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At least 127 records · Page 7

Structure of the St. Francois Mountains and surrounding lead belt, S. E. Missouri: Inferences from thermal IR and other data sets

Heat Capacity Mapping Mission (HCMM) in the form of an apparent thermal inertia image were merged with shaded relief maps and Bouguer gravity maps. The HCMM data show that the dominant structural grain in Missouri strikes in a northwesterly direction. The strike is the same as a major basement fault or flexure identified on the basis of gravity images.

Arvidson, R. E.↗

The Pikwitonei granulite domain: A lower crustal level along the Churchill-Superior boundary in central Manitoba

The greenschist to amphibolite facies tonalite-greenstone terrain of the Gods Lake subprovince grades - in a northwesterly direction - into the granulite facies Pikwitonei domain at the western margins of the Superior Province. The transition is the result of prograde metamorphism and takes place over 50 - 100 km without any structural or lithological breaks. Locally the orthopyroxene isograd is oblique to the structural grain and transects greenstone belts, e.g., the Cross Lake belt. The greenstone belts in the granulite facies and adjacent lower grade domain consist mainly of mafic and (minor) ultramafic metavolcanics, and clastic and chemical metasedimentary rocks. Typical for the greenstone belts crossed by the orthopyroxene isograd are anorthositic gabbros and anorthosites, and plagiophyric mafic flows. The Pikwitonei granulite domain has been interpreted as to represent a lower crustal level which was uplifted to the present level of erosion. On the basis of gravimetric data this uplift has been modelled as an obduction onto the Churchill Province during the Hudsonian orogeny, similar to the Ivrea Zone. The fault between the Churchill and Superior Province is described.

Weber, W.↗

Effects of Non-equilibrium Solidification on the Material Properties of Brick Silicon for Photovoltaics

Silicon ingot growth technologies like the Ubiquitous Crystallization Process (UCP) are solidified within a shaping crucible. The rate at which heat can be lost from this crucible minus the rate at which heat is input from an external source determines the rate at which crystallization will occur. Occasionally, when the process parameters for solidification are exceeded, the normally large multi-centimeter grain size material assocated with the UCP will break down into regions containing extremely small, millimeter or less, grain size material. Accompanying this breakdown in grain growth is the development of so called sinuous grain boundaries. The breakdown in grain growth which results in this type of small grain structure with sinuous boundaries is usually associated with the rapid crystallization that would accompany a system failure. This suggests that there are limits to the growth velocity that one can obtain and still expect to produce material that would possess good photovoltaic properties. It is the purpose to determine the causes behind the breakdown of this material and what parameters will determine the best rates of solidification.

Regnault, W. F.↗

Electromagnetic Hammer for Metalworking

High eddy currents apply pressure for cold-forming. Coil housing constructed for mechanical strength to hold coil against magnetic force, to maintain electrical contact with coil ends, and to maintain insulation between coil turns. Drilled holes placed to facilitate release of bubbles during potting. In contrast with mechanical hammers, electromagnetic hammer requires no dynamic material contact with workpiece; consequently, produces almost no change in metal grain structure.

Anderson, S. A.↗

Plasma diagnosis from thermal noise and limits on dust flux or mass in comet Giacobini-Zinner

Thermal noise spectroscopy was used to measure the density and temperature of the main (cold) electron plasma population during two hours around the point of closest approach of the International Cometary Explorer (ICE) to comet Giacobini-Zinner. The time resolution was 18 seconds in the plasma tail and 54 seconds elsewhere. Near the tail axis, the maximum plasma density was 670/cu cm and the temperature slightly above one volt. Away from the axis, the plasma density dropped to 100/cu cm over 2000 km, then decreased to 10/cu cm over 15,000 km; at the plasma tail, the density fluctuated between 10 and 30/cu cm, and the temperature, between 100,000 and 400,000 K. No evidence was found of grain impact on the spacecraft or antennas in the plasma tail. This yields an upper limit for the dust flux or particle mass, indicating either fluxes or masses in the tail smaller than those implied by models or an anomalous grain structure. Outside the tail, and particularly near 100,000 km from its axis, impulsive noises indicating plasma turbulence were observed.

Meyer-Vernet, N.↗

A preliminary study of factors affecting the calibration stability of the iridium versus iridium-40 percent rhodium thermocouple

An iridium versus iridium-40% rhodium thermocouple was studied. Problems associated with the use of this thermocouple for high temperature applications (up to 2000 C) were investigated. The metallurgical studies included X-ray, macroscopic, resistance, and metallographic studies. The thermocouples in the as-received condition from the manufacturer revealed large amounts of internal stress caused by cold working during manufacturing. The thermocouples also contained a large amount of inhomogeneities and segregations. No phase transformations were observed in the alloy up to 1100 C. It was found that annealing the thermocouple at 1800 C for two hours, and then at 1400 C for 2 to 3 hours yielded a fine grain structure, relieving some of the strains, and making the wire more ductile. It was also found that the above annealing procedure stabilized the thermal emf behavior of the thermocouple for application below 1800 C (an improvement from + or - 1% to + or - 0.02% within the range of the test parameters used).

Ahmed, Shaffiq↗

Curvilinear ridges and related features in southwest Cydonia Mensae, Mars

Examined is a region on Mars in southwest Cydonia Mensae (32 deg lat., 17 deg long.) just northwest of the lowland/upland boundary escarpment. The dominant morphological features in this region are the clusters of large massifs and plateau outliers (PI), knobby material (K), and smooth lowland plains (Ps). Surrounding the clusters and linking many isolated knobs is a system of curvilinear ridges and arcuate terrain boundaries which tend to separate the massifs and knobs from the smooth plains. Curvilinear ridges are arcuate to nearly linear and smoother in plan than wrinkle ridges and show no apparent correlation with regional structural grain. They are typically 5 to 10 km long but can range from as little as 2 or 3 km to greater than 50 km long. The widths vary from about 100 m to as much as 2 km. Curvilinear ridges are most numerous within 100 km of the lowland/upland boundary escarpment and are associated with massifs and knobby terrain. Arcuate terrain boundaries appear between units of different apparent albedo or arcuate breaks in slope.

Parker, Timothy J.↗

Microstructural variations induced by gravity level during directional solidification of near-eutectic iron-carbon type alloys

The effects of gravity on the microstructure of directionally solidified near-eutectic cast irons are studied, using a Bridgman-type automatic directional solidification furnace aboard a NASA KC-135 aircraft which flies parabolic arcs and generates alternating periods of low-g (0.01 to 0.001 g, 30 seconds long) and high-g (1.8 g, 1.5 minutes long). Results show a refinement of the interlamellar spacing of the eutectic during low-g processing of metastable Fe-C eutectic alloys. Low-g processing of stable Fe-C-Si eutectic alloys (lamellar or spheroidal graphic) results in a coarsening of the eutectic grain structure. Secondary dendrite arm spacing of austenite increases in low-g and decreases in high-g. The effectiveness of low-gravity in the removal of buoyancy-driven graphite phase segregation is demonstrated.

Stefanescu, Doru M.↗

Microstructures of undercooled germanium droplets

Undercoolings at crystal nucleation onset of liquid Ge droplets are measured and the microstructures of the droplets are examined. Undercooling values ranging from 150-415 + or 20 C were obtained. It is observed that for the samples undercooled less than 300 C prior to solidification the grain size was greater than 100 microns; for samples undercooled between 300-400 C the grain size was between 50-100 microns; and for samples undercooled greater than 400 C the grain size was 10-20 microns. Consideration is given to dendritic growth and interfacial undercooling. It is noted that there is a correlation between undercooling and as-crystallized grain structure.

Devaud, G.↗

Effect of processing on fracture toughness of silicon carbide as determined by Vickers indentations

Several alpha-SiC materials were processed by hot isostatic pressing (HIPing) and by sintering an alpha-SiC powder containing boron and carbon. Several beta-SiC materials were processed by HIPing a beta-SiC powder with boron and carbon additions. The fracture toughnesses K(sub 1c) of these beta- and alpha-SiC materials were estimated from measurements of Vickers indentations. The three formulas used to estimate K(sub 1c) from the indentation fracture patterns resulted in three ranges of K(sub 1c) estimates. Furthermore, each formula measured the effects of processing differently. All three estimates indicated that fine-grained HIPed alpha-SiC has a higher K(sub 1c) than coarsed-grained sintered alpha-SiC. Hot isostatically pressed beta-SiC, which had an ultrafine grain structure, exhibited a K(sub 1c) comparable to that of HIPed alpha-SiC.

Dannels, Christine M.↗

Melt-processed bulk superconductors: Fabrication and characterization for power and space applications

Melt-process bulk superconducting materials based on variations on the base YBa2Cu3O(x) were produced in a variety of shapes and forms. Very high values of both zero-field and high-field magnetization were observed. These are useful for levitation and power applications. Magnetic measurements show that the effects of field direction and intensity, temperature and time are consistent with an aligned grain structure with multiple pinning sites and with models of thermally activated flux motion.

Hojaji, Hamid↗

Recrystallization and superplasticity at 300 C in an aluminum-magnesium alloy

Variations in thermomechanical processing (TMP) which regulate the microstructural characteristics and superplastic response of an Al-10Mg-0.1Zr alloy at 300 C were evaluated. Mechanical property data revealed that the superplastic ductility can be enhanced by simultaneously increasing the total rolling strain, the reduction per pass, and the duration of reheating intervals between passes during isothermal rolling. Texture and microscopy data were consistent with the development of a refined microstructure by recovery-dominated processes, i.e., continuous recrystallization, during the processing. The mechanisms by which a refined substructure can be progressively converted into a fine-grained structure during repeated cycles of deformation and annealing are addressed. A qualitative description of the complex sequence of developments leading to a microstructure better suited to support superplastic response is presented.

Hales, S. J.↗

Improved Warm-Working Process For An Iron-Base Alloy

Warm-working process produces predominantly unrecrystallized grain structure in forgings of iron-base alloy A286 (PWA 1052 composition). Yield strength and ultimate strength increased, and elongation and reduction of area at break decreased. Improved process used on forgings up to 10 in. thick and weighing up to 900 lb.

Cone, Fred P.↗

Crack-Growth Resistance of in Situ-Toughened Silicon Nitride

The fracture toughness of a commercial, hot-pressed, in situ-toughened silicon nitride with an elongated grain structure is determined by four different testing methods. The fracture toughness is found to be 5.76 +/- 0.27, 8.48 +/- 0.50, 10.16 +/- 0.66, and 10.68 +/- 0.39 MPa x m(exp 1/2), respectively, by indentation crack size measurement, indentation strength, single-edge-precracked-beam, and chevron-notched-beam methods. The discrepancy in fracture toughness between the testing methods is related to R-curve behavior, as measured using the indentation strength technique. These results indicate that there is no unique fracture toughness value and that a fracture toughness testing method with appropriate qualifiers is needed for rising R-curve materials. Therefore, care should be taken in interpreting and utilizing fracture toughness values evaluated from different testing methods if a material exhibits a rising R-curve. Complete characterization of the R-curve may be a prerequisite.

Salem, Jonathan A.↗

Use of NH4Cl-H2O Analogue Castings to Model Aspects of Continuous Casting: Asymmetry in Inclined Moulds - Part 1

Crystallisation of NH4Cl from aqueous solutions has been used to examine grain formation in a configuration similar to that existing in the curved mould of a continuous, steel casting machine. The observations show how falling equiaxed crystals accumulate at the lower (outer) columnar front earlier than at the upper (inner) front and, thus, lead to an asymmetric grain structure. The usefulness of the aqueous system as a realistic model for steel casting is discussed in terms of relative temperature profiles, materials properties, and observed columnar and eutectic growth rates.

Jang, J.↗

Process Model for Friction Stir Welding

Friction stir welding (FSW) is a relatively new process being applied for joining of metal alloys. The process was initially developed by The Welding Institute (TWI) in Cambridge, UK. The FSW process is being investigated at NASA/MSEC as a repair/initial weld procedure for fabrication of the super-light-weight aluminum-lithium shuttle external tank. The FSW investigations at MSFC were conducted on a horizontal mill to produce butt welds of flat plate material. The weldment plates are butted together and fixed to a backing plate on the mill bed. A pin tool is placed into the tool holder of the mill spindle and rotated at approximately 400 rpm. The pin tool is then plunged into the plates such that the center of the probe lies at, one end of the line of contact, between the plates and the shoulder of the pin tool penetrates the top surface of the weldment. The weld is produced by traversing the tool along the line of contact between the plates. A lead angle allows the leading edge of the shoulder to remain above the top surface of the plate. The work presented here is the first attempt at modeling a complex phenomenon. The mechanical aspects of conducting the weld process are easily defined and the process itself is controlled by relatively few input parameters. However, in the region of the weld, plasticizing and forging of the parent material occurs. These are difficult processes to model. The model presented here addresses only variations in the radial dimension outward from the pin tool axis. Examinations of the grain structure of the weld reveal that a considerable amount of material deformation also occurs in the direction parallel to the pin tool axis of rotation, through the material thickness. In addition, measurements of the axial load on the pin tool demonstrate that the forging affect of the pin tool shoulder is an important process phenomenon. Therefore, the model needs to be expanded to account for the deformations through the material thickness and the forging affect of the shoulder. The energy balance at the boundary of the plastic region with the environment required that energy flow away from the boundary in both radial directions. One resolution to this problem may be to introduce a time dependency into the process model, allowing the energy flow to oscillate across this boundary. Finally, experimental measurements are needed to verify the concepts used here and to aid in improving the model.

Adams, Glynn↗

Real-Time X-Ray Microscopy of Al-Cu Eutectic Solidification

Recent improvements in the resolution of the X-ray Transmission Microscope (XTM) for Solidification Studies provide microstructure feature detectability down to 5 micrometers during solidification. This presentation will show the recent results from observations made in real-time of the solid-liquid interfacial morphologies of the Al-CuAI2 eutectic alloy. Lamellar dimensions and spacings, transitions of morphology caused by growth rate changes, and eutectic grain structures are open to measurements. A unique vantage point viewing the face of the interface isotherm is possible for the first time with the XTM due to its infinite depth of field. A video of the solid-liquid interfaces seen in-situ and in real-time will be shown.

Kaukler, William F.↗

Diagnostic Clast-Texture Criteria for Recognition of Impact Deposits

It is difficult to find definitive evidence for impact in the geological record because there are many endogenous geological processes that can produce diamictites similar to those generated by impact ejecta. The classic impact criteria of shock fabrics in certain minerals, and iridium layers, for example, may be either difficult to find, or long-since erased from the impact site (shock fabrics also anneal with time). It is important to be able to recognize impact-generated materials in order to understand earth's crustal development and biological evolution. In future exploration of Mars and other solar-system bodies, recognition of impact materials will be important for elucidating planetary evolution, planetary volatile inventories, and exobiological issues. The cobble depicted is typical of many that have been found in diamictite deposits in Belize generated by the Chicxulub K-T impact event. The pebbles are roughly-hewn in general shape with smoothed corners and edges. Surfaces are almost uniformly frosted (on both protuberances and hollows), but some asperities are glazed. Optical microscopy and thin-section petrographic microscopy reveal the frosting to be only a few microns thick, with a well-defined granular structure; grains are the same size as those composing the bulk of the limestone, but their clearer appearance may represent annealing. One or two adjacent pebble faces are often decorated with striated gouges and closely-spaced hemispherical depressions representing indentation hollows produced by well-rounded impacting clasts of up to 0.5 cm in diameter. Some of the impactors are still embedded in the cobble surface. Non-destructive x-ray diffraction techniques showed the impactors to be of the same mineralogy as the target cobble. We believe this unusual glazing and frosting to be related to the impact event, but this must be reconciled with its survival for over 60 my. since it is composed of one of the most alterable substances, CaCO3. We focus, however, on the non-fractured rounded pebbles that appear to have impacted the larger cobble as a swarm of clasts, probably encountered during ballistic flight. It cannot be defined whether the cobble swept through the pebble cloud, or the pebbles rained upon a slowermoving cobble. Two interesting questions arise: (1) Where did large numbers of such well rounded pebbles come from in the ejecta curtain?, and (2) How did they embed themselves in a nominally brittle rock without suffering damage? Are the well-rounded pebbles crystalline (devitrified) melt spherules? Further investigations are in progress. If the cobble was cold and brittle, impact of well-rounded pebbles would have produced Hertzian fracture patterns (a) in the virtually elastically isotropic cobble target. For penetration depths of about 0.5 of the impactor diameter, the pebbles would require a relative impact velocity sufficient to cause pebble fragmentation and crushing, and the development of a complex Hertzian-Boussinesq fracture field (b) involving deep fracturing and lateral surface spalling (impact velocities > 50 m/s). The existing relationship could only evolve by the impact of cold, hard pebbles into a soft, plastic cobble surface (c). For limestone to have been plastic, it must have been at elevated temperature, but to prevent calcification of the material, the ambient pressure must also have been elevated. This would be possible either in the impact's gas plume, or within the confines of a thin aerodynamically-produced shock bow generated by supersonic ballistic motion of the cobble. In the latter case, it is implied that the cobble swept through the pebbles rather than vice-versa. Although there are high T-P conditions associated with volcanism, such textures have not been reported on volcaniclastic materials, nor from other high T-P environments; e.g., metamorphic (as far as the authors are aware). We propose that this very easily recognizable embedding and indentation surface texture can be used as a diagnostic criterion for the recognition of impact ejecta. The term "peening texture" is suggested, because it is absolutely analogous to the plastic-deformation induced, metal-surface textures generated by ball-bearing bombardment used in engineering metallurgy to work-harden metal surfaces. Additional information is contained in the original (Figures).

Marshall, J. R.↗