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At least 127 records · Page 7

Preliminary Design of a Galactic Cosmic Ray Shielding Materials Testbed for the International Space Station

The preliminary design of a testbed to evaluate the effectiveness of galactic cosmic ray (GCR) shielding materials, the MISSE Radiation Shielding Testbed (MRSMAT) is presented. The intent is to mount the testbed on the Materials International Space Station Experiment-X (MISSE-X) which is to be mounted on the International Space Station (ISS) in 2016. A key feature is the ability to simultaneously test nine samples, including standards, which are 5.25 cm thick. This thickness will enable most samples to have an areal density greater than 5 g/sq cm. It features a novel and compact GCR telescope which will be able to distinguish which cosmic rays have penetrated which shielding material, and will be able to evaluate the dose transmitted through the shield. The testbed could play a pivotal role in the development and qualification of new cosmic ray shielding technologies.

Gaier, James R.↗

Characterization of multilayer GaAs/AlGaAs transistor structures by variable angle spectroscopic ellipsometry

Variable angle of incidence spectroscopic ellipsometry (VASE) has been implemented as a means of determining layer thickness, alloy composition, and growth quality of GaAs/AlGaAs samples composed of relatively thick layers as well as superlattices. The structures studied in this work contained GaAs/AlGaAs multilayers with a superlattice 'barrier' and were grown for later formation of modulation-doped field effect transistors (MODFETs). Sample modeling was performed by treating the superlattice as a bulk AlGaAs layer of unknown composition. Extremely good data fits were realized when five layer thicknesses and two alloy ratios were allowed to vary in a regression analysis. Room temperature excitonic effects associated with the e-hh(1), e-lh(1) and e-hh(2) transitions were observed in the VASE data.

Merkel, Kenneth G.↗

Transmission measurement based on STM observation to detect the penetration depth of low-energy heavy ions in botanic samples

The penetration depth of low-energy heavy ions in botanic samples was detected with a new transmission measurement. In the measurement, highly oriented pyrolytic graphite (HOPG) pieces were placed behind the botanic samples with certain thickness. During the irradiation of heavy ions with energy of tens of keV, the energetic particles transmitted from those samples were received by the HOPG pieces. After irradiation, scanning tunneling microscope (STM) was applied to observe protrusion-like damage induced by these transmitted ions on the surface of the HOPG. The statistical average number density of protrusions and the minimum transmission rate of the low-energy heavy ions can be obtained. The detection efficiency of the new method for low-energy heavy ions was about 0.1-1 and the background in the measurement can be reduced to as low as 1.0 x 10(8) protrusions/cm2. With this method, the penetration depth of the energetic particles was detected to be no less than 60 micrometers in kidney bean slices when the slices were irradiated by 100 keVAr+ ion at the fluence of 5 x 10(16) ions/cm2. c2002 Elsevier Science Ltd. All rights reserved.

DNA Damage↗

Test Report: Direct and Indirect Lightning Effects on Composite Materials

Lightning tests were performed on composite materials as a part of an investigation of electromagnetic effects on the materials. Samples were subjected to direct and remote simulated lightning strikes. Samples included various thicknesses of graphite filament reinforced plastic (GFRP), material enhanced by expanded aluminum foil layers, and material with an aluminum honeycomb core. Shielding properties of the material and damage to the sample surfaces and joints were investigated. Adding expanded aluminum foil layers and increasing the thickness of GFRP improves the shielding effectiveness against lightning induced fields and the ability to withstand lightning strikes. A report describing the lightning strike tests performed by the U.S. Army Redstone Technical Test Center, Redstone Arsenal, AL, STERT-TE-E-EM, is included as an appendix.

Composite materials↗

Modeling of electrically thick materials theoretical and experimental aspects

The shielding effectiveness of modern aircraft depends upon the nature and the electromagnetic properties of the materials used. It was shown that thin materials are modeled well by a sheet surface impedance. Unfortunately, this formalism fails in the high frequency domain (when skin effect occurs) and when the materials are physically thick. The purpose is to propose a general formalism that renders the skin effect and can be used with multilayered samples. These electrically thick materials are studied using symmetrical boundary conditions applied to tangential fields. The domain of validity of the method is discussed and experimental validations are presented.

Gobin, V.↗

Air Flow and Pressure Drop Measurements Across Porous Oxides

This report summarizes the results of air flow tests across eight porous, open cell ceramic oxide samples. During ceramic specimen processing, the porosity was formed using the sacrificial template technique, with two different sizes of polystyrene beads used for the template. The samples were initially supplied with thicknesses ranging from 0.14 to 0.20 in. (0.35 to 0.50 cm) and nonuniform backside morphology (some areas dense, some porous). Samples were therefore ground to a thickness of 0.12 to 0.14 in. (0.30 to 0.35 cm) using dry 120 grit SiC paper. Pressure drop versus air flow is reported. Comparisons of samples with thickness variations are made, as are pressure drop estimates. As the density of the ceramic material increases the maximum corrected flow decreases rapidly. Future sample sets should be supplied with samples of similar thickness and having uniform surface morphology. This would allow a more consistent determination of air flow versus processing parameters and the resulting porosity size and distribution.

Fox, Dennis S.↗

Non-Equilibrium Superconductivity and Magnetic Pair Breaking in Perovskite Half-Metallic Ferromagnet-Insulator-Superconductor (F-I-S) Heterostructures

The effect of spin-polarized quasiparticle currents on the critical current density (J-c) of cuprate superconductors is studied in perovskite F-I-S heterostructures as a function of insulator thickness and of underlying magnetic materials. A pulsed current technique is employed to minimize extraneous Joule heating on the superconductor. At temperatures near T-c, F-I-S samples with insulator thicknesses\1e2nm show precipitous decrease in J_c as current injection (I_m) is increased. In contrast, J_c in a controlled sample with a substituted non-magnetic material (N-I-S) exhibit no dependence on I_m. Similarly, a F-I-S sample with a 10 mn insulating barrier also show little J_c effect versus I_m. At low temperatures with I_m = 0, significant suppression of J-c is observed only in the thin barrier F-I-S samples, although T_c and the normal-state resistivity of all samples are comparable. These phenomena can be attributed to the Cooper pair breaking induced by externally-injected and internally-reflected spin-polarized quasiparticle currents. We estimate an order of magnitude range for the spin diffusion length of 100 nm to 100\ mum.

Fu, C.-C.↗

Surface characterization of selected LDEF tray clamps

The surface characterization of chromic acid anodized 6061-T6 aluminum alloy tray clamps has shown differences in surface chemistry depending upon the position on the Long Duration Exposure Facility (LDEF). Water contact angle results showed no changes in wettability of the tray clamps. The overall surface topography of the control, trailing edge(E3) and leading edge(D9) samples was similar. The thickness of the aluminum oxide layer for all samples determined by Auger depth profiling was less than one micron. X-ray photoelectron spectroscopy (XPS) analysis of the tray clamps showed significant differences in the surface composition. Carbon and silicon containing compounds were the primary contaminants detected.

Cromer, T. F.↗

Effects on LDEF exposed copper film and bulk

Two forms of copper were exposed to the Long Duration Exposure Facility (LDEF) Mission 1 environment: a copper film initially 74.2 plus or minus 1.1 nm thick sputter coated on a fused silical flat and a bulk piece of oxygen free, high conductivity (OFHC) copper. The optical density of the copper film changed from 1.33 to 0.70 where exposed and the film thickness increased to 106.7 plus or minus 0.5 nm where exposed. The exposed area appears purple by reflection and green by transmission for the thin film and maroon color for the bulk copper piece. The exposed areas increased in thickness, but only increase in the thickness of thin film samples could be readily measured. The increase in film thickness is consistent with the density changes occurring during conversion of copper to an oxide. However, we have not been able to confirm appreciable conversion to an oxide by x ray diffraction studies. We have not yet subjected the sample to e-beams or more abusive conditions out of concern that the film might be modified.

Peters, Palmer N.↗

LDEF SP-HVDE (Space Plasma-High Voltage Drainage Experiment) post-flight results: Leakage current and discharge

TRW designed and fabricated two identical SP-HVDE trays which were flown in the NASA LDEF (Long Duration Exposure Facility) for 5.75 years in the LEO (low earth orbit) environment. One tray was placed near the leading edge and one near the trailing edge, and investigations were performed to compare the environmental interactions on the dielectric samples of the two trays. Each tray consisted of six assemblies with Kapton dielectric samples of varying thicknesses (i.e., 2 mils, 3 mil, and 5 mils) biased under +/- 300 V, +/- 500 V, and +/- 1000 V. The original objective was successfully achieved by measuring the first in-flight average leakage current through the samples. Less than 5 percent of the post-flight coulometers behaved anomalously. The data should be valuable to the design and evaluation of spacecraft with high voltage systems. M/D (micrometeoroid and debris) impacts over the dielectric samples were examined using a SEM (Scanning Electron Microscope) and an EDS (Energy Dispersive x-ray Spectrometer). These impact sites were sprayed by silver which were most likely caused either by the impact or a 'local ESD' (electrostatic discharge).

Yaung, J. Y.↗

Preliminary Results of the Third Test Series of Nonmetal Material Flammability Evaluation In SKOROST Apparatus on the Space Station Mir

The work has been done according to the US/Russian Joint Project "Experimental Evaluation of the Material Flammability in Microgravity" a continued combustion study in the SKOROST test apparatus on the OS Mir. The objective of the project was to evaluate the flammability and flame-spread rate for the selected polymer materials in low velocity flow in microgravity. Lately, the issue of nonmetal material combustion in microgravity has become of great importance, based on the necessity to develop the fire safety system for the new International Space Station (ISS). Lack of buoyant flow in microgravity reduces oxygen transfer into the combustion zone, which leads to flame extinction when the flow velocity is less than the limiting flow velocity V(sub lim) for the material. The ISS FGB fire-safety system was developed based on this phenomenon. The existence of minimum flow velocity V(sub lim) to sustain fire for the selected materials was determined both theoretically and experimentally. In the latter, it is shown that, even for thermally thin nonmetal materials with a very low oxygen index C(sub lim) of 12.5% (paper sheets with the thickness of 0.1 mm), a limiting flow velocity V(sub lim) exists at oxygen concentration Co(sub OX) = 17-21%, and is about 1.0 - 0.1 cm/sec. This might be explained by the relative increase in thermal losses due to radiation from the surface and from the gaseous phase. In the second series of experiments in Skorost apparatus on Orbital Station Mir the existence of the limiting flow velocity V(sub lim) for combustion was confirmed for PMMA and glass-epoxy composite strip samples 2 mm thick at oxygen concentration C(sub OX) = 21.5%. It was concluded that V(sub lim) depends on C(sub OX) for the PMMA sample with a low oxygen index of 15.5%, the limiting flow velocity V(sub lim) was less than 0.5 cm/sec, and for the glass-epoxy composite sample with a high oxygen index of 19%, the limiting flow velocity V(sub lim) was higher than 15 cm/sec. As of now only those materials that maintain their integrity during combustion were investigated. The materials that disintegrate when burning present more danger for fire safety because the flame can spread farther with the parts of the structure, ejected melt drops, et cetera. Materials such as polyethylene are of great interest since they form a lengthy melt zone during the combustion in normal gravity. This melt zone generates drops of liquids that promote faster flame spread compared to usual combustion. The preliminary results of polyethylene insulation flammability evaluation in microgravity are shown in the NASA Wire Insulation Flammability (WIF) experiment during Space Shuttle flight STS-50. A lot of interesting data was collected during the WIF test program. However, one of the most important results was that, in microgravity, the extinction of the polyethylene occurred almost immediately when the flow of relatively low oxygen concentration (C(sub OX)=21%) was stopped. The purpose of the work reported here is to expand the existing data base on material flammability in microgravity and to conduct the third series of the space experiment using Skorost apparatus on Orbiatl Station Mir with melting polymers, which might increase the probability of fire and its propagation in ventilated microgravity environment of orbiting spacecraft.

Ivanov, A. V.↗

Superconductivity devices: Commercial use of space

A YBCO thick film containing 20 percent Ag2O with a T(sub c) of 86.8 K and J(sub c) of 108 A/sq cm was obtained. The film was fabricated by a two-step firing process, i.e., firing the film at 1000 C for 10 minutes and annealing at 970 C for 30 minutes. The two-step firing process, however, was not suitable for the multiple-lead YBCO sample due to the formation of the 211 green phase at 1000 C in the multiple-lead YBCO sample. A BSCCO thick film printed on a MgO coated MSZ substrate and fired at 845 C for 2 hours exhibited a superconducting behavior at 89 K. Because of its porous microstructure, the critical current density of the BSCCO thick film was limited. This report also includes the results of the YBCO and BSCCO materials used as oxide electrodes for ferroelectric materials. The YBCO electroded PLZT showed higher remanent polarization and coercive field than the sample electroded with silver paste. A higher Curie temperature for the PLZT was obtained from the YBCO electroded sample. The BSCCO electroded sample, however, exhibited the same Curie temperature as that of a silver electroded sample. Dissipation factors of the ferroelectric samples increased when the oxide electrode was applied.

Haertling, Gene↗

Flamelet Formation In Hele-Shaw Flow

A Hele-Shaw flow apparatus constructed at Michigan State University (MSU) produces conditions that reduce influences of buoyancy-driven flows. In addition, in the MSU Hele-Shaw apparatus it is possible to adjust the heat losses from the fuel sample (0.001 in. thick cellulose) and the flow speed of the approaching oxidizer flow (air) so that the "flamelet regime of flame spread" is entered. In this regime various features of the flame-to-smolder (and vice versa) transition can be studied. For the relatively wide (approx. 17.5 cm) and long (approx. 20 cm) samples used, approximately ten flamelets existed at all times. The flamelet behavior was studied mechanistically and statistically. A heat transfer analysis of the dominant heat transfer mechanisms was conducted. Results indicate that radiation and conduction processes are important, and that a simple 1-D model using the Broido-Shafizadeh model for cellulose decomposition chemistry can describe aspects of the flamelet spread process. Introduction

Wichman, I. S.↗

Cooling Rate Study of Nickel-Rich Material During Thermal Treatment and Quench

To investigate quench cracking that results from water quenching after heat treatment of binary and Ni-rich material, cooling rates of specimens were measured during quenching and hardness post-thermal treatment. For specific applications binary Ni-Ti is customarily thermally treated and quenched to attain desired mechanical properties and hardness. However, one problem emerging from this method is thermal cracking, either during the heat treatment process or during the specimen's application. This can result in material and equipment failure as well as financial losses. The objective of the study is to investigate the internal cooling rate of 60-NiTi during quenching and determine possible factors causing thermal cracking. Cubic (1 in.3) samples of both material were heat treated in air at 1000 deg C for 2 hrs and quenched in room temperature water using two methods: (1) dropped in the water and (2) agitated in the water. Hardness of the two fore-mentioned methods was measured post heat treatment. Results indicate that the quenching method had an effect on cooling rate during quenching but hardness was observed to be essentially the same through the thickness of the samples.

Thermal Crack↗

Development of a Composite Material Aerodynamic Demise Model for the Object Reentry Survival Analysis Tool (ORSAT)

The reentry demise of fiber-reinforced polymer (FRP) composites is an increasing concern for modern spacecraft at end of life. Unlike traditional materials such as metals, shredding of the material by aerodynamic forces appears to be a major component of the reentry demise mechanism. This paper will describe a new mechanical, strength-based, material demise model for the Object Reentry Survival Analysis Tool (ORSAT) Version 7.1. The model is based on laboratory in-situ and residual strength tests of several FRP materials performed during the NASA Orbital Debris Program Office’s Phase II Composite Material Demise test campaign. To test the residual strength of partially charred FRP materials, the authors tested 107 rectangular shaped samples of different thicknesses that were previously exposed to high-enthalpy flow at the University of Texas at Austin’s Inductively Coupled Plasma Torch facility. Tests were performed under normal atmospheric conditions at NASA Johnson Space Center’s Experimental Impact Laboratory using a Chatillon TCD1000 tensile test machine configured with a three-point bending jig. Mean fracture load, residual strength, delamination, and flexural modulus were measured for each test. An engineering model of aeromechanical demise for each material was developed by correlating the measured residual strength of the samples with the duration and magnitude of the applied heat flux and the mass loss and char progression. This model has been implemented in ORSAT 7.1 for the built-in, charring carbon fiber/epoxy and charring glass fiber/epoxy material models. The new model was verified by calculating the demise of hundreds of FRP composite fragments of various shapes and sizes and checking the calculations for consistency, with specific focus on material characterization in one-dimension. Further tests are planned in hypersonic flow facilities to validate the assumptions used in the model.

Priscilla A. Mendoza↗

Development of a Composite Material Aerodynamic Demise Model for the Object Reentry Survival Analysis Tool (ORSAT)

The reentry demise of fiber-reinforced polymer (FRP) composites is an increasing concern for modern spacecraft at end of life. Unlike traditional materials such as metals, shredding of the material by aerodynamic forces appears to be a major component of the reentry demise mechanism. This paper will describe a new mechanical, strength-based, material demise model for the Object Reentry Survival Analysis Tool (ORSAT) Version 7.1. The model is based on laboratory in-situ and residual strength tests of several FRP materials performed during the NASA Orbital Debris Program Office’s Phase II Composite Material Demise test campaign. To test the residual strength of partially charred FRP materials, the authors tested 107 rectangular shaped samples of different thicknesses that were previously exposed to high-enthalpy flow at the University of Texas at Austin’s Inductively Coupled Plasma Torch facility. Tests were performed under normal atmospheric conditions at NASA Johnson Space Center’s Experimental Impact Laboratory using a Chatillon TCD1000 tensile test machine configured with a three-point bending jig. Mean fracture load, residual strength, delamination, and flexural modulus were measured for each test. An engineering model of aeromechanical demise for each material was developed by correlating the measured residual strength of the samples with the duration and magnitude of the applied heat flux and the mass loss and char progression. This model has been implemented in ORSAT 7.1 for the built-in, charring carbon fiber/epoxy and charring glass fiber/epoxy material models. The new model was verified by calculating the demise of hundreds of FRP composite fragments of various shapes and sizes and checking the calculations for consistency, with specific focus on material characterization in one-dimension. Further tests are planned in hypersonic flow facilities to validate the assumptions used in the model.

Priscilla A. Mendoza↗

Sample Polishing Without Epoxy

In recent years, we have received requests for meteorite sample sections to be prepared without using epoxy impregnation or mounting. The reasoning for these requests ranges from potential contamination of analyses from epoxy chemical components to degradation of instrumental vacuum from epoxy outgassing (e.g., SEM, SIMS, EPMA, etc.). An alternative approach that we employ involves sawing off a 1-5 mm thick wafer of the sample. The wafer is ground using silica carbide lapping media wetted with 190 proof ethyl alcohol to make both sides flat and parallel. The sample is then polished on one or both sides using diamond paste or dry diamond powder on a rotating lap wheel until the desired finish is obtained. The sample is cleaned in between steps using 200 proof ethyl alcohol in an ultrasonic cleaner. Friable and altered samples need to have higher thickness in order for polishing to be attempted. Without epoxy to hold the sample together or a glass slide for backing, the sample needs additional material to provide the necessary support structure. The machining steps of this process need to be undertaken at a much slower speed than in traditional thin or thick section preparation.

Meteorite↗

Scale Dependence of Cirrus Horizontal Heterogeneity Effects on TOA Measurements: MODIS Brightness Temperatures in the Thermal Infrared - Part I

This paper presents a study on the impact of cirrus cloud heterogeneities on MODIS simulated thermal infrared (TIR) brightness temperatures (BTs) at the top of the atmosphere (TOA) as a function of spatial resolution from 50 meters to 10 kilometers. A realistic 3-D (three-dimensional) cirrus field is generated by the 3DCLOUD model (average optical thickness of 1.4, cloudtop and base altitudes at 10 and 12 kilometers, respectively, consisting of aggregate column crystals of D (sub eff) equals 20 microns), and 3-D thermal infrared radiative transfer (RT) is simulated with the 3DMCPOL (3-D Monte Carlo Polarized) code. According to previous studies, differences between 3-D BT computed from a heterogenous pixel and 1-D (one-dimensional) RT computed from a homogeneous pixel are considered dependent at nadir on two effects: (i) the optical thickness horizontal heterogeneity leading to the plane-parallel homogeneous bias (PPHB); and the (ii) horizontal radiative transport (HRT) leading to the independent pixel approximation error (IPAE). A single but realistic cirrus case is simulated and, as expected, the PPHB mainly impacts the low-spatial resolution results (above approximately 250 meters), with averaged values of up to 5-7 K (thousand), while the IPAE mainly impacts the high-spatial resolution results (below approximately 250 meters) with average values of up to 1-2 K (thousand). A sensitivity study has been performed in order to extend these results to various cirrus optical thicknesses and heterogeneities by sampling the cirrus in several ranges of parameters. For four optical thickness classes and four optical heterogeneity classes, we have found that, for nadir observations, the spatial resolution at which the combination of PPHB and HRT effects is the smallest, falls between 100 and 250 meters. These spatial resolutions thus appear to be the best choice to retrieve cirrus optical properties with the smallest cloud heterogeneity-related total bias in the thermal infrared. For off-nadir observations, the average total effect is increased and the minimum is shifted to coarser spatial resolutions.

TOA↗