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Electro-optical system measures reflectance, reflectance ratio, transmission, absorption, refractive index, and absorption coefficient in both visible and infrared (IR) spectral regions. System effectively combining capabilities of ellisometer, reflectometer, and spectrophotometer is expected to find application in environmental and material composition testing fields.
Method of measuring total reflectance employs relatively inexpensive reflectometer with gold-coated hemispherical reflector. Light sources may be tungsten lamp for visable region, or Globar lamp for infrared.
The behavior in space environment of evaporated Al uncoated and coated with reactively deposited silicon oxide (SiOx), electron beam evaporated SiO2 and Al2O3, and Al and Ag coated with double layers of Al2O3 + SiOx is compared with metallized Teflon and Kapton, anodized Al (Alzak), and white paints. Flight data from three calorimetric experiments and one reflectometer flown in different orbital environments are compared with laboratory test data. The results demonstrate that evaporated thin films are extremely versatile and stable coatings for space applications. Through the use of control samples studied in different laboratory tests and monitored for up to 12,000 hours of solar exposure in different orbits, a classification of orbital severity and an estimate of laboratory simulation accuracy is obtained.
The spectral emittance of a NASA developed zirconia ceramic thermal barrier coating system, consisting of a metal substrate, a layer of Ni-Cr-Al-Y bond material and a layer of yttria-stabilized zirconia ceramic material, is analyzed. The emittance, needed for evaluation of radiant heat loads on cooled coated gas turbine components, was measured over a range of temperatures that would be typical of its use on such components. Emittance data were obtained with a spectrometer, a reflectometer and a radiation pyrometer at a single bond coating thickness of 0.010 cm and at a ceramic coating thickness of 0-0.076 cm. The data were transformed into the hemispherical total emittance and were correlated to the ceramic coating thickness and temperature using multiple-regression curve-fitting techniques. The system was found to be highly reflective, and, consequently, capable of significantly reducing radiation heat loads on cooled gas turbine engine components.
Detector, intended for use with longwall shearer, determines when cut has pierced through coal layer. Accelerometer measures hardness of material struck by penetrometer ram, while reflectometers measure reflectivity of surface on either side of penetrometer. Signals are combined in voting circuit that indicates "coal" or "shale", depending on information supplied by three sensors. It distinguishes by differences in accelerometer waveforms.
A nonspecular reflectometer and its operation at far-infrared wavelengths are described. Large differences in nonspecular reflectance were found to exist between different optically black coatings. Normal incidence bidirectional reflectance distribution function /BRDF) measurements at wavelengths between 12 and 316 microns of three black coatings show that their mean BRDFs increase with wavelength. The specularity of two of these coatings also showed a strong wavelength dependence, while the specularity of one coating seemed independent of wavelength. The BRDF of one coating depended on the angle of incidence at 12 and 38 microns, but not at 316 microns. Beyond 200 microns, it was found necessary to correct the measurements for the beam spread of the instrument.
The use of a time domain reflectometer (TDR) for planetary exploration is considered. Determination of the apparent dielectric constant and hence, the volumetric water content of frozen and unfrozen soils using the TDR is described. Earth-based tests were performed on a New York state sandy soil and a Wyoming Bentonite. Use of both a cylindrical coaxial transmission line and a parallel transmission line as probes was evaluated. The water content of the soils was varied and the apparent dielectric constant measured in both frozen and unfrozen states. Advantages and disadvantages of the technique are discussed.
A Barnes field spectral reflectometer which collected information in 373 channels covering the region from 0.4 to 2.5 micrometers was assessed for signal utility. A band was judged unsatisfactory if the probability was 0.1 or greater than its signal to noise ratio was less than eight to one. For each of the bands the probability of a noisy observation was estimated under a binomial assumption from a set of field crop spectra covering an entire growing season. A 95% confidence interval was calculated about each estimate and bands whose lower confidence limits were greater than 0.1 were judged unacceptable. As a result, 283 channels were deemed statistically satisfactory. Excluded channels correspond to portions of the electromagnetic spectrum (EMS) where high atmospheric absorption and filter wheel overlap occur. In addition, the analyses uncovered intervals of unsatisfactory detection capability within the blue, red and far infrared regions of vegetation spectra. From the results of the analysis it was recommended that 90 channels monitored by the instrument under consideration be eliminated from future studies. These channels are tabulated and discussed.
Two experiments were performed employing swept frequency microwaves for the purpose of investigating the reflectivity from soil volumes containing both discontinuous and continuous changes in subsurface soil moisture content. Discontinuous moisture profiles were artificially created in the laboratory while continuous moisture profiles were induced into the soil of test plots by the environment of an agricultural field. The reflectivity for both the laboratory and field experiments was measured using bi-static reflectometers operated over the frequency ranges of 1.0 to 2.0 GHz and 4.0 to 8.0 GHz. Reflectivity models that considered the discontinuous and continuous moisture profiles within the soil volume were developed and compared with the results of the experiments. This comparison shows good agreement between the smooth surface models and the measurements. In particular the comparison of the smooth surface multi-layer model for continuous moisture profiles and the yield experiment measurements points out the sensitivity of the specular component of the scattered electromagnetic energy to the movement of moisture in the soil.
The basic approach to this experiment is to expose a wide variety of material surfaces to the atomic flux in orbit. The experiment is passive and depends on preflight and postflight measurements of the test surfaces in the laboratory. The experiment will also include a reflectometer device to measure atomic beam reflection angles and thus momentum accommodations, and a unique passive spacecraft attitude sensor. Samples consisting of solid disks or thin film coatings on substrate disks will be mounted in a panel. The face of this panel will be flown on Long Duration Exposure Facility normal to the incident stream of oxygen atoms. Each disk will have part of its front surface masked so exposure to the atomic-oxygen reaction will be limited to selected areas, the shadowed areas being used as control surfaces in the measurements. A typical sample is an optically flat quartz disk overcoated with a film of the material of interest. These include Ag, Au, Pt, Nb, Ni, Al, C, Si, Ge, LiF, and a few engineering materials. Some materials for which the expected removal rate is high, such as carbon, will be solid disks rather than thin films.
The Poker Flat 49.92-MHz MST radar uses 64 phase-controlled transmitters in individual shelters distributed throughout the antenna array. Phase control is accomplished by sampling the transmitted pulse at the directional coupler of each transmitter and sending the sample pulse back to a phase-control unit. This method requires phase matching 64 long (256 meter) coaxial cables (RG-213) to within several electrical degrees. Tests with a time domain reflectometer showed that attenuation of high frequency components in the long RG-213 cable rounded the leading edge of the reflected pulse so that the cables could only be measured to within 50 cm (about 45 deg at 49.92 MHz). Another measurement technique using a vector voltmeter to compare forward and reflected phase required a directional coupler with unattainable directivity. Several other techniques were also found lacking, primarily because of loss in the long RG-213 cables. At this point it was realized that what was needed was a simple version of the phase-coherent clear-air radar, i.e., a cable radar. The design and operation of this cable are described.
Reflectance measurements were made of several metals illuminated from various angles with light at 14 wavelengths in the interval 46.5-283 A. The metals, Rh, Os, Pt and Au were deposited as 125 A films on a binding substrate through electron beam epitaxy. Measurements were made with a grazing incidence monochromator and a reflectometer. The data generally showed lowered reflectance with increasing angles of illumination and shorter wavelengths. The reflectance peak, however, was located at wavelengths of 100-160 A, particularly at large grazing incidences. The wavelengths correspond with the 5p to epsilon-d transition in all of the elements. Rh displayed the highest overall reflectance, and both Rh and Os were more efficient than Au or Pt.
The inflight repair of the Solar Maximum Spacecraft provided the first opportunity to make actual measurements of thermal control surfaces after 4 years exposure in low Earth orbit. Defective hardware was replaced by astronauts and returned to Earth while protected from reentry damage in the Shuttle Payload bay. A preliminary thermal surface assessment was made soon after retrieval in support of Space Telescope and other current spacecraft programs. This included visual examination and measurement of Kapton and Teflon film to determine change in thermal radiative properties after 4 years exposure to solar radiation and reaction with atomic oxygen. Comparative measurements were made with a portable solar reflectometer used for inspection of spacecraft hardware. Post flight measurements and observations reveal significant surface changes that further confirm Kapton mass loss predictions made prior to Solar Maximum repair. Details of thermal surface application, measurements and experimental results are presented and discussed.
An experimental method has been developed to determine the droplet impingement characteristics on two- and three-dimensional bodies. The experimental results provide the essential droplet impingement data required to validate particle trajectory codes, used in aircraft icing analyses and engine inlet particle separator analyses. A body whose water droplet impingement characteristics are required is covered at strategic locations by thin strips of moisture absorbing (blotter) paper, and then exposed to an air stream containing a dyed-water spray cloud. Water droplet impingement data are extracted from the dyed blotter strips, by measuring the optical reflectance of the dye deposit on the strips, using an automated reflectometer. Impingement efficiency data obtained for a NACA 65(2)015 airfoil section, a supercritical airfoil section, and Being 737-300 and axisymmetric inlet models are presented in this paper.
The theory of hard target calibration of lidar backscatter data, including laboratory measurements of the pertinent target reflectance parameters, is extended to include the effects of polarization of the transmitted and received laser radiation. The bidirectional reflectance-distribution function model of reflectance is expanded to a 4 x 4 matrix allowing Mueller matrix and Stokes vector calculus to be employed. Target reflectance parameters for calibration of lidar backscatter data are derived for various lidar system polarization configurations from integrating sphere and monostatic reflectometer measurements. It is found that correct modeling of polarization effects is mandatory for accurate calibration of hard target reflectance parameters and, therefore, for accurate calibration of lidar backscatter data.
Monolithic diode grids have been fabricated on 2-cm square gallium-arsenide wafers with 1600 Schottky-barrier varactor diodes. Shorted diodes are detected with a liquid-crystal technique, and the bad diodes are removed with an ultrasonic probe. A small-aperture reflectometer that uses wavefront division interference was developed to measure the reflection coefficient of the grids. A phase shift of 70 deg with a 7-dB loss was obtained at 93 GHz when the bias on the diode grid was changed from -3 V to 1 V. A simple transmission-line grid model, together with the measured low-frequency parameters for the diodes, was shown to predict the measured performance over the entire capacitive bias range of the diodes, as well as over the complete reactive tuning range provided by a reflector behind the grid, and over a wide range of frequencies from 33 GHz to 141 GHz. This shows that the transmission-line model and the measured low-frequency diode parameters can be used to design an electronic beam-steering array and to predict its performance. An electronic beam-steering array made of a pair of grids using state-of-the-art diodes with 5-ohm series resistances would have a loss of 1.4 dB at 90 GHz.
Results are reported from measurements of the specular reflectances (SRs) and bidirectional reflectance distribution functions (BRDFs) of three black optical coatings in the FIR wavelength range. The nonspecular reflectometer apparatus described by Smith (1984) is employed, and the data are presented in tables and graphs and discussed in detail. It is found that Ames 24E has an FIR SR one order of magnitude lower than that of Martin black (MB), with BRDF values characteristic of a nearly Lambertian surface, while Infrablack has SR two orders lower than MB and a specular-diffuse surface; MB itself has a very specular surface.
A calorimetric vacuum emissometer (CVE) capable of measuring total hemispherical emittance of surfaces at elevated temperatures was designed, built, and tested. Several materials with a wide range of emittances were measured in the CVE between 773 to 923 K. These results were compared to values calculated from spectral emittance curves measured in a room temperature Hohlraum reflectometer and in an open-air elevated temperature emissometer. The results differed by as much as 0.2 for some materials but were in closer agreement for the more highly-emitting, diffuse-reflecting samples. The differences were attributed to temperature, atmospheric, and directional effects, and errors in the Hohlraum and emissometer measurements (plus or minus 5 percent). The probable error of the CVE measurements was typically less than 1 percent.