficient performance. Pyrolysis depth, bondline temperature, back-side temperature, and a thermal factor of safety were used to define the necessary material thickness profile. Adhesives were included in the analyses with considerations for maximum temperature and application method. One dimensional thermal analyses at several stations along the heat shield surface were performed for the initial screening and follow-on analyses. The methodology used standard processes and computer programs applicable to solid rocket motor internal insulation and nozzle thermal analysis such as Chemical Equilibrium and Applications (CEA), Aerotherm Chemical Equilibrium (ACE), Momentum/Energy Integral Technique (MEIT), and Insulation Thermal Response and Ablation Code (ITRAC). The baseline SCP/Nomex honeycomb multi-layer configuration thermal performance predictions satisfied the objectives with an acceptable mass estimate for the design maturity. The EA9673 film adhesive and SCP resin were the best performing bonding agents considered for the SCP/Nomex honeycomb and Nomex honeycomb/structural substrate interfaces. The baseline mass estimate was lowest when the resin was the bonding agent due to the higher maximum service temperature. These thermal analyses evaluated typical internal and external nozzle materials using a calculated thermal environment and heat loads that were lower than a typical rocket motor internal environment but greater than standard external aeroheating.

Andrew T Hiatt↗

In-flight environmental effects on airplane composite vertical fin caps

The NASA-Langley Storm Hazards Program has given attention to the effects of severe in-flight weather environments on composite structures, using an instrumented F-106B in storm penetration experiments. The vertical fin cap was chosen for the study of lightning strike attachments on composite structures of four different types: (1) glass/epoxy with flame-sprayed aluminum; (2) Kevlar/epoxy with aluminized glass cloth; (3) graphite-epoxy without lightning protection; and (4) unprotected graphite-epoxy with electrical isolation from the rest of the aircraft structure. Flight test results are evaluated.

Howell, William E.↗

MISSE 6, 7 and 8 Materials Sample Experiments from the International Space Station Materials and Processes Team

The International Space Station Materials and Processes (ISS M&P) team has multiple material samples on MISSE 6, 7 and 8 to observe Low Earth Orbit (LEO) environmental effects on Space Station materials. Optical properties, thickness/mass loss, surface elemental analysis, visual and microscopic analysis for surface change are some of the techniques employed in this investigation. The ISS M&P team has participated in previous MISSE activities in order to better characterize the LEO effects on Space Station materials. This investigation will further this effort. Results for the following MISSE 6 samples materials will be presented: a comparison of anodize and chemical conversion coatings on various aluminum alloys, electroless nickel; AZ93 white ceramic thermal control coating with and without Teflon; Hyzod(TM) polycarbonate used to temporarily protect ISS windows; Russian quartz window material; reformulated Teflon (TM) coated Beta Cloth (Teflon TM without perfluorooctanoic acid (PFOA)) and a Dutch version of beta cloth. Discussion for current and future MISSE materials experiments will be presented. MISSE 7 samples are: deionized water sealed anodized aluminum Photofoil(TM); indium tin oxide (ITO)- coated Kapton(TM) used as thermo-optical surfaces; mechanically scribed tin-plated beryllium-copper samples for "tin pest" growth ( alpha/Beta transformation); Crew Exploration Vehicle (CEV) parachute soft goods. MISSE 8 sample: exposed "scrim cloth" (fiberglass weave) from the ISS solar array wing material, Davlyn fiberglass sleeve material, Permacel and Intertape protective tapes, and ITO-coated Kapton.

Kravchenko, Michael↗

Development of an improved protective cover/light block for multilayer insulation

The feasibility of using a scrim-reinforced, single metallized, 4-mil Tedlar film as a replacement for the Teflon coated Beta-cloth/single metallized 3-mil Kapton film presently used as the protective cover/light block for multilayer insulation (MLI) on the Orbiter, Spacelab, and other space applications was demonstrated. The proposed Tedlar concept is lighter and potentially lower in cost. Thermal analysis with the proper concept was much simpler than with the present system. Tests have already demonstrated that white Tedlar has low alpha (adsorption) degradation in space from U.V. The proposed concept was 4400 percent cheaper with nominal weight savings of 50 percent.

Thompson, L. M.↗

SRB thermal curtain design support

The objective of the program during this time period was to evaluate candidate materials that could be used to design an improved Solid Rocket Motor (SRM) Aft Skirt Thermal Curtain (ASTC). The ASTC is a flexible, high temperature, cloth and insulation composite that is used to protect the hardware located inside the aft skirt of the shuttle solid rocket booster. The current ASTC consists of nine layers of insulating materials and is 2.58 inches thick. The ASTC is made up of twenty four segments. The segments are hand sewn together during installation on the aft skirt. The weight of the current ASTC is approximated at about six hundred pounds. This weight does not include the weight of the mounting hardware and ties required to install the twenty four ASTC segments (which is significant). The current effort entailed measuring the thermophysical properties of six candidate materials (quartz, S glass, and Kevlar woven into nominal 0.25 inch thick layers by angle interlock and polar-weave) and then using these properties in a computer program to predict the thermal performance of various curtain configurations subjected to an SRM heat flux.

Dixon, Carl A.↗

In Situ MOF Pyrolysis Construction of Hierarchical Porous Co‐Nanoparticles/Carbon Cloth Composites for Enhanced Electromagnetic Wave Shielding and Absorption

The development of high-performance electromagnetic protection materials integrating broadband absorption and effective shielding capabilities is hindered by challenges in simultaneously optimizing multiple electromagnetic properties through conventional material designs. This study pioneers a hierarchical porous Co nanoparticle/carbon cloth (Co/CC) composite via controlled annealing of a Co-MOF precursor on carbon cloth. The Co-MOF served a dual role as both magnetic source and pore-forming agent, enabling in situ generation of uniformly dispersed Co nanoparticles and creation of abundant pores/interfaces on the CC fibers during pyrolysis. This unique architecture synergistically enhanced dielectric loss (via interfacial/dipolar polarization) and magnetic loss (via natural resonance, exchange interactions, and eddy currents), significantly improving impedance matching. The hierarchical pores further functioned as integrated “absorption–reflection” units for efficient electromagnetic energy attenuation. Consequently, the Co/CC composite annealed at 800°C (Co/CC-800) achieves minimum reflection loss (−40.69 dB) and 120% effective absorption bandwidth extension (6.16 GHz) as a filler, and exhibits superior electromagnetic interference shielding effectiveness (46.66 dB) as an integrated component. Significantly, Co/CC-800 demonstrated robust photothermal and electrothermal conversion capabilities, ensuring operational stability in ice-covered and humid harsh environments. This work pioneers a pore-structure-mediated strategy to harmonize dielectric–magnetic synergy, providing a new paradigm for designing advanced multifunctional electromagnetic protection materials.

dielectric‐magnetic synergy↗

Household Materials Selection for Homemade Cloth Face Coverings and Their Filtration Efficiency Enhancement with Triboelectric Charging

The COVID-19 pandemic is currently causing a severe disruption and shortage in the global supply chain of necessary personal protective equipment (e.g., N95 respirators). The U.S. CDC has recommended use of household cloth by the general public to make cloth face coverings as a method of source control. We evaluated the filtration properties of natural and synthetic materials using a modified procedure for N95 respirator approval. Common fabrics of cotton, polyester, nylon, and silk had filtration efficiency of 5–25%, polypropylene spunbond had filtration efficiency 6–10%, and paper-based products had filtration efficiency of 10–20%. An advantage of polypropylene spunbond is that it can be simply triboelectrically charged to enhance the filtration efficiency (from 6 to >10%) without any increase in pressure (stable overnight and in humid environments). Using the filtration quality factor, fabric microstructure, and charging ability, we are able to provide an assessment of suggested fabric materials for homemade facial coverings.

36 MATERIALS SCIENCE↗

Observations Regarding Commonly Available Materials for Face Shield Emulated-Personal Protective Equipment

The Center for Disease Control has recommended that to reduce potential exposure to COVID-19 the public should wear cloth face coverings in public settings where other social distancing measures are difficult to maintain. These face coverings and other Emulated-Personal Protective Equipment (E-PPE) can be made by using Commonly Available Materials (CAMs). As E-PPE recommendations continue to flood the media, a Sandia COVID-19 LDRD effort, the Sandia E-PiPEline Team, systematically evaluated E-PPE design options considering their effectiveness, durability, build difficulty, build cost, and comfort. Using qualitative and semi-quantitative evaluation tools, results of the investigation are presented here to provide guidelines for home and office construction of E-PPE.

36 MATERIALS SCIENCE↗

Observations Regarding Commonly Available Materials for Face Covering Emulated-Personal Protective Equipment

The Center for Disease Control has recommended that to reduce potential exposure to COVID-19 the public should wear cloth face coverings in public settings where other social distancing measures are difficult to maintain. These face coverings and other Emulated-Personal Protective Equipment (E-PPE) can be made by using Commonly Available Materials (CAMs). As E-PPE recommendations continue to flood the media, a Sandia COVID-19 LDRD effort, the Sandia E-PiPEline Team, systematically evaluated E-PPE design options considering their effectiveness, durability, build difficulty, build cost, and comfort. Using qualitative and semi-quantitative evaluation tools, results of the investigation are presented here to provide guidelines for home and office construction of E-PPE.

36 MATERIALS SCIENCE↗

Evaluation of an Additively Manufactured Respirator for Personnel Protection from Particulates

Additively manufactured respirators (AMRs) made using rigid plastic can be fitted with repurposed filter media to yield a wearable mask capable of passing a quantitative fit test with criteria set for commercial, N95 health care particulate respirators. This has been verified through an evaluation study assessing AMR masks fabricated using open-source design files and a commercial fused-filament fabrication machine, using N95 filter cloth and a P100 respirator cartridge. A few examples of filter media not designed for human respiratory protection were also evaluated in an AMR mask but did not demonstrate filtering sufficient to pass the N95 test criteria. All attributes of an AMR mask system must be considered during design and when testing performance, including the mask frame, gasket, and the cord used to secure the mask to the face. AMR masks are not the same as commercially available respiratory masks. If AMR masks are used as personal protective equipment (PPE) during a crisis when there is a shortage of regular PPE it is important that wearers are fully informed of the differences, tradeoffs, and risks associated with their use. Quantitative fit testing and proper training on how to don and doff the AMR mask are important to help achieve the best possible outcome when they are used.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Flame Retardant Fibers for Human Space Exploration - Past, Present, and Future

The National Aeronautics and Space Administration (NASA) has led in the development of unique flame retardant fibers for human spaceflight since the beginning of the Apollo program. After the Apollo 1 fire which killed Command Pilot Virgil I 'Gus' Grissom, Senior Pilot Edward H. White II, and Pilot Roger B. Chaffee from cardiac arrest on January 27, 1967, the accident investigators found severe third degree burns and melted spacesuits on the astronauts bodies. NASA immediately initiated an extensive research program aimed at developing flame retardant and flame resistant fibers for the enriched oxygen atmosphere of the Apollo crew cabin. Fibers are flame retardant when they have been modified by chemical and thermal treatments. Fibers are flame resistant when they are made of inherently flame resistant materials (i.e. glass, ceramic, highly aromatic polymers). Immediately after this tragic accident, NASA funded extensive research in specifically developing flame retardant fibers and fabrics. The early developmental efforts for human spaceflight were for the outer layer of the Apollo spacesuit. It was imperative that non-flammable fabrics be used in a 100% oxygen environment. Owens-Corning thus developed the Beta fiber that was immediately used in the Apollo program and later in the Space Shuttle program. Aside from the urgent need for protective fabrics for the spacesuit, NASA also needed flame retardant fabrics for both clothing and equipment inside the spacecraft. From the mid-1960s to the early 1980's, NASA contracted with many companies to develop inherently flame retardant fibers and flame retardant finishes for existing fibers. Fluorocarbons and aromatic polyamides were the polymers of great interest for the development of new inherently flame retardant fibers for enriched oxygen environments. These enriched environments varied for different space programs. For example, the Apollo program requirements were for materials that would not support combustion in a 70%/30% oxygen/nitrogen environment at 6.3 pounds per square inch (psi). The Skylab program flammability requirements were set at 80%/20% oxygen/nitrogen ratios at 5 psi. While many fibers produced under several NASA contracts were never used, a few have become commercial products. The intent of this paper is to present the developmental history of some of these new or modified textile fibers. These developmental efforts are presented at various levels of details depending on the source of the historical records.

Orndoff, Evelyne↗