Diffusion wave phenomena
Thermal and bleaching waves as diffusion phenomena in opposite limits, discussing laser heating
Ahlstrom, H. G.↗
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Beryllium particle combustion
A two-year study of the combustion efficiency of single beryllium droplets burning in a variety of oxidizers (primarily mixtures of oxygen/argon and oxygen/nitrogen) is summarized. An advanced laser heating technique was used to acquire systematic quantitative data on the burning of single beryllium droplets at atmospheric pressure. The research confirmed the sensitivity of beryllium droplet combustion to the chemistry of environmental species and provides experimental documentation for the nitrogen-induced droplet fragmentation of burning beryllium droplets.
Prentice, J. L.↗
Advanced photon engines
Photon engines which convert coherent radiation back to energy with efficiencies of approximately 60 percent are considered. Components of the system include; a simple regenerated Brayton cycle, an energy exchanger device, and laser heating techniques.
Hertzberg, A.↗
Absorption of CO2-laser radiation in a hypocycloidal-pinch plasma
Absorption of a 50-J pulsed CO2 laser beam in the plasma produced in a hypocycloidal-pinch apparatus was studied. The apparatus consists of three disk electrodes with a 5-cm hole on the axis. The current sheets are snow-plowed toward the center of the hole to produce a plasma with a density greater than 10 to the 18th/cu cm and a temperature near 1 keV which emits soft X rays for 5 microsec. IR detectors measured the laser radiation incident onto, transmitted through, and scattered from the plasma as functions of time. For a period up to 70 microsec from the onset of X-ray emission, neither transmitted nor scattered laser radiation was observed above the detector threshold of 0.3% of the incident flux. This indicates effective absorption of the laser beam (greater than 99%) and that the particle confinement time extends far beyond the energy confinement time of 5 microsec. Thus, the plasma in this apparatus appears much more amenable to laser heating than that in a theta pinch.
Lee, J. H.↗
Alternative approaches to plasma confinement
The paper discusses 20 plasma confinement schemes each representing an alternative to the tokamak fusion reactor. Attention is given to: (1) tokamak-like devices (TORMAC, Topolotron, and the Extrap concept), (2) stellarator-like devices (Torsatron and twisted-coil stellarators), (3) mirror machines (Astron and reversed-field devices, the 2XII B experiment, laser-heated solenoids, the LITE experiment, the Kaktus-Surmac concept), (4) bumpy tori (hot electron bumpy torus, toroidal minimum-B configurations), (5) electrostatically assisted confinement (electrostatically stuffed cusps and mirrors, electrostatically assisted toroidal confinement), (6) the Migma concept, and (7) wall-confined plasmas. The plasma parameters of the devices are presented and the advantages and disadvantages of each are listed.
Roth, J. R.↗
Data acquisition techniques for exploiting the uniqueness of the time-of-flight mass spectrometer: Application to sampling pulsed gas systems
Mass spectra are produced in most mass spectrometers by sweeping some parameter within the instrument as the sampled gases flow into the ion source. It is evident that any fluctuation in the gas during the sweep (mass scan) of the instrument causes the output spectrum to be skewed in its mass peak intensities. The time of flight mass spectrometer (TOFMS) with its fast, repetitive mode of operation produces spectra without skewing or varying instrument parameters and because all ion species are ejected from the ion source simultaneously, the spectra are inherently not skewed despite rapidly changing gas pressure or composition in the source. Methods of exploiting this feature by utilizing fast digital data acquisition systems, such as transient recorders and signal averagers which are commercially available are described. Applications of this technique are presented including TOFMS sampling of vapors produced by both pulsed and continuous laser heating of materials.
Lincoln, K. A.↗
Vapor phase diamond growth technology
Ion beam deposition chambers used for carbon film generation were designed and constructed. Features of the developed equipment include: (1) carbon ion energies down to approx. 50 eV; (2) in suit surface monitoring with HEED; (3) provision for flooding the surface with ultraviolet radiation; (4) infrared laser heating of substrate; (5) residual gas monitoring; (6) provision for several source gases, including diborane for doping studies; and (7) growth from either hydrocarbon source gases or from carbon/argon arc sources. Various analytical techniques for characterization of from carbon/argon arc sources. Various analytical techniques for characterization of the ion deposited carbon films used to establish the nature of the chemical bonding and crystallographic structure of the films are discussed. These include: H2204/HN03 etch; resistance measurements; hardness tests; Fourier transform infrared spectroscopy; scanning auger microscopy; electron spectroscopy for chemical analysis; electron diffraction and energy dispersive X-ray analysis; electron energy loss spectroscopy; density measurements; secondary ion mass spectroscopy; high energy electron diffraction; and electron spin resonance. Results of the tests are summarized.
Angus, J. C.↗
Laser materials processing facility
The laser materials processing facility and its capabilities are described. A CO2 laser with continuous wave, repetitive pulse, and shaped power-time cycles is employed. The laser heated crystal growth station was used to produce metal and metal oxide single crystals and for cutting and shaping experiments using Si3N4 to displace diamond shaping processes.
Haggerty, J. S.↗
Containerless high temperature property measurements by atomic fluorescence
The use of laser induced fluorescence (LIF) techniques for containerless study of high temperature processes and material properties is studied. Gas jet and electromagnetic levitation and electromagnetic and laser heating techniques are used with LIF in Earth-based containerless high temperature experiments. The work to date includes development of an apparatus and its use in studies of chemical reactions on Al2O3, molybdenum, and tungsten specimens, novel methods for noncontact specimen temperature measurement, and levitation jet properties. Brief summaries of these studies are given. The apparatus is described and detailed results for the current reporting period are presented.
Source record↗
Containerless high temperature property measurements by atomic fluorescence
Laser induced fluorescence (LIF) techniques for containerless study of high temperature processes and material properties was studied. Gas jet and electromagnetic levitation and electromagnetic and laser heating techniques are used with LIF in earth-based containerless high temperature experiments. Included are the development of an apparatus and its use in the studies of (1) chemical reactions on Al2O3, molybdenum, tungsten and LaB6 specimens, (2) methods for noncontact specimen temperature measurement, (3) levitation jet properties and (4) radiative lifetime and collisional energy transfer rates for electronically excited atoms.
Schiffman, R. A.↗
Containerless High Temperature Property Measurements by Atomic Fluorescence
Laser induced fluorescence (LIF) provides a noncontact method for measuring high temperature properties. It is used with aerodynamic and/or electromagnetic levitation, and electromagnetic and/or CW CO2 laser heating to develop new methods for containerless high temperature property measurements and process control. The capabilities and limitations of Earth-based experiments are demonstrated and the information necessary to design improved experiments in space is obtained. The LIF methods were developed to measure temperature and component activities, which will be applied to containerless property measurements on liquids and to process control in synthesis experiments. Component activities will be obtained from relative LIF intensities over a compound and its components at the same temperature.
Nordine, P. C.↗
Spectroscopic analysis of insulating crystal fibers
A new technique is described for investigating the optical properties of solid-state laser materials using single-crystal fibers grown by a laser-heated pedestal-growth technique. Single-crystal fiber samples can be prepared more rapidly and less expensively than crystals grown by more conventional methods; however, they are smaller and less uniform, making spectroscopic measurements difficult. A simple procedure for extracting the optical absorption and emission spectra of insulating crystal fibers is demonstrated with a titanium-doped sapphire fiber sample; results are comparable to those from Czochralski-grown material.
Buoncristiani, A. M.↗
Laboratory studies of the electrical conductivity of silicate perovskites at high pressures and temperatures
The electrical conductivities of two silicate perovskites and a perovskite-magnesiowuestite assemblage, all having an atomic ratio of Mg to Fe equal to 0.88/0.12, have been measured with alternating current and direct current (dc) techniques at simultaneously high pressures and temperatures. Measurements up to pressures of 80 GPa and temperatures of 3500 K, using a laser-heated diamond anvil cell, demonstrate that the electrical conductivity of these materials remains below 10-3 S/m at lower mantle conditions. The activation energies for electrical conduction are between 0.1 and 0.4 eV from the data, and the conduction in these perovskites is ascribed to an extrinsic electronic process. The new measurements are in agreement with a bound that was previously obtained from dc measurements for the high-PT conductivity of perovskite-dominated assemblages. The results show that the electrical conductivity of (Mg/0.88/Fe/0.12)SiO3 perovskite differs significantly from that of the earth's deep mantle, as inferred from geophysical observations.
Li, Xiaoyuan↗
Ultrahigh-pressure melting of lead - A multidisciplinary study
Measurements of the melting temperatures of lead, carried out to pressures of 1 megabar and temperatures near 4000 kelvin by means of a laser-heated diamond cell are in excellent agreement with the results of previous shock-wave experiments. The data are analyzed by means of first principles quantum mechanical calculations, and the agreement documents the reliability of current experimental and theoretical techniques for studies of melting at ultrahigh pressures. These studies have potentially wide-ranging applications from planetary science to condensed matter physics.
Godwal, B. K.↗
Processes of deep terrestrial mantles and cores
Ultrahigh pressure experiments are currently focused on revealing processes occurring deep inside planets. This is in addition to the traditional emphasis on the constitution of planetary interiors, such as the identification of the high pressure perovskite phase of (Mg,Fe)SiO3 as the predominant mineral inside the Earth, and probably Venus. For example, experiments show that the mechanism of geochemical differentiation, separation of partial melts, differs fundamentally in the lower mantles of Earth and Venus than at near surface conditions. In addition to structural transformations, changes in chemical bonding caused by pressure can also be significant for planetary interiors. Measurements of AC and DC electrical conductivity can be obtained at ultrahigh pressures and temperatures, to greater than 80 GPa and 3000 K simultaneously, using the laser heated diamond cell. Anhydrous lower mantle assemblages (perovskite + or - oxide phases) exhibit an electrical conductivity that depends strongly on Fe content. Contrary to traditional assumptions, temperature affects the conductivity of lower mantle assemblages relatively little. The Earth's deep focus seismicity can be explained by the recycling of water into the mantle.
Jeanloz, Raymond↗
Growth of Sr(0.61)Ba(0.39)Nb2O6 fibers - New results regarding orientation
The paper describes stable growth of Sr(0.61)Ba(0.39)Nb2O6 (SBN) single-crystal optical fibers (grown by the laser-heated pedestal growth method) along the 100-line and 110-line crystallographic axes. The orientation of SBN fibers was investigated using transmission holograms recorded by focusing two separate, but mutually coherent, optical wavefronts into one end of the fiber. Results showed that the crystal quality of 100-line and 110-line SBN fibers grown at a given pull velocity strongly depended on the fiber diameter; generally, the quality improves with decreasing diameter.
Wilde, Jeffrey P.↗
Growth of new materials for solid state laser applications. The growth of ZnGeP2 by the vertical Bridgman method
This is the final technical report on the cooperative NASA program 'Growth of New Materials for Solid State Laser Applications,' covering the period from 9-1-86 through 3-31-91. The first two and one half years of the program, from 9-1-86 through 3-31-89, was devoted to the development of new eye-safe laser sources. Single crystal fibers of rare earth doped and co-doped YAG were grown by the laser-heated pedestal growth method, characterized for their structural properties and supplied to NASA/Langley for spectroscopic evaluation. From 4-1-89 though 3-31-91, research focused on the growth of zinc germanium phosphide for nonlinear optical applications in the IR. The vertical Bridgman growth process was evaluated as a means to achieve better control over the short wavelength optical absorption in this material that adversely affects 2 micron-pumped optical parametric oscillators.
Feigelson, R. S.↗
A neural network controller for automated composite manufacturing
At McDonnell Douglas Aerospace (MDA), an artificial neural network based control system has been developed and implemented to control laser heating for the fiber placement composite manufacturing process. This neurocontroller learns an approximate inverse model of the process on-line to provide performance that improves with experience and exceeds that of conventional feedback control techniques. When untrained, the control system behaves as a proportional plus integral (PI) controller. However after learning from experience, the neural network feedforward control module provides control signals that greatly improve temperature tracking performance. Faster convergence to new temperature set points and reduced temperature deviation due to changing feed rate have been demonstrated on the machine. A Cerebellar Model Articulation Controller (CMAC) network is used for inverse modeling because of its rapid learning performance. This control system is implemented in an IBM compatible 386 PC with an A/D board interface to the machine.
Lichtenwalner, Peter F.↗