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The operating principles of a new kind of room-temperature thermal radiation detector are described. In this device modulated light heats a gas, either directly or by conduction from a thin absorbing membrane, and the resultant change in density of the gas is detected by optical heterodyning. The performance of a membrane device of this kind agrees well with the predictions of theory.
Full-density Si3N4-SiO2-Ce2O3 compositions were prepared by sintering with 2.5 MPa nitrogen pressure at temperatures of 1900 and 2090 C. Room-temperature flexural strengths near 700 MPa for sintered material compared favorably with the strength of hot-pressed material. At 1370 C, where flexural strengths as high as 363 MPa were obtained, it was observed that the coarsest structure was the strongest and the finest structure was the weakest. One of the compositions tested, Si3N4-8.7 wt pct SiO2-8.3 wt pct-Ce2O3, was found to have excellent 200-h oxidation resistance at 700, 1000, and 1370 C, without incidence of 700 to 1000 C phase instability and cracking.
Twenty-four different epoxy resin systems were evaluated by a variety of test techniques to identify materials that exhibited improved impact damage tolerance in graphite/epoxy composite laminates. Forty-eight-ply composite panels of five of the material systems were able to sustain 100 m/s impact by a 1.27-cm-diameter aluminum projectile while statically loaded to strains of 0.005. Of the five materials with the highest tolerance to impact, two had elastomeric additives, two had thermoplastic additives, and one had a vinyl modifier; all the five systems used bisphenol A as the base resin. An evaluation of test results shows that the laminate damage tolerance is largely determined by the resin tensile properties, and that improvements in laminate damage tolerance are not necessarily made at the expense of room-temperature mechanical properties. The results also suggest that a resin volume fraction of 40 percent or greater may be required to permit the plastic flow between fibers necessary for improved damage tolerance.
Rate coefficients for several two- and three-body ion-molecule reactions involving hydrocarbons have been determined at thermal energies and above using drift tube-mass spectrometer techniques. The measured rates for clustering and breakup reactions involving CH5(+) and C2H5(+) ions in methane are found to be strongly temperature dependent in the range from 80 to 240 K. The equilibrium constants determined for these reactions differ somewhat from those of Hiraoka and Kebarle (1975). Rate coefficients for two-body reactions of CH5(+), C2H5(+), N(+), H(+), and D(+) ions with methane and/or ethane have been measured. The results indicate that the product yields of several of the fast ion-molecule reactions depend strongly on ion energy (temperature), and therefore previous room-temperature results may be of limited value for model calculations of Titan's atmosphere.
Uniformity of thermal expansion has been measured for fused quartz and borosilicate glass. The variation of expansion coefficient for three melts of TO8E was 5 x 10 to the -9th/K over a temperature range of 300 to 100 K and was found to vary linearly with position in the melt. This spatial gradient averaged 3.5 x 10 to the -11th/K-cm. The room-temperature thermal expansivity variation of Duran (Tempax) glass was about 27 x 10 to the -9th/K, while that of E6 glass was about 52 x 10 to the -9th/K.
Enhanced electron trapping has been observed in n-channels of rad-hard CMOS devices due to electron and gamma-ray irradiation. Room-temperature annealing results in a positive shift in the threshold potential far beyond its initial value. The slope of the annealing curve immediately after irradiation was found to depend strongly on the gate bias applied during irradiation. Some dependence was also observed on the electron dose rate. No clear dependence on energy and shielding over a delidded device was observed. The threshold shift is probably due to electron trapping at the radiation-induced interface states and tunneling of electrons through the oxide-silicon energy barrier to fill the radiation-induced electron traps. A mathematical analysis, based on two parallel annealing kinetics, hole annealing and electron trapping, is applied to the data for various electron dose rates.
Theoretical work of two decades ago adequately explained the transport behavior and effectively guided the development of thermoelectric materials of high conversion efficiencies of conventional semiconductors (e.g., SiGe alloys). The more significant contributions involved the estimaiation of optimum doping concentrations, the reduction of thermal conductivity by solid solution doping and the development of a variety of materials with ZT approx. 1 in the temperature range 300 K to 1200 K. ZT approx. 1 is not a theoretical limitation although, experimentally, values in excess of one were not achieved. Work has continued with emphasis on higher temperature energy conversion. A number of promising materials have been discovered in which it appears that ZT 1 is realizable. These materials are divided into two classes: (1) the rare-earth chalcogenides which behave as itinerant highly-degenerate n-type semiconductors at room-temperature, and (2) the boron-rich borides, which exhibit p-type small-polaronic hopping conductivity.
An attempt is made to refine the grain structure of equiatomic NiAl by means of rapid solidification processing, and to examine the effect of small grain size on room temperature ductility. Free melt spinning was used to produce the rapidly solidified material. Room temperature bend testing of both as-spun and heat-treated NiAl ribbon was conducted by free bending the ribbon around a mandrel of successively smaller diameter until failure occurred. Room-temperature plastic deformation was exhibited both before and after a 1-h heat treatment at 1000 C. Heat treatment increased the observed ductility.
A relatively simple room-temperature preamp design that satisfies both the low-noise and wideband requirements for the InSb Putley-mode detector and which is based on a common-drain JFET input, is presented. The design has an input capacitance of 28 pf which is much less than comparably noisy common-source amplifiers. It can be used for preamplification of 0.1 to 10 MHz signals from liquid-helium-cooled radiation detectors.
The use of the resonant Doppler velocimeter for flow visualization in a free supersonic nitrogen jet is demonstrated experimentally. In the experiment reported here, room-temperature nitrogen at 12.7 psi expands through a Mach 3.4 converging diverging nozzle into a plenum chamber; small amount of sodium is injected through a heated needle centered 0.5-in. upstream of the nozzle throat. The beam of a single frequency dye laser is expanded into a sheet of light with a cylindrical beam expander and directed counter to the jet to spatially resolve any slice across the core of the flow. By tuning the laser to different frequencies, particular velocity and density fields can be highlighted.
Pressure regulated and flow timed to control amount dispensed. Dispenser provides measured amount of water for reconstituting dehydrated foods and beverages. Dispenser holds food or beverage package while being filled with either cold or room-temperature water. Other uses might include dispensing of fluids or medicine. Pressure regulator in dispenser reduces varying pressure of water supply to constant pressure. Electronic timer stops flow after predetermined length of time. Timed flow at regulated pressure ensures controlled volume of water dispensed.
Rietveld analyses of room-temperature neutron diffraction data for seven Nd2(Co/x/Fe/1-x/)14B alloys (x = 0,0.1, 0.3, 0.5, 0.7, 0.9, 1) are reported. Throughout the entire composition range the Nd2Fe14B-type tetragonal crystal structure is maintained, with the lattice constants decreasing significantly as the Co concentration x increases. It is found that the J2-type transition-metal sites are preferentially occupied by Fe ions in the pseudoternary systems, a result which is analogous to the preferential Fe occupation of c sites previously observed in hexagonal Nd2(Co/x/Fe/1-x/)17 alloys.
Specimens of a nickel-bonded titanium carbide cermet were given the following surface treatments: (1) grinding, (2) lapping, (3) blast cleaning, (4) acid roughening, (5) oxidizing, and (6) oxidizing and refinishing. Room-temperature modulus-of-rupture and impact strength varied with the different surface treatments. Considerable strength losses resulted from the following treatments: (1) oxidation at 1600 F for 100 hours, (2) acid roughening, and (3) severe grinding with 60-grit silicon carbide abrasive. The strength loss after oxidation was partially recovered by grit blasting or diamond grinding.
A Nusselt-Reynolds number relation for cylindrical thermocouple wires in crossflow was obtained from the experimental determination of time constants. Tests were conducted in exhaust gas over a temperature range of 2000 to 3400 R, a Mach number range of 0.3 to 0.8, and a static-pressure range from 2/3 to 1-1/3 atmospheres, yielding a Reynolds number range of 450 to 3000. The correlation obtained is Nu=(0.428 plus or minus 0.003) times the square root of Re* with average deviations of a single observation of 8.5 percent. This relation is the same as one previously reported for room-temperature conditions.
Effect of three surface finishes of roughness 4 to 5, 20 to 25, and 70 to 80 micro inches rms on fatigue properties were determined for low-carbon N-155 alloy of grain size A.S.T.M. 1 at temperatures of 80 , 1000, 1350, and 1500 F. The fatigue properties for the various finishes differed appreciably at room temperature; however, after short periods at 1000 F and for all periods investigated at temperatures above 1000 F, the specimen finishes had the same fatigue strength. It was concluded that the primary cause of the difference in room-temperature strength was due to compressive stresses set up in the surface and that at elevated temperatures these compressive stresses were relieved by annealing. Apparently, roughness alone did not significantly affect fatigue strength.
Local cooling-air flow rates through the walls of a sintered porous-metal turbine blade were measured at room temperature for a range of pressure drops. In order to check the validity of the correlation procedure, this procedure was used to correlate air-flow rates thorough two porous disks at temperatures up to 600 degrees F.245:00:Experimental investigation of coolant Data indicate the method permits room-temperature flow data to be used for heat-transfer work at elevated temperatures with reasonable accurach. Cooling-air flow distribution around the periphery of the test blade is presented for two internal cooling air pressures with the blade in a 1000 degrees Fahrenheit gas stream at a cascade-inlet Mach number of 0.45.
The outstanding oxidation resistance of molybdenum disilicide at 2400 F and above was found to depend on the formation of a protective siliceous coating which a-cristobalie has been identified. Molybdenum disilicide is not inherently resistant to oxidation and in powdered form burns at low temperatures.Melting and casting experiments have demonstrated the decomposition of the material at the melting point. The room-temperature modulus of elasticity has been determined and electric-resistivity data are given to 2000 F.
Experimental results are presented from crippling tests of stainless-steel sandwich specimens in the temperature range from 80 F to 1,200 F. The specimens included resistance-welded 17-7 PH stainless-steel sandwiches with single-corrugated cores, type 301 stainless-steel sandwiches with double-corrugated cores, and brazed 17-7 PH stainless-steel sandwiches with honeycomb cores. The experimental strengths are compared with predicted buckling and crippling strengths. The crippling strengths were predicted from the calculated maximum strength of the individual plate elements of the sandwiches and from a correlation procedure which gives the elevated-temperature crippling strength when the experimental room-temperature crippling strengths are known. Photographs of some of the tested specimens are included to show the modes of failure.