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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 127 records · Page 7

Radiographic and ultrasonic characterization of sintered silicon carbide

The capabilities were investigated of projection microfocus X-radiography, ultrasonic velocity and attenuation, and reflection scanning acoustic microscopy for characterizing silicon carbide specimens. Silicon carbide batches covered a range of densities and different microstructural characteristics. Room temperature, four point flexural strength tests were conducted. Fractography was used to identify types, sizes, and locations of fracture origins. Fracture toughness values were calculated from fracture strength and flaw characterization data. Detection capabilities of radiography and acoustic microscopy for fracture-causing flaws were evaluated. Applicability of ultrasonics for verifying material strength and toughness was examined.

Baaklini, G. Y.↗

Reliability analysis applied to structural tests

The application of reliability theory to predict, from structural fatigue test data, the risk of failure of a structure under service conditions because its load-carrying capability is progressively reduced by the extension of a fatigue crack, is considered. The procedure is applicable to both safe-life and fail-safe structures and, for a prescribed safety level, it will enable an inspection procedure to be planned or, if inspection is not feasible, it will evaluate the life to replacement. The theory has been further developed to cope with the case of structures with initial cracks, such as can occur in modern high-strength materials which are susceptible to the formation of small flaws during the production process. The method has been applied to a structure of high-strength steel and the results are compared with those obtained by the current life estimation procedures. This has shown that the conventional methods can be unconservative in certain cases, depending on the characteristics of the structure and the design operating conditions. The suitability of the probabilistic approach to the interpretation of the results from full-scale fatigue testing of aircraft structures is discussed and the assumptions involved are examined.

Diamond, P.↗

Advanced Gas Turbine (AGT) Technology Project

Engine testing, ceramic component fabrication and evaluation, component performance rig testing, and analytical studies comprised AGT 100 activities during the 1985 year. Ten experimental assemblies (builds) were evaluated using two engines. Accrued operating time was 120 hr of burning and 170 hr total, bringing cumulative total operating time to 395 hr, all devoid of major failures. Tests identified the generator seals as the primary working fluid leakage sources. Power transfer clutch operation was demonstrated. An alpha SiC gasifier rotor engine test resulted in blade tip failures. Recurring case vibration and shaft whip have limited gasifier shaft speeds to 84%. Ceramic components successfully engine tested now include the SiC scroll assembly, Si3N3 turbine rotor, combustor assembly, regenerator disk bulkhead, turbine vanes, piston rings, and couplings. A compressor shroud design change to reduce heat recirculation back to the inlet was executed. Ceramic components activity continues to focus on the development of state-of-the-art material strength characteristics in full-scale engine hardware. Fiber reinforced glass-ceramic composite turbine (inner) backplates were fabricated by Corning Glass Works. The BMAS/III material performed well in engine testing. Backplates of MAS material have not been engine tested.

Source record↗

Materials Assessment of Components of the Extravehicular Mobility Unit

Current research interests for Extravehicular Mobility Unit (EMU) design and development are directed toward enhancements of the Shuttle EMU, implementation of the Mark 3 technology for Shuttle applications, and development of a next generation suit (the X suit) which has applications for prolonged space flight, longer extravehicular activity (EVA), and Moon and Mars missions. In this research project two principal components of the EMU were studied from the vantage point of the materials and their design criteria. An investigation of the flexible materials which make up the lay-up of materials for abrasion and tear protection, thermal insulation, pressure restrain, etc. was initiated. A central focus was on the thermal insulation. A vacuum apparatus for measuring the flexibility of the materials was built to access their durability in vacuum. Plans are to include a Residual Gas Analyzer on the vacuum chamber to measure volatiles during the durability testing. These tests will more accurately simulate space conditions and provide information which has not been available on the materials currently used on the EMU. Durability testing of the aluminized mylar with a nylon scrim showed that the material strength varied in the machine and transverse directions. Study of components of the EMU also included a study of the EMU Bearing Assemblies as to materials selection, engineered materials, use of coatings and flammability issues. A comprehensive analysis of the performance of the current design, which is a stainless steel assembly, was conducted and use of titanium alloys or engineered alloy systems and coatings was investigated. The friction and wear properties are of interest as are the general manufacturing costs. Recognizing that the bearing assembly is subject to an oxygen environment, all currently used materials as well as titanium and engineered alloys were evaluated as to their flammability. An aim of the project is to provide weight reduction since bearing weights constitute 1/3 of the total EMU weight. Our investigations have shown favorable properties using a titanium or nickel base alloy in conjunction with a coating system. Interest lies in developing titanium as a more nonflammable material. Methodology for doing this lies in adding coatings and surface alloying the titanium. This report is brief and does not give all necessary details. The reader should contact the authors as to the detailed study and for viewing of raw data.

Olivas, John D.↗

Pressure vessel with improved impact resistance and method of making the same

A composite overwrapped pressure vessel is provided which includes a composite overwrapping material including fibers disposed in a resin matrix. At least first and second kinds of fibers are used. These fibers typically have characteristics of high strength and high toughness to provide impact resistance with increased pressure handling capability and low weight. The fibers are applied to form a pressure vessel using wrapping or winding techniques with winding angles varied for specific performance characteristics. The fibers of different kinds are dispersed in a single layer of winding or wound in distinct separate layers. Layers of fabric comprised of such fibers are interspersed between windings for added strength or impact resistance. The weight percentages of the high toughness and high strength materials are varied to provide specified impact resistance characteristics. The resin matrix is formed with prepregnated fibers or through wet winding. The vessels are formed with or without liners.

DeLay, Thomas K.↗

Concepts and techniques for ultrasonic evaluation of material mechanical properties

Ultrasonic methods that can be used for material strength are reviewed. Emergency technology involving advanced ultrasonic techniques and associated measurements is described. It is shown that ultrasonic NDE is particularly useful in this area because it involves mechanical elastic waves that are strongly modulated by morphological factors that govern mechanical strength and also dynamic failure modes. These aspects of ultrasonic NDE are described in conjunction with advanced approaches and theoretical concepts for signal acquisition and analysis for materials characterization. It is emphasized that the technology is in its infancy and that much effort is still required before the techniques and concepts can be transferred from laboratory to field conditions.

Vary, A.↗

Performance analysis of advanced spacecraft TPS

For the Space Shuttle several types of ceramic heat shield materials were developed, both flexible and rigid. Improvements on the materials are continuously evolving. Material properties that have been studied and improved are high temperature limits, material strength, surface ruggedness, and surface catalycity. The results are presented of preliminary analyses concerning the thermal protection systems of future spacecraft and their sensitivity to the above material properties.

Pitts, William C.↗

Preliminary design of composite wings for buckling, strength and displacement constraints

An unstiffened panel buckling constraint for balanced, symmetric laminated composites is included on the global design level in a mathematical programming structural optimization procedure for designing wing structures. Constraints are introduced by penalty functions, and Newton's method based on approximate second derivatives of the penalty terms is used as the search algorithm to obtain minimum-mass designs. Constraint approximations used during the optimization process contribute to the computational efficiency of the procedure. A criterion is developed that identifies the appropriate conservative form of the constraint approximations that are used with the optimization procedure. Minimum-mass design results are obtained for a multispar high-aspect-ratio wing subjected to material strength, minimum-gage, displacement, panel buckling and twist constraints. The material systems considered for the examples are all graphite-epoxy, graphite-epoxy with boron-epoxy spar caps, and all aluminum. The composite material designs are shown to have an advantage over the aluminum designs since they can often satisfy additional constraints with only small mass increases.

Starnes, J. H., Jr.↗

Lifetime Predictions of a Titanium Silicate Glass with Machined Flaws

A dynamic fatigue study was performed on a Titanium Silicate glass to assess its susceptibility to delayed failure and to compare the results with those of a previous study. Fracture mechanics techniques were used to analyze the results for the purpose of making lifetime predictions. The material strength and lifetime was seen to increase due to the removal of residual stress through grinding and polishing. Influence on time-to-failure is addressed for the case with and without residual stress present. Titanium silicate glass otherwise known as ultra-low expansion (ULE)* glass is a candidate for use in applications requiring low thermal expansion characteristics such as telescope mirrors. The Hubble Space Telescope s primary mirror was manufactured from ULE glass. ULE contains 7.5% titanium dioxide which in combination with silica results in a homogenous glass with a linear expansion coefficient near zero. delayed failure . This previous study was based on a 230/270 grit surface. The grinding and polishing process reduces the surface flaw size and subsurface damage, and relieves residual stress by removing the material with successively smaller grinding media. This results in an increase in strength of the optic during the grinding and polishing sequence. Thus, a second study was undertaken using samples with a surface finish typically achieved for mirror elements, to observe the effects of surface finishing on the time-to-failure predictions. An allowable stress can be calculated for this material based upon modulus of rupture data; however, this does not take into account the problem of delayed failure, most likely due to stress corrosion, which can significantly shorten lifetime. Fortunately, a theory based on fracture mechanics has been developed enabling lifetime predictions to be made for brittle materials susceptible to delayed failure. Knowledge of the factors governing the rate of subcritical flaw growth in a given environment enables the development of relations between lifetime, applied stress and failure probability for the material under study. Dynamic fatigue is one method of obtaining the necessary information to develop these relationships. In this study, the dynamic fatigue method was used to construct a time-to-failure diagram for polished ULE glass.

Tucker, Dennis S.↗

Full-Field Strain Methods for Investigating Failure Mechanisms in Triaxial Braided Composites

Recent advancements in braiding technology have led to commercially viable manufacturing approaches for making large structures with complex shape out of triaxial braided composite materials. In some cases, the static load capability of structures made using these materials has been higher than expected based on material strength properties measured using standard coupon tests. A more detailed investigation of deformation and failure processes in large-unit-cell-size triaxial braid composites is needed to evaluate the applicability of standard test methods for these materials and to develop alternative testing approaches. This report presents some new techniques that have been developed to investigate local deformation and failure using digital image correlation techniques. The methods were used to measure both local and global strains during standard straight-sided coupon tensile tests on composite materials made with 12- and 24-k yarns and a 0 /+60 /-60 triaxial braid architecture. Local deformation and failure within fiber bundles was observed and correlations were made between these local failures and global composite deformation and strength.

Littell, Justin D.↗

Oxidation protected carbon-carbon

Pyrolized carbon-carbon has one unique advantage over other materials that makes its application to the space shuttle thermal protection system very attractive. This unique characteristic is the increase in material strength and modulus with increase in temperature up to about 2500 K (4040 F). Offsetting this unique advantage are disadvantages which include brittleness, high cost, and the tendency of the material to react with oxygen, particularly at high temperatures. The development of an oxidation inhibitor for the material and the definition of fabrication processes for selected full-scale components are considered.

Pavlosky, J. E.↗

Probabilistic material degradation under high temperature, fatigue, and creep

A methodology has been developed and embodied in two computer codes for quantitatively characterizing the material strength degradation of aerospace propulsion system structural components that are subjected to various random effects over the course of their service lives. The codes, PROMISS and PROMISC, constitute a material-resistance model that is used in the NESSUS aerospace structural-reliability program. NESSUS addresses the service life-reducing effects of high temperature, mechanical fatigue, and creep.

Boyce, L.↗

Creep and Environmental Durability of EBC/CMCs Under Imposed Thermal Gradient Conditions

Interest in SiC fiber-reinforced SiC ceramic matrix composite (CMC) environmental barrier coating (EBC) systems for use in high temperature structural applications has prompted the need for characterization of material strength and creep performance under complex aerospace turbine engine environments. Stress-rupture tests have been performed on SiC/SiC composites systems, with varying fiber types and coating schemes to demonstrate material behavior under isothermal conditions. Further testing was conducted under exposure to thermal stress gradients to determine the effect on creep resistance and material durability. In order to understand the associated damage mechanisms, emphasis is placed on experimental techniques as well as implementation of non-destructive evaluation; including electrical resistivity monitoring. The influence of environmental and loading conditions on life-limiting material properties is shown.

Appleby, Matthew↗

Cryogenic piping material selection for the Component Test Facility (CTF)

The anticipated high cost of the 8500 psi cryogenic and 15,000 psi gas piping systems used in the CTF at NASA's John C. Stennis Space Center led to the consideration of high-strength materials for these piping systems. Based on years of satisfactory service using austenitic stainless steels in cryogenic applications, particularly for hydrogen service, consideration was limited to the austenitic stainless steels. Attention was focused on alternatives to the 304/304L grades of stainless steel traditionally used in these applications. This paper discusses the various considerations that resulted in the decision to continue using 304/304L for the cryogenic piping and the selection of the nitrogen-strengthened 21Cr-6Ni-9Mn alloy (UNS S21903) for the high-pressure gas systems at the CTF.

St. Cyr, William W.↗

Areas of Seal R/D at GE

About four years ago, work was completed on a 36 inch diameter gas to gas carbon ring seal used to buffer low pressure turbine air at the rim of the forward outer flowpath on the GE36 unducted fan (UDF) engine. At about the same time, we were developing a long life counter-rotating intershaft air-oil seal of approximately 7.6 inch diameter for operation at 800 fps, 800 F, and 50 psid. Although we were successful in meeting most program goals with a split ring seal of the axial bushing type, the seal with the greatest payoff in life and air leakage rates, bearing many features in common with the GE36 seal, could not be successfully tested because of the structural weakness of the primary seal ring carbon material. This was a split ring seal using a hybrid combination of orifice compensated hydrostatic and shrouded hydrodynamic gas bearings. We are presently working to develop this design in conjunction with high strength materials being developed by Pure Carbon Co. In the area of engine secondary gas flow path-sealing for performance improvement, we are currently working with carbon and all metal face seals. A 15 inch diameter all metal 'aspirating' face seal, using self-acting hydrostatic bearings, was successfully tested to 700 fps, 100 psid, and 1000 F, demonstrating long life at flow reduction of 86 percent compared to a 'best' labyrinth. This seal will be developed through 1400 F, 900 fps, and 350 psid. The seal 'aspirates' closed at about idle speed pressure during engine start and reopens at engine shutdown. A hydraulic thrust balance seal, currently using orifice compensated hydrostatics, is under development. Other aspects of these projects are briefly covered.

Pope, A. Nelson↗

Mechanical property characterization and impact resistance of selected graphite/PEEK composite materials

To use graphite polyetheretherketone (PEEK) material on highly curved surfaces requires that the material be drapable and easily conformable to the surface. This paper presents the mechanical property characterization and impact resistance results for laminates made from two types of graphite/PEEK materials that will conform to a curved surface. These laminates were made from two different material forms. These forms are: (1) a fabric where each yarn is a co-mingled Celion G30-500 3K graphite fiber and PEEK thermoplastic fiber; and (2) an interleaved material of Celion G30-500 3K graphite fabric interleaved with PEEK thermoplastic film. The experimental results from the fabric laminates are compared with results for laminates made from AS4/PEEK unidirectional tape. The results indicate that the tension and compression moduli for quasi-isotropic and orthotropic laminates made from fabric materials are at least 79 percent of the modulus of equivalent laminates made from tape material. The strength of fabric material laminates is at least 80 percent of laminates made from tape material. The evaluation of fabric material for shear stiffness indicates that a tape material laminate could be replaced by a fabric material laminate and still maintain 89 percent of the shear stiffness of the tape material laminate. The notched quasi-isotropic compression panel failure strength is 42 to 46 percent of the unnotched quasi-isotropic laminate strength. Damage area after impact with 20 ft-lbs of impact energy is larger for the co-mingled panels than for the interleaved panels. The inerleaved panels have less damage than panels made from tape material. Residual compression strength of quasi-isotropic panels after impact of 20 ft-lbs of energy varies between 33 percent of the undamaged quasi-isotropic material strength for the tape material and 38 percent of the undamaged quasi-isotropic material strength for the co-mingled fabric material.

Baker, Donald J.↗

Multilayer Pressure Vessel Materials Testing and Analysis

To provide NASA a comprehensive suite of materials strength, fracture toughness and crack growth rate test results for use in remaining life calculations for aging multilayer pressure vessels, Southwest Research Institute (R) (SwRI) was contracted in two phases to obtain relevant material property data from a representative vessel. This report describes Phase 1 of this effort which includes a preliminary material property assessment as well as a fractographic, fracture mechanics and fatigue crack growth analyses of an induced flaw in the outer shell of a representative multilayer vessel that was subjected to cyclic pressure test. SwRI performed this Phase 1 effort under contract to the Digital Wave Corporation in support of their contract to Jacobs ATOM for the NASA Ames Research Center.

Cardinal, Joseph W.↗