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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 127 records · Page 7
All sourcesNASA NTRSDOE OSTI
NASA NTRS1994

New techniques for diffusing-wave spectroscopy

We present two new types of measurements that can be made with diffusing-wave spectroscopy (DWS), a form of dynamic light scattering that applies in limit of strong multiple scattering. The first application is to measure the frequency-dependent linear viscoelastic moduli of complex fluids using light scattering. This is accomplished by measuring the mean square displacement of probe particles using DWS. Their response to thermal fluctuations is determined by the fluctuation-dissipation relation, and is controlled by the response of the surrounding complex fluid. This response can be described in terms of a memory function, which is directly related to the complex elastic modulus of the system. Thus by measuring the mean square displacement, we are able to determine the frequency dependent modulus. The second application is the measurement of shape fluctuations of scattering particles. This is achieved by generalizing the theory for DWS to incorporate the effects if amplitude fluctuations in the scattering intensity of the particles. We apply this new method to study the thermally induced fluctuations in the shape of spherical emulsion droplets whose geometry is controlled by surface tension.

Mason, T. G.↗
NASA NTRS1994

A spectral formalism for computing three-dimensional deformations due to surface loads. 1: Theory

We outline a complete spectral formalism for computing high spatial resolution three-dimensional deformations arising from the surface mass loading of a spherically symmetric planet. The main advantages of the formalism are that all surface mass loads are always described using a consistent mathematical representation and that calculations of deformation fields for various spatial resolutions can be performed by simpley altering the spherical harmonic degree truncation level of the procedure. The latter may be important when incorporating improved observational constraints on a particular surface mass load, when considering potential errors in the computed field associated with mass loading having a spatial scale unresolved by the observational constraints, or when treating a number of global surface mass loads constrained with different spatial resolutions. The advantages do not extend to traditional 'Green's function' approaches which involve surface element discretizations of the global mass loads. Another advantage of the spectral formalism, over the Green's function approach, is that a posteriori analyses of the computed deformation fields are easily performed. In developing the spectral formalism, we consider specific cases where the Earth's mantle is assumed to respond as an elastic, slightly anelastic, or linear viscoelastic medium. In the case of an elastic or slightly anelastic mantle rheology the spectral response equations incorporate frequency dependent Love numbers. The formalism can therefore be used, for example, to compute the potentially resonant deformational response associated with the free core nutation and Chandler wobble eigenfunctions. For completeness, the spectral response equations include both body forces, as arise from the gravitational attraction of the Sun and the Moon, and surface mass loads. In either case, and for both elastic and anelastic mantle rheologies, we outline a pseudo-spectral technique for computing the ocean adjustment associated with the total gravitational perturbation induced by the external forcing. Three-dimensional deformations computed using the usual Love number approach are generally referenced to an origin at the center of mass of the undeformed planet. We derive a spectral technique for transforming the results to an origin located at the center of mass of the deformed planet.

Mitrovica, J. X.↗
NASA NTRS1994

A spectral formalism for computing three-dimensional deformations due to surface loads. 2: Present-day glacial isostatic adjustment

Using a spherically symmetric, self-gravitating, linear viscoelastic Earth model, we predict present-day three-dimensional surface deformation rates and baseline evolutions arising as a consequence of the late Pleistocene glacial cycles. In general, we use realistic models for the space-time geometry of the final late Pleistocene deglaciation event and incorporate a gravitationally self-consistent ocean meltwater redistribution. The predictions of horizontal velocity presented differ significantly, in both their amplitude and their spatial variation, from those presented in earlier analysis of others which adopted simplified models of both the late Pleistocene ice history and the Earth rheology. An important characteristic of our predicted velocity fields is that the melting of the Laurentide ice sheet over Canada is capable of contributing appreciably to the adjustment in Europe. The sensitivity of the predictions to variations in mantle rheology is investigated by considering a number of different Earth models, and by computing appropriate Frechet kernels. These calculations suggest that the sensitivity of the deformations to the Earth's rheology is significant and strongly dependent on the location of the site relative to the ancient ice sheet. The effects on the predictions of three-dimensional deformation rates of altering the ice history or adopting approximate models for the ocean meltwater redistribution have also been considered and found to be important (the former especially so). Finally, for a suite of Earth models we provide predictions of the velocity of a number of baselines in North America and Europe. We find that, in general, both radial and tangential motions contribute significantly to baseline length changes, and that these contributions are a strong function of the Earth model. We have, furthermore, found a set of Earth models which, together with the ICE-3G deglaciation chronology, produce predictions of baseline length changes that are consistent with very long baseline interferometry measurements of baselines within Europe.

Mitrovica, J. X.↗
NASA NTRS1998

Effects of Aging-Time Reference on the Long Term Behavior of the IM7/K3B Composite

An analytical study was undertaken to investigate the effects of the time-based shift reference on the long term behavior of the graphite reinforced thermoplastic polyimide composite IM7/K3B at elevated temperature. Creep compliance and the effects of physical aging on the time dependent response was measured for uniaxial loading at several isothermal conditions below the glass transition temperature (T(sub g). Two matrix dominated loading modes, shear and transverse, were investigated in tension and compression. The momentary sequenced creep/aging curves were collapsed through a horizontal (time) shift using the shortest, middle and longest aging time curve as the reference curve. Linear viscoelasticity was used to characterize the creep/recovery behavior and superposition techniques were used to establish the physical aging related material constants. The use of effective time expressions in a laminated plate model allowed for the prediction of long term creep compliance. The effect of using different reference curves with time/aging-time superposition was most sensitive to the physical aging shift rate at lower test temperatures. Depending on the loading mode, the reference curve used can result in a more accurate long term prediction, especially at lower test temperatures.

Veazie, David R.↗
NASA NTRS2004

Characterization of Space Shuttle External Tank Thermal Protection System (TPS) Materials in Support of the Columbia Accident Investigation

NASA suffered the loss of the seven-member crew of the Space Shuttle Columbia on February 1, 2003 when the vehicle broke apart upon re-entry to the Earth's atmosphere. The final report of the Columbia Accident Investigation Board (CAIB) determined that the accident was caused by a launch ascent incident-a suitcase-sized chunk of insulating foam on the Shuttle's External Tank (ET) broke off, and moving at almost 500 mph, struck an area of the leading edge of the Shuttle s left wing. As a result, one or more of the protective Reinforced Carbon-Carbon (RCC) panels on the wing leading edge were damaged. Upon re-entry, superheated air approaching 3,000 F breached the wing damage and caused the vehicle breakup and loss of crew. The large chunk of insulating foam that broke off during the Columbia launch was determined to come from the so-called bipod ramp area where the Shuttle s orbiter (containing crew) is attached to the ET. Underneath the foam in the bipod ramp area is a layer of TPS that is a cork-filled silicone rubber composite. In March 2003, the NASA Marshall Space Flight Center (MSFC) in Huntsville, Alabama received cured samples of the foam and composite for testing from the Michoud Assembly Facility (MAF) in New Orleans, Louisiana. The MAF is where the Shuttle's ET is manufactured. The foam and composite TPS materials for the ET have been well characterized for mechanical property data at the super-cold temperatures of the liquid oxygen and hydrogen fuels used in the ET. However, modulus data on these materials is not as well characterized. The TA Instruments 2980 Dynamic Mechanical Analyzer (DMA) was used to determine the modulus of the two TPS materials over a range of -145 to 95 C in the dual cantilever bending mode. Multi-strain, fixed frequency DMA tests were followed by multi-frequency, fixed strain tests to determine the approximate bounds of linear viscoelastic behavior for the two materials. Additional information is included in the original extended abstract.

Wingard, Charles D.↗
NASA NTRS1981

Postseismic rebound due to creep of the lower lithosphere and asthenosphere

Postseismic surface deformations are attributed to the inelastic flow of the subcrustal regions of the Earth following an earthquake. A multilayer representation of the Earth's rheological properties is used in conjunction with a finite element computational scheme to calculate time dependent displacements and strains subsequent to a strike slip earthquake. The deviatoric stress strain relations for the uppermost layer is assumed elastic. Lower layers are assumed to be, in order of increasing depth, a standard, linear, three element, viscoelastic solid; a linear viscoelastic fluid; and another elastic solid. Physically these layers correspond to the upper lithosphere, lower lithosphere, asthenosphere, and lower mantle, respectively. Elastic dilatational properties are assumed throughout. Appreciable postseismic displacements, possibly approaching meters, for large earthquakes, arise from viscoelastic relaxation following sudden coseismic slip. Furthermore, compared to the simpler case of an elastic lithosphere over a viscoelastic asthenosphere and the near fault postseismic shear, strain is increased, by a factor of two or more in some cases, by the presence of a viscoelastic lower lithosphere. Also, the duration of postseismic straining is increased by the relatively slow relaxation of this layer.

Cohen, S. C.↗
DOE OSTI2021

Linear and nonlinear viscoelasticity of concentrated thermoresponsive microgel suspensions

We present an integrated experimental and theoretical study of the dynamics and rheology of self-crosslinked, slightly charged, temperature responsive soft poly(N-isopropylacrylamide) (pNIPAM) microgels over a wide range of concentration and temperature spanning the sharp change in particle size and intermolecular interactions across the lower critical solution temperature (LCST). Dramatic, non-monotonic changes in viscoelasticity are observed as a function of temperature, with distinct concentration dependence in the dense fluid, glassy, and soft-jammed regimes. Motivated by our experimental observations, we formulate a minimalistic model for the size dependence of a single microgel particle and the change of the interparticle interaction from purely repulsive to attractive upon heating. Using microscopic equilibrium and time-dependent statistical mechanical theories, theoretical predictions are quantitatively compared with experimental measurements of the shear modulus. Good agreement is found for the nonmonotonic temperature behavior that originates as a consequence of the competition between reduced microgel packing fraction and increasing interparticle attractions. Furthermore, testable predictions are made for nonlinear rheological properties such as the yield stress and strain. To our knowledge, this is the first attempt to quantitatively understand in a unified manner the viscoelasticity of dense, temperature-responsive microgel suspensions spanning a wide range of temperatures and concentrations.

42 ENGINEERING↗
NASA NTRS1990

Bending and stretching finite element analysis of anisotropic viscoelastic composite plates

Finite element algorithms have been developed to analyze linear anisotropic viscoelastic plates, with or without holes, subjected to mechanical (bending, tension), temperature, and hygrothermal loadings. The analysis is based on Laplace transforms rather than direct time integrations in order to improve the accuracy of the results and save on extensive computational time and storage. The time dependent displacement fields in the transverse direction for the cross ply and angle ply laminates are calculated and the stacking sequence effects of the laminates are discussed in detail. Creep responses for the plates with or without a circular hole are also studied. The numerical results compare favorably with analytical solutions, i.e. within 1.8 percent for bending and 10(exp -3) 3 percent for tension. The tension results of the present method are compared with those using the direct time integration scheme.

Hilton, Harry H.↗
DOE OSTI2020

Soft sample deformation, damage and induced electromechanical property changes in contact- and tapping-mode atomic force microscopy

Probe-induced soft sample damage in atomic force microscopy (AFM), as well as the resulting alteration of local mechanical and electrical properties of the material are explored, specifically comparing contact-mode and intermittent-contact-mode imaging methods. In our experiments, performed on conductive polymer films, induced changes are present in contact-mode imaging while they are negligible or absent in tapping-mode imaging. Here, to understand this result, a viscoelastic parameter extraction is performed, which suggests that permanent sample deformation can readily occur for tip-sample interactions with a duration on the timescale of contact-mode interactions. Using the extracted viscoelastic parameters, a dynamic AFM simulation is conducted, which suggests that the material responds more elastically with reduced or absent sample damage in tapping-mode AFM, due to the higher rate of mechanical deformation and shorter timescales.

42 ENGINEERING↗
NASA NTRS1982

Dynamic response of lined tunnels by boundary elements

The dynamic stress concentration manifested around a lined cylindrical tunnel buried in an infinitely extending linear elastic or viscoelastic medium due to the passage of transient disturbances was investigated. Plane strain is assumed to hold and the transient disturbances can be of any arbitrary time variation. The boundary element method formulated in the Laplace transform domain is employed. Isoparametric boundary elements are used in the discretization of the liner and tunnel surfaces. Viscoelastic material behavior can be readily obtained from the linear elastic case in the Laplace transform domain through the use of the correspondence principle. The transient solution is recovered by numerical inversion of the solution obtained in the transformed domain.

Manolis, G. D.↗
DOE OSTI2020

Modular Linear Thermoviscoelastic Model

Time-dependent, viscoelastic responses of materials like polymers and glasses have long been studied. As such, a variety of models have been put forth to describe the behavior including simple rheological models (e.g. Maxwell, Kelvin), linear "fading memory" theories, and hereditary integral based linear thermal viscoelastic approaches as well as more recent nonlinear theories that are either integral, fictive temperature, or differential internal state variable based. The current work details a new LINEAR_THERMOVISCOELASTIC model that has been added to LAME. This formulation represents a viscoelastic theory that neglects some of the phenomenological details of the PEC/SPEC models in favor of efficiency and simplicity. Furthermore, this new model is a first step towards developing "modular" viscoelastic capabilities akin to those available with hardening descriptions for plasticity models in LAME. Specifically, multiple different (including user-defined) shift-factor forms are implemented with each being easily selected via parameter specification rather than requiring distinct material models.

36 MATERIALS SCIENCE↗
NASA NTRS1985

Durability predictions of adhesively bonded composite structures using accelerated characterization methods

The utilization of adhesive bonding for composite structures is briefly assessed. The need for a method to determine damage initiation and propagation for such joints is outlined. Methods currently in use to analyze both adhesive joints and fiber reinforced plastics is mentioned and it is indicated that all methods require the input of the mechanical properties of the polymeric adhesive and composite matrix material. The mechanical properties of polymers are indicated to be viscoelastic and sensitive to environmental effects. A method to analytically characterize environmentally dependent linear and nonlinear viscoelastic properties is given. It is indicated that the methodology can be used to extrapolate short term data to long term design lifetimes. That is, the method can be used for long term durability predictions. Experimental results for near adhesive resins, polymers used as composite matrices and unidirectional composite laminates is given. The data is fitted well with the analytical durability methodology. Finally, suggestions are outlined for the development of an analytical methodology for the durability predictions of adhesively bonded composite structures.

Brinson, H. F.↗
DOE OSTI2020

Long-Range Lamellar Alignment in Diblock Bottlebrush Copolymers via Controlled Oscillatory Shear

A simple strategy is presented to achieve well-ordered nanostructures in microphase-separated diblock bottlebrush copolymers (dbBB) for potential opportunities in nanotechnology that require large grain sizes and directed orientation. The unique architecture and relaxation processes of dbBBs offer a pathway to enhanced dynamic ordering and reorientation over macroscopic scales. Here, controlled shear is used to align lamellar domains. The high molecular mobility of dbBBs in the melt state, as shown by linear and nonlinear viscoelastic characterization, supports this alignment process. When subjected to large-amplitude oscillatory shear at controlled frequency (ω), strain amplitude (γ), and temperature (T shear ), microphase-separated lamellae transition into highly aligned states as determined by small-angle X-ray scattering (SAXS) and transmission electron microscopy (TEM). High throughput synchrotron SAXS is used to rapidly characterize microphase separation and lamellar alignment across the entire bulk sample. Lamellae align parallel to shear planes with an orientation order parameter (S) approaching S = 0.8 over a large cubic volume (V ~ mm 3 ).

36 MATERIALS SCIENCE↗
NASA NTRS1985

Constraints on the rheological structure of the mantle

Rheological models of the mantle are at present limited to radial symmetry, usually with homogeneous linearly viscous or viscoelastic incompressible layers. While such models are probably overly simple, they readily allow calculation of geophysical effects, such as post glacial rebound and related changes in the Earth's shape. They are also directly applicable to problems of global mantle flow and plate motions.

Oconnell, R. J.↗
DOE OSTI2024

Stress-controlled medium-amplitude oscillatory shear (MAOStress) of PVA–Borax

We report the first-ever complete measurement of MAOStress material functions, which reveal that stress can be more fundamental than strain or strain rate for understanding linearity limits as a function of Deborah number. The material used is a canonical viscoelastic liquid with a single dominant relaxation time: polyvinyl alcohol (PVA) polymer solution cross-linked with tetrahydroborate (Borax) solution. We outline experimental limit lines and their dependence on geometry and test conditions. These MAOStress measurements enable us to observe the frequency dependence of the weakly nonlinear deviation as a function of stress amplitude. The observed features of MAOStress material functions are distinctly simpler than MAOStrain, where the frequency dependence is much more dramatic. The strain-stiffening transient network model was used to derive a model-informed normalization of the nonlinear material functions that accounts for their scaling with linear material properties. Moreover, we compare the frequency dependence of the critical stress, strain, and strain-rate for the linearity limit, which are rigorously computed from the MAOStress and MAOStrain material functions. While critical strain and strain-rate change by orders of magnitude throughout the Deborah number range, critical stress changes by a factor of about 2, showing that stress is a more fundamental measure of nonlinearity strength. This work extends the experimental accessibility of the weakly nonlinear regime to stress-controlled instruments and deformations, which reveal material physics beyond linear viscoelasticity but at conditions that are accessible to theory and detailed simulation.

Mechanics↗
DOE OSTI2021

Evaluation of Two-Dimensional to One-Dimensional Site Response for Idaho National Laboratory

We perform two-dimensional (2D) site response analyses accounting for spatial variability of soil properties and subsurface geometry of the Eastern Snake River Plane (ESRP), and quantify their effects on ground surface motion relative to one-dimensional (1D) site response analyses at the Idaho National Laboratory (INL). We first present the development of random field idealizations of the repeated basalt lava flows, heterogeneously inter-layered with sediments, from seismic velocity data collected over four decades in the ESRP. Using realizations of the stochastic fields mapped on 2D deterministic finite element models, we perform 2D viscoelastic and equivalent-linear wave propagation simulations, and quantify the mean and variance of site response aggravation factors, defined as the response spectral ratio of 2D to 1D analyses on the ground surface. Results are shown to be insensitive to the constitutive material behavior considered here, for strains induced by rock outcrop peak ground acceleration (PGA) as high as 0.7g: viscoelastic and equivalent-linear analyses predict peak mean 2D/1D aggravation factor 1.05 at period T=0.075 sec (i.e. the 2D response spectrum is 5% higher than the corresponding 1D at that period, on average), which corresponds to the wavelength of the horizontal correlation length of the random field (50m). For periods longer than the fundamental period of the site (here, T 1 =0.3125 sec), the propagating wavelengths are too long to be affected by the 1D site response and the aggravation factor becomes equal to 1. The standard deviation of the natural logarithms of the 2D/1D aggravation factors is ~0.15 for periods shorter than the fundamental period of the site, and decays thereafter at a steady rate.

58 GEOSCIENCES↗