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DOE OSTI2026

SuperLab 2.0 Showcase: Connecting Five Labs to Tackle Grid Complexity and Unlock Unique Grid Asset Potential

SuperLab 2.0 (5-Lab Demo) is a collaborative, national-scale experiment showcasing the coordination of geographically distributed energy assets in real time. The demonstration integrates 25 physical and digital assets, spanning wind, PV, batteries, electrolyzers, DC fast chargers, microgrid controllers, building automation systems, small modular reactor (SMR), control centers, and gas turbines, across five DOE national laboratories-NLR, INL, NETL, LBNL, and SNL. These assets are unified using Energy Sciences Network (ESnet), a low-latency, high-performance U.S. Department of Energy's (DOE) network, and controlled via a centralized energy controller hosted at NLR's ARIES facility. The demonstration validates the ability to stress-test hybrid energy systems under dynamic scenarios to de-risk advanced control strategies for greater resilience and flexibility. SuperLab 2.0 (5-Lab Demo) showcased a major advancement in federated national laboratory collaboration, enabling real-time, cross-laboratory experimentation to coordinate geographically dispersed distributed energy resources (DERs) using various communication protocols and networks. SuperLab 2.0 (5-Lab Demo) built on previous demonstrations conducted between NLR-PNNL and NLR-INL connecting diverse assets including distant protection devices, a SMR simulator, and a high temperature electrolyzer (HTE). Previous demos were based on a single connection between two labs with minimal coordination challenges. The 5-Lab demo with a centralized controller, distributed testbeds across different geographical locations, and use of protocols-based communication represents a scenario closer to real-world grid operations that coordinate resources across a region to meet system needs. This experiment studied how local DER controllers interact with a centralized energy controller during normal and abnormal events to maintain reliability. The SuperLab team across the five labs implemented a notional power system model equivalent of transmission and distribution lines, represented by the data networks interconnecting the labs. Each lab continuously exchanged local parameters (such as P and Q) from its Hardware-In-Loop (CHIL) and Power Hardware-In-Loop (PHIL) assets through centralized energy controller at NLR, enabling real-time interaction and coordination across sites. By leveraging ESnet as the communication backbone, the team successfully operated the distributed assets as a unified power system, with each bus represented by a different laboratory. This setup mirrors how assets interact in real-world power systems across dispersed locations with various protocols and latencies. At each lab site, assets were operated using their own local controllers which were coordinated through an overarching operation and control layer of centralized energy controller, equivalent to how an energy management system (EMS) orchestrates assets across a regional or national grid. SuperLab's federated connectivity utilized a Digital Real-Time Simulators (DRTS)-type gateway to connect Controller Hardware-In-Loop (CHIL) and PHIL assets between labs. To enable this federated connection through ESnet, a deterministic network was established where latency variations were consistent. This consistency allowed the development of digital filters for the power system assets across CHIL and PHIL interfaces to avoid unstable and unreliable grid conditions. This report provides an overview of the cross-laboratory configuration and offers insights into interconnecting geographically distributed research assets to test them as if they were co-located. This experiment represents a step toward linking nine DOE national laboratories, enabling nation-wide simulations that can address utility-driven challenges with grid resilience, flexibility, and modernization.

24 POWER TRANSMISSION AND DISTRIBUTION↗

DOE OSTI2017

Pilot Plant Test of Removal of Co-60 and Cs-137 from the Evaporator Concentrates of Forsmark unit 3 - 17158

A pilot plant test has been conducted to treat evaporator concentrates at Forsmark BWR NPP unit 3 in Sweden using Fortum's selective ion exchanger technology. The concentrate contains an array of radionuclides of which C-60 and Cs-137 are radiologically the most important ones. Concentrate also contained a high salt content ∼ 20 g/l and high organic carbon loading ∼ 1 g/l The pilot system consisted of pre-treatment (mechanical filters, activated carbon, UV oxidation) and Cs and Co selective ion exchangers. CsTreat ion exchanger was very effective in removing Cs from the evaporator concentrate: {sup 137}Cs activity was lowered from the initial value 280 MBq/m{sup 3} to below detection limit 550 Bq/m{sup 3}. Removing Co was more complicated: results suggest that Co is bound to organic chelating compounds, thus fairly compete oxidation of organic carbon was required in order to achieve good ion exchange results. Finally, after total organic carbon (TOC) was treated to below 50 ppm, {sup 60}Co activity was lowered from the initial value of 57 MBq/m{sup 3} to 2.7 kBq/m{sup 3}. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

DOE OSTI2017

Water Cleaning System for the Exhaust Pipe of HLW Glass Melter (LFCM) - 17180

Vitrification technology has been generally applied to stabilize High-Level Radioactive Waste (HLW) generated from spent fuel reprocessing. In Japan, Joule Heated Liquid Fed Ceramic Melter (LFCM) system is selected for HLW vitrification and the recent active test has been successfully demonstrated its stable operation. The higher reliability of off-gas treatment system (OGTS) which consists of wet scrubber, absorbers and filters connected to the LFCM is also important to ensure long term system operation. The OGTS removes radioactive gases, mists and dust generated by LFCM and maintains radioactive containments by keeping negative pressure inside. In the past active and inactive tests, it was observed that differential pressure in the exhaust pipe attached to LFCM gradually increased during continuous operation and some deposits were observed inside the off-gas pipe. So the cleaning operation needs to be improved and more frequent in order to avoid the exhaust pipe clogging. Therefore we investigated several cleaning systems and operational methods for the exhaust pipe of LFCM. As a result, we have successfully developed the modified water cleaning system. In this presentation we will introduce our water cleaning system. In addition, we will present the result of inactive mock-up tests for the visualization of this water cleaning system. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

DOE OSTI2019

Preliminary Interpretations from Fall 2018 Field Test at Ne’ot Hovav

Presentation conclusions: Conservative tracer transport was reasonably consistent with earlier tests between RH11c and RH11a; No attempt to model bentonite colloids because of minimal elevation of Al concentrations over background; Modeling confirms what we knew already for Cs and Ce; Cs transports as solute that sorbs in matrix (after diffusion into matrix); Ce transports as colloid that is rapidly filtered; Sr not modeled, but qualitatively appears consistent with combination of colloid and solute transport

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2015

THE DARK ENERGY CAMERA

The Dark Energy Camera is a new imager with a 2.°2 diameter field of view mounted at the prime focus of the Victor M. Blanco 4 m telescope on Cerro Tololo near La Serena, Chile. The camera was designed and constructed by the Dark Energy Survey Collaboration and meets or exceeds the stringent requirements designed for the wide-field and supernova surveys for which the collaboration uses it. The camera consists of a five-element optical corrector, seven filters, a shutter with a 60 cm aperture, and a charge-coupled device (CCD) focal plane of 250 μm thick fully depleted CCDs cooled inside a vacuum Dewar. The 570 megapixel focal plane comprises 62 2k × 4k CCDs for imaging and 12 2k × 2k CCDs for guiding and focus. The CCDs have 15 μm × 15 μm pixels with a plate scale of 0.″263 pixel{sup −1}. A hexapod system provides state-of-the-art focus and alignment capability. The camera is read out in 20 s with 6–9 electron readout noise. This paper provides a technical description of the camera's engineering, construction, installation, and current status.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2012

High-performance analysis of filtered semantic graphs

High performance is a crucial consideration when executing a complex analytic query on a massive semantic graph. In a semantic graph, vertices and edges carry "attributes" of various types. Analytic queries on semantic graphs typically depend on the values of these attributes; thus, the computation must either view the graph through a filter that passes only those individual vertices and edges of interest, or else must first materialize a subgraph or subgraphs consisting of only the vertices and edges of interest. The filtered approach is superior due to its generality, ease of use, and memory efficiency, but may carry a performance cost. In the Knowledge Discovery Toolbox (KDT), a Python library for parallel graph computations, the user writes filters in a high-level language, but those filters result in relatively low performance due to the bottleneck of having to call into the Python interpreter for each edge. In this work, we use the Selective Embedded JIT Specialization (SEJITS) approach to automatically translate filters defined by programmers into a lower-level efficiency language, bypassing the upcall into Python. We evaluate our approach by comparing it with the high-performance C++ /MPI Combinatorial BLAS engine, and show that the productivity gained by using a high-level filtering language comes without sacrificing performance.

97 MATHEMATICS AND COMPUTING↗

DOE OSTI2019

Filter Aerosol Measurements for ARM

The goal of this study was to determine the best filter media for use in ARM PSAPs following the manufacturer discontinuation of the current filter media. The study comprised by multiple experiments to assess four potential replacement filter medium relative to the Pallflex E-70, which is being discontinued, and is documented in ARM ServiceNow under ENG0003846. The experiments laid out in the document ‘180504 Filter Aerosol Measurements for ARM.docx’ and several subsequent tests suggest that the Pallflex Emfab media is the best candidate for ongoing ARM filter-based absorbance measurements. Other media were ruled out based on particle-capture efficiency for small particles. In tests with Nigrosin, EMFAB exceeded all other media. Tests were done measuring reported absorbance for all media in Particle Soot Absorption Photometers (PSAPs) operated in parallel sampling under several conditions: ambient air, 3 sizes of black-dyed PSL (Poly Styrene Latex) spheres, and Nigrosin particles. These tests indicate a different factor of reported absorbance for each media relative to the original Pallflex E70 filter. The factor for the Azumi media was consistent with unpublished work by Ogren (NOAA). The tests described here were not exhaustive and were complicated by time-varying differences among the PSAPs used. However, it is concluded that they are sufficient to justify ARM switching to Emfab filter media for future ARM PSAP measurements. The remaining store of E70 will be reserved to quantitatively characterize differences between Emfab and E70 (and Azumi?) in both laboratory and field side-by-side tests as put forth in a succeeding ENG. This future work will empirically identify correction factors applicable to Emfab and quantify the uncertainty in comparing the historical E70 measurements with ongoing Emfab measurements. Comparison of PSAP measurements with an independent absolute ‘reference’ for aerosol absorbance, i.e., PhotoThermal Interferometry or difference measurements of Cavity Attenuated Phase Shift extinction (CAPS) minus Nephelometry scattering would be valuable but exceed the scope of ARM Infrastructure. While the characterization of correction factors is required for maintaining and improving accuracy in future absorption measurements, it was beyond the scope of the current study.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2019

Filter Aerosol Measurements for ARM

The goal of this study was to determine the best filter media for use in Atmospheric Radiation Measurement (ARM) particle soot absorption photometers (PSAPs) following the manufacturer discontinuation of the current filter media. The study comprised multiple experiments to assess four potential replacement filter medium relative to the Pallflex E-70, which is being discontinued, and is documented in ARM’s ServiceNow system under ENG0003846. The experiments laid out in the document ‘180504 Filter Aerosol Measurements for ARM.docx’ and several subsequent tests suggest that the Pallflex Emfab media is the best candidate for ongoing ARM filter-based absorbance measurements. Other media were ruled out based on particle capture efficiency for small particles. In tests with Nigrosin, Emfab exceeded all other media. Tests were done measuring reported absorbance for all media in PSAPs operated in parallel sampling under several conditions: ambient air, three sizes of black-dyed PSL (polystyrene latex) spheres, and Nigrosin particles. These tests indicate a different factor of reported absorbance for each media relative to the original Pallflex E70 filter. The factor for the Azumi media was consistent with unpublished work by Ogren (National Oceanic and Atmospheric Administration [NOAA]). The tests described here were not exhaustive and were complicated by time-varying differences among the PSAPs used. However, it is concluded that they are sufficient to justify ARM switching to Emfab filter media for future ARM PSAP measurements. The remaining store of E70 will be reserved to quantitatively characterize differences between Emfab and E70 (and Azumi?) in both laboratory and field side-by-side tests as put forth in a succeeding ENG. This future work will empirically identify correction factors applicable to Emfab and quantify the uncertainty in comparing the historical E70 measurements with ongoing Emfab measurements. Comparison of PSAP measurements with an independent absolute ‘reference’ for aerosol absorbance, i.e., photo thermal interferometry or difference measurements of cavity attenuated phase shift extinction (CAPS) minus nephelometry scattering, would be valuable but exceed the scope of ARM Infrastructure. While the characterization of correction factors is required for maintaining and improving accuracy in future absorption measurements, it was beyond the scope of the current study.

aerosol observing system↗

DOE OSTI2019

Energy efficient photonic millimeter-wave generation using cascaded polarization modulators

A filter-less millimeter-wave generation scheme consisting of four polarization modulators in series, each followed by a polarizer is proposed to achieve optoelectronic frequency octupling. The cascade of polarization modulator and polarizer provides an intensity modulator whose biasing condition can be set by the polarizer angle and polarization state of the input light to each polarization modulator. A theoretical analysis of the architecture is performed using a transfer function method and validated by industry-standard software simulation tools. The circuit shows high potential in achieving desired performance with lower input RF power when compared to the another configuration based on a generalized Mach–Zehnder interferometer structure. Although the operating range in terms of applied RF drive becomes narrow, low RF input operation can be achieved by this circuit. The effect of imbalances in the key circuit parameters is also investigated in terms of electrical side harmonic suppression ratio.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2016

Assessing global fossil fuel availability in a scenario framework

This study assesses global, long-term economic availability of coal, oil and gas within the Shared Socio-economic Pathway (SSP) scenario framework considering alternative assumptions as to highly uncertain future developments of technology, policy and the economy. Diverse sets of trajectories are formulated varying the challenges to mitigation and adaptation of climate change. The potential CO2 emissions from fossil fuels make it a crucial element subject to deep uncertainties. The analysis is based on a well-established data set of cost-quantity combinations that assumes favorable techno-economic developments, but ignores additional constraints on the extraction sector. This study significantly extends that analysis to include alternative assumptions for the fossil fuel sector consistent with the SSP scenario families and applies these filters to the original data set, thus resulting in alternative cumulative fossil fuel availability curves. In a Middle-of-the-Road scenario, low cost fossil fuels embody carbon consistent with a RCP6.0 emission profile, if all the CO2 were emitted freely during the 21st century. In scenarios with high challenges to mitigation, the assumed embodied carbon in low-cost fossil fuels can trigger a RCP8.5 scenario; low mitigation challenges scenarios are still consistent with a RCP4.5 scenario.

Extraction Cost↗

DOE OSTI2025

Effects of Quantum Dot Loading on the Radioluminescence Efficiency in Quantum-Dot-Embedded Composites

Nanoparticle-embedded plastic scintillators are an emerging technology for fast, large-area, high-resolution radiation detection and imaging. Here, this study investigates the properties of such composites, focusing on the effects of the quantum dot (QD) concentration on the radioluminescence (RL) intensity, spectra, and dynamics. Experiments using CdSe/CdS QDs in a polymer reveal a superlinear increase in RL with the QD concentration despite optical losses from inner filtering and interparticle interactions. When corrected for inner filtering, RL shows a quadratic concentration dependence, consistent with simple analytical models of improving the secondary electron capture. Practically, the benefits of high QD concentrations are muted by optical losses, but the findings apply to other systems with insulating hosts. In addition to manipulating emission for large effective Stokes shifts, future improvements may come from hosts with higher stopping power and better charge transport, which enable more effective funneling of excitations but without concomitant optical losses associated with high nanoparticle concentrations.

Auger recombination↗

DOE OSTI2016

Digging deeper into the Southern skies: A compact Milky Way companion discovered in first-year Dark Energy Survey data

Here, the Dark Energy Survey (DES) is a 5000 sq. degree survey in the southern hemisphere, which is rapidly reducing the existing north-south asymmetry in the census of MW satellites and other stellar substructure. We use the first-year DES data down to previously unprobed photometric depths to search for stellar systems in the Galactic halo, therefore complementing the previous analysis of the same data carried out by our group earlier this year. Our search is based on a matched filter algorithm that produces stellar density maps consistent with stellar population models of various ages, metallicities, and distances over the survey area. The most conspicuous density peaks in these maps have been identified automatically and ranked according to their significance and recurrence for different input models. We report the discovery of one additional stellar system besides those previously found by several authors using the same first-year DES data. The object is compact, and consistent with being dominated by an old and metal-poor population. DES J0034-4902 is found at high significance and appears in the DES images as a compact concentration of faint blue point sources at ~ 87 {kpc}.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2017

A simple dynamic subgrid-scale model for LES of particle-laden turbulence

In this study, a dynamic model for large-eddy simulations is proposed in order to describe the motion of small inertial particles in turbulent flows. The model is simple, involves no significant computational overhead, contains no adjustable parameters, and is flexible enough to be deployed in any type of flow solvers and grids, including unstructured setups. The approach is based on the use of elliptic differential filters to model the subgrid-scale velocity. The only model parameter, which is related to the nominal filter width, is determined dynamically by imposing consistency constraints on the estimated subgrid energetics. The performance of the model is tested in large-eddy simulations of homogeneous-isotropic turbulence laden with particles, where improved agreement with direct numerical simulation results is observed in the dispersed-phase statistics, including particle acceleration, local carrier-phase velocity, and preferential-concentration metrics.

42 ENGINEERING↗

DOE OSTI2012

Effectiveness of copper and bronze for zinc capture

A series of experiments was conducted to determine the efficacy of using copper and bronze sheet and screen under high vacuum conditions to capture zinc vapor. The experiments were conducted in a parametric manner using a fixed zinc vaporization temperature (350°C) but varying the filter temperature from ambient to 550°C. Consistent with previous work, metallic zinc was deposited at low temperatures, but the deposit was non-adherent. At an intermediate temperature range (350-450°C), the deposit formed an alloy with both copper and bronze materials. At higher temperatures (> 500°C) the zinc did not deposit on the surfaces likely due to its high vapor pressure. Additional testing to optimize the zinc 'getter' chemistry and surface condition is warranted.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

DOE OSTI2011

Biodiesel Impact on Engine Lubricant Dilution During Active Regeneration of Aftertreatment Systems

Experiments were conducted with ultra low sulfur diesel (ULSD) and 20% biodiesel blends (B20) to compare lube oil dilution levels and lubricant properties for systems using late in-cylinder fuel injection for aftertreatment regeneration. Lube oil dilution was measured by gas chromatography (GC) following ASTM method D3524 to measure diesel content, by Fourier transform infrared (FTIR) spectrometry following a modified ASTM method D7371 to measure biodiesel content, and by a newly developed back-flush GC method that simultaneously measures both diesel and biodiesel. Heavy-duty (HD) engine testing was conducted on a 2008 6.7L Cummins ISB equipped with a diesel oxidation catalyst (DOC) and diesel particle filter (DPF). Stage one of engine testing consisted of 10 consecutive repeats of a forced DPF regeneration event. This continuous operation with late in-cylinder fuel injection served as a method to accelerate lube-oil dilution. Stage two consisted of 16 hours of normal engine operation over a transient test cycle, which created an opportunity for any accumulated fuel in the oil sump to evaporate. Light duty (LD) vehicle testing was conducted on a 2010 VW Jetta equipped with DOC, DPF and a NOx storage catalyst (NSC). Vehicle testing comprised approximately 4,000 miles of operation on a mileage-accumulation dynamometer (MAD) using the U.S. Environmental Protection Agency's Highway Fuel Economy Cycle because of the relatively low engine oil and exhaust temperatures, and high DPF regeneration frequency of this cycle relative to other cycles examined. Comparison of the lube oil dilution analysis methods suggests that D3524 does not measure dilution by biodiesel. The new back-flush GC method provided analysis for both diesel and biodiesel, in a shorter time and with lower detection limit. Thus all lube oil dilution results in this paper are based on this method. Analysis of the HD lube-oil samples showed only 1.5% to 1.6% fuel dilution for both fuels during continuous operation under DPF regeneration events. During the second stage of HD testing, the ULSD lube-oil dilution levels fell from 1.5% to 0.8%, while for B20, lube-oil dilution levels fell from 1.6% to 1.0%, but the fuel in the oil was 36% biodiesel. For the LD vehicle tests, the frequency of DPF regeneration events was observed to be the same for both ULSD and B20. No significant difference between the two fuels' estimated soot loading was detected by the engine control unit (ECU), although a 23% slower rate of increase in differential pressure across DPF was observed with B20. It appears that the ECU estimated soot loading is based on the engine map, not taking advantage of the lower engine-out particulate matter from the use of biodiesel. After 4,000 miles of LD vehicle operation with ULSD, fuel dilution in the lube-oil samples showed total dilution levels of 4.1% diesel. After 4,000 miles of operation with B20, total fuel in oil dilution levels were 6.7% consisting of 3.6% diesel fuel and 3.1% biodiesel. Extrapolation to the 10,000-mile oil drain interval with B20 suggests that the total fuel content in the oil could reach 12%, compared to 5% for operation on ULSD. Analysis of the oil samples also included measurement of total acid number, total base number, viscosity, soot, metals and wear scar; however, little difference in these parameters was noted.

09 BIOMASS FUELS↗

DOE OSTI2023

IPN Absorption Coefficients

The dataset contains aerosol light absorption and scattering coefficients measured by three single-wavelength Integrated Photoacoustic Nephelometers (IPN). The absorption coefficients were measured at 405, 721, and 1047 nm, while the scattering coefficients were measured at 405 and 721 nm. The single scattering albedo (SSA) at 405 and 721 nm were also calculated from the IPN measurements. The three IPNs shared a common inlet without impactor/cyclone in July; in August, a PM2.5 cyclone inlet was installed to reduce measurement noise and improve data quality. The 721-nm IPN experienced laser shutdown issues, causing missing of a large fraction of the 721-nm measurements, especially in July. As described before, the 721-nm laser issue was less frequent in August after the cyclone installation, improving the data completeness and quality. The IPN raw data were noisy, making identifying patterns and trends difficult; therefore, the hourly average data are recommended over the raw data. The hourly average data were cross-checked with the filter-based TAP and PSAP measurements, which showed that their patterns, trends, and peaks matched. However, due to the differences in working mechanisms and principles of the filter-based and photoacoustic particle-phase instruments, the IPN measurements are lower than the filter-based measurements despite that they have consistent patterns, trends, and peaks.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2013

Plan for the Purchase of MCT and EDS Reference Materials, Source Filters, Cu Strips, and Carousel Sub-Assemblies

The goal of this effort is to improve the quality and consistency of MCT and EDS data across the program. New references, aluminum (Al) and Cu filters, and Cu strips will be of known high purity and quality, traceable to documented chemical analyses. A single Program organization will be responsible to purchase, fabricate, assemble, inspect, control, and supply these items to the Program to ensure adequate and uniform quality and quality control.

42 ENGINEERING↗

DOE OSTI2015

In-situ tube burst testing and high-temperature deformation behavior of candidate materials for accident tolerant fuel cladding

The high resistance of cladding to plastic deformation and burst failure is one of the most essential properties of accident tolerant fuel (ATF) for maintaining structural integrity during a loss-of-coolant accident (LOCA) since the deformation and burst behavior governs the cooling efficiency of flow channels and process of fission product release. To simulate and evaluate such deformation and burst process of thin-walled cladding, an in-situ testing and evaluation method has been developed on the basis of visual imaging and image analysis techniques. The method uses a specialized optics system consisted of a high-resolution video camera, light filtering unit, and monochromatic light sources, and the in-situ testing is performed using a 50 mm long pressurized thin-walled tubular specimen set in a programmable furnace. In this study eleven (11) candidate cladding materials for ATF, i.e., 6 FeCrAl alloys and 5 nanostructured steels, were tested using the newly developed method, and the time-dependent images were analyzed to produce detailed deformation and burst data such as true hoop stress, strain (creep) rate, and failure stress. Relatively soft FeCrAl alloys deformed and burst below 800°C while negligible strain rates were measured for higher strength alloys and/or for relatively thick wall specimens.

Gussev, Maxim N.↗