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The Genesis Non-flight Implant Sample Archive

Introduction: For the past 20 years the Genesis science community has been analyzing solar wind captured in sample collectors now curated at Johnson Space Center (JSC). Non-flown flight like collector materials (non-flight) considered reference material was always allocated by the JSC Genesis team for testing experimental procedures. However, to expedite Genesis science, distribution of non-flown reference materials were also provided by, D. S. Burnett (Genesis PI, Caltech) and A. J. G. Jurewicz (ASU) who were funded to aid all Genesis PIs by providing engineering test materials archived at Caltech pre-flight as well as ion implants into these materials [1]. Implanted materials (non-flight reference, flight-like semiconductor materials, and NIST SRM glass) received from the Caltech collection during a pilot project are being used to develop an accession procedure for the purpose of making these materials available to researchers in the future. These implant samples are important because they can be utilized as measurement standards [2]. This is a work in progress and this work reports progress in documentation and imaging. The pilot program received 63 implanted reference materials with known implanted ions. Genesis Non-Flight Database: The existing non-flight material database was modified to allow for the description of implant sessions and to allow correlation of the implant information to individual specimens. An implant session has three main components: a known ion, a known dose (ion/cm2), and a known energy (keV). Procedure: Laboratory Procedure. Upon receiving non-flight analytical standards (independently calibrated implants), or implant samples (nominally calibrated implants), they will be imaged in their current containers to capture any information written before being brought into the Genesis Sample Laboratory. Documentation is provided by the donor and used for correlating the data between the implant sessions and implant samples. This information is not verified by Genesis Curation. The microscope used to image samples in the laboratory has an automated stage with a stainless-steel plate to hold samples and a camera that utilizes the software Surveyor to take photomosaic images of the implant samples. The camera attached to the microscope is a QICAM High Performance IEEE 1394 FireWire Digital CCD Camera. This setup, shown in Fig. 1, allows for photomosaics of small-scale samples with a 10x objective or 25x objective. Examples of images taken with this microscope setup are shown in Fig.2 and Fig. 3. After imaging, samples get stored in a clean fluoroware container or polypropylene vial depending on sample size for long term storage. Database Procedure. The Genesis Non-Flight Database currently allows for the addition of implant sessions. The required fields for adding an implant session are the implant session ion, the implant session dose, and the implant session energy. There are also fields for the date and vendor of the sessions as well as a field for if the session was calibrated or not. Once an implant session has been inserted into the database, additional documentation from the session can be attached. The database will automatically assign an Implant Session Number. After inserting an implant session, the implanted samples can be inserted. The fields required for an implant sample are the material of the sample and the size of the sample. The Generic name for the implant sample with be automatically generated by the database once it has been inserted. Implant sample numbers begin with 3X to distinguish from flown Genesis sample numbers. There are also fields for processors to add the location (room, cabinet, tray) and container type (fluoroware, polypropylene vial). Once an implant session and an associated sample(s) have been inserted into the database the sample can be then tied to all associated implant sessions. An implant sample can be tied to multiple implant sessions. Future work: For curation, future work consists of creating an online catalogue for implant samples as well as updating the database with more samples as we receive them. For the scientific community these implant samples have many potential uses. For Genesis research, they are directly applicable for testing and, in some cases, as analytical standards. For non-Genesis research, implants (especially calibrated implants) could be used for calibrating other, unique planetary materials [1].

C D Calva↗

Identifying Solar Wind and Other Volatiles in Space-Weathered Samples From Asteroid Bennu

On September 24, 2023, NASA’s Origins, Spectral Interpretation, Resource Identification, and Security–Regolith Explorer (OSIRIS-REx) mission returned >70 g of material from asteroid Bennu to Earth. The Sample Return Capsule was opened at NASA Johnson Space Center (JSC), and a spillover sample was collected from the avionics deck to perform quick-look (QL) analyses. In addition to providing a reconnaissance investigation of its mineralogy, the sample was also examined for evidence of surface exposure on asteroid Bennu by identifying signatures of space weathering. Space weathering changes the morphology, microstructure, and chemistry of regolith on the surfaces of airless bodies. Driven by micrometeoroid bombardment and solar wind irradiation, our understanding of how space weathering modifies particles on the surfaces of carbonaceous asteroids is still developing. To bolster the interpretation of remote sensing data and to further address driving Hypothesis 10, we must investigate the nanoscale structural and chemical changes in returned samples from Bennu to understand how space weathering affects carbonaceous surface materials. Here we explore evidence for solar wind irradiation in QL samples from asteroid Bennu.

M S Thompson↗

Very long baseline IPS observations of the solar wind speed in the fast polar streams

Observations of intensity scintillation (IPS) with two or more spaced antennas have been widely used to measure the solar wind velocity. Such methods are particularly valuable in regions which spacecraft have not yet penetrated, but they are also very useful in improving the spatial temporal sampling of the solar wind, even in regions where spacecraft data are available. The principle of the measurement is to measure the time delay tau(sub d) between the scintillations observed with an antenna baseline b. The velocity estimate is just V = b/tau(sub d). The error in estimation of the time delay delta tau(sub d) is independent of the baseline length, thus the error in the velocity estimate delta V given by delta(V)/V approximately equals to (delta tau(sub d))/tau(sub d) is inversely proportional to tau(sub d) and hence to b. However the use of a long baseline b has a less obvious advantage; it provides a means for separating fast and slow contributions when both are present in the scattering region. Here we will present recent observations made using the large cylinder antenna at Ooty in the Nilgiri Hills of South India, and one of the 45 m dishes of GMRT near Pune in West-Central India. The baseline of 900 km is, by a considerable margin, the longest ever used for IPS and provides excellent velocity resolution. These results compared with the ULYSSES observations and other IPS measurements made closer to the sun with higher frequency instruments such as EISCAT and the VLBA will provide a precise measure of the velocity profile of the fast north-polar stream.

Rao, A. Pramesh↗

Direct Determination of the Space Weathering Rates in Lunar Soils and Itokawa Regolith from Sample Analyses

Space weathering effects on airless bodies result largely from micrometeorite impacts and solar wind interactions. Decades of research have provided insights into space weathering processes and their effects, but a major unanswered question still remains: what is the rate at which these space weathering effects are acquired in lunar and asteroidal regolith materials? To determine the space weathering rate for the formation of rims on lunar anorthite grains, we combine the rim width and type with the exposure ages of the grains, as determined by the accumulation of solar flare particle tracks. From these analyses, we recently showed that space weathering effects in mature lunar soils (both vapor-deposited rims and solar wind amorphized rims) accumulate and attain steady state in 10(sup 6)-10(sup 7) y. Regolith grains from Itokawa also show evidence for space weathering effects, but in these samples, solar wind interactions appear to dominate over impactrelated effects such as vapor-deposition. While in our lunar work, we focused on anorthite, given its high abundance on the lunar surface, for the Itokawa grains, we focused on olivine. We previously studied 3 olivine grains from Itokawa and determined their solar flare track densities and described their solar wind damaged rims]. We also analyzed olivine grains from lunar soils, measured their track densities and rim widths, and used this data along with the Itokawa results to constrain the space weathering rate on Itokawa. We observe that olivine and anorthite have different responses to solar wind irradiation.

Keller, L. P.↗

The Chandra X-Ray Observatory Radiation Environment Model

CRMFLX (Chandra Radiation Model of ion FluX) is an environmental risk mitigation tool for use as a decision aid in planning the operations times for Chandra's Advanced CCD Imaging Spectrometer (ACIS) detector. The accurate prediction of the proton flux environment with energies of 100 - 200 keV is needed in order to protect the ACIS detector against proton degradation. Unfortunately, protons of this energy are abundant in the region of space Chandra must operate, and the on-board Electron, Proton, and Helium Instrument (EPHIN) does not measure proton flux levels of the required energy range. In addition to the concerns arising from the radiation belts, substorm injections of plasma from the magnetotail may increase the protons flux by orders of magnitude in this energy range. The Earth's magnetosphere is a dynamic entity, with the size and location of the magnetopause driven by the highly variable solar wind parameters (number density, velocity, and magnetic field components). Operational times for the telescope must be made weeks in advance, decisions which are complicated by the variability of the environment. CRMFLX is an engineering model developed to address these problems and provides proton flux and fluence statistics for the terrestrial outer magnetosphere, magnetosheath, and solar wind for use in scheduling ACIS operations. CRMFLX implements a number of standard models to predict the bow shock, magnetopause, and plasma sheet boundaries based on the sampling of historical solar wind data sets. Measurements from the GEOTAIL and POLAR spacecraft are used to create the proton flux database. This paper describes the recently released CRMFLX v2 implementation that includes an algorithm that propagates flux from an observation location to other regions of the magnetosphere based on convective ExB and VB-curvature particle drift motions in electric and magnetic fields. This technique has the advantage of more completely filling out the database and makes maximum use of limited data obtained during high Kp periods or in areas of the magnetosphere with poor satellite coverage.

Blackwell, W. C.↗

Catastrophic Impact of Silicon on Silicon: Unraveling the Genesis Impact Using Sample 61881

The Genesis mission collected solar wind and brought it back to Earth in order to provide precise knowledge of solar isotopic and elemental compositions. The ions in the solar wind were stopped in the collectors at depths on the order of 10 to a few hundred nanometers. This shallow implantation layer is critical for scientific analysis of the composition of the solar wind and must be preserved throughout sample handling, cleaning, processing, distribution, preparation and analysis. The current work is motivated by the need to understand the interaction of the Genesis payload with contamination during the crash in the Utah desert. Silicon contamination has been found to be notoriously difficult to remove from silicon samples despite multiple cleanings with multiple techniques. However, the question has been posed, "Does the silicon really need to be removed for large area analyses?." If the recalcitrant silicon contamination is all pure silicon from fractured collectors, only a very tiny fraction of that bulk material will contain solar wind, which could skew the analyses. This could be complicated if the silicon trapped other materials and/or gases as it impacted the surface.

Kuhlman, K. R.↗

Cellulose Acetate Replica Cleaning Study of Genesis Non-Flight Sample 3CZ00327

The Genesis mission collected solar wind and brought it back to Earth in order to provide precise knowledge of solar isotopic and elemental compositions. The ions in the solar wind were stopped in the collectors at depths on the order of 10 to a few hundred nanometers. This shallow implantation layer is critical for scientific analysis of the composition of the solar wind and must be preserved throughout sample handling, cleaning, processing, distribution, preparation and analysis. We are working interactively with the community of scientists analyzing Genesis samples, using our unique laboratory facilities -- and, where needed, our unique cleaning techniques -- to significantly enhance the science return from the Genesis mission. This work is motivated by the need to understand the submicron contamination on the collectors in the Genesis payload as recovered from the crash site in the Utah desert, and -- perhaps more importantly -- how to remove it. That is, we are evaluating the effectiveness of the wet-chemical "cleaning" steps used by various investigators, to enable them to design improved methods of stripping terrestrial contamination from surfaces while still leaving the solar-wind signal intact.

Kuhlman, K. R.↗

Measurements of heavy solar wind and higher energy solar particles during the Apollo 17 mission

The lunar surface cosmic ray experiment, consisting of sets of mica, glass, plastic, and metal foil detectors, was successfully deployed on the Apollo 17 mission. One set of detectors was exposed directly to sunlight and another set was placed in shade. Preliminary scanning of the mica detectors shows the expected registration of heavy solar wind ions in the sample exposed directly to the sun. The initial results indicate a depletion of very-heavy solar wind ions. The effect is probably not real but is caused by scanning inefficiencies. Despite the lack of any pronounced solar activity, energetic heavy particles with energies extending to 1 MeV/nucleon were observed. Equal track densities of approximately 6000 tracks/cm sq 0.5 microns in length were measured in mica samples exposed in both sunlight and shade.

Walker, R. M.↗

Small Particulate Contamination Survey Of Genesis Flight Sample 61423

The Genesis mission collected solar wind and brought it back to Earth in order to provide precise knowledge of solar isotopic and elemental compositions. The ions in the solar wind stop in the collectors at depths on the order of 10 to a few hundred nanometers. This shallow implantation layer is critical for scientific analysis of the composition of the solar wind and must be preserved throughout sample handling, cleaning, processing, distribution, preparation and analysis. We continue to work with the community of scientists analyzing Genesis samples using our unique laboratory facilities -- and, where needed, our unique cleaning techniques -- to significantly enhance the science return from the Genesis mission. This work is motivated by the need to understand the submicron contamination on the collectors in the Genesis payload as recovered from the crash site in the Utah desert, and -- perhaps more importantly -- how to remove it. We continue to evaluate the effectiveness of the wet-chemical "cleaning" steps used by various investigators, to enable them to design improved methods of stripping spacecraft and terrestrial contamination from surfaces while still leaving the solar-wind signal intact.

Kuhlman, K. R.↗

Using Image Pro Plus Software to Develop Particle Mapping on Genesis Solar Wind Collector Surfaces

The continued success of the Genesis mission science team in analyzing solar wind collector array samples is partially based on close collaboration of the JSC curation team with science team members who develop cleaning techniques and those who assess elemental cleanliness at the levels of detection. The goal of this collaboration is to develop a reservoir of solar wind collectors of known cleanliness to be available to investigators. The heart and driving force behind this effort is Genesis mission PI Don Burnett. While JSC contributes characterization, safe clean storage, and benign collector cleaning with ultrapure water (UPW) and UV ozone, Burnett has coordinated more exotic and rigorous cleaning which is contributed by science team members. He also coordinates cleanliness assessment requiring expertise and instruments not available in curation, such as XPS, TRXRF [1,2] and synchrotron TRXRF. JSC participates by optically documenting the particle distributions as cleaning steps progress. Thus, optical document supplements SEM imaging and analysis, and elemental assessment by TRXRF.

Rodriquez, Melissa C.↗

A new predictive model for determining solar wind-terrestrial planet interactions

A computational model has been developed for the determination of the gasdynamic and magnetic field properties of the solar wind flow around a magnetic planet, such as the earth, or a nonmagnetic planet, such as Venus. The procedures are based on an established single-fluid, steady, dissipationless, magnetogasdynamic model and are appropriate for the calculation of axisymmetric, supersonic, super-Alfvenic solar wind flow past a planetary magneto/ionosphere. Sample results are reported for a variety of solar wind and planetary conditions. Some of these are new applications; others are included to show that the new procedures produce the same results as previous procedures when applied to the same conditions. The new methods are completely automated and much more efficient and versatile than those employed heretofore.

Spreiter, J. R.↗

Molecular Substrate Alteration by Solar Wind Radiation Documented on Flown Genesis Mission Array Materials

The Genesis spacecraft sampling arrays were exposed to various regimes of solar wind during flight that included: 313.01 days of high-speed wind from coronal holes, 335.19 days of low-speed inter-stream wind, 191.79 days of coronal mass ejections, and 852.83 days of bulk solar wind at Lagrange 1 orbit. Ellipsometry measurements taken at NASA s Johnson Space Center show that all nine flown array materials from the four Genesis regimes have been altered by solar wind exposure during flight. These measurements show significant changes in the optical constant for all nine ultra-pure materials that flew on Genesis when compared with their non-flight material standard. This change in the optical constant (n and k) of the material suggests that the molecular structure of the all nine ultra-pure materials have been altered by solar radiation. In addition, 50 samples of float-zone and czochralski silicon bulk array ellipsometry results were modeled with an effective medium approximation layer (EMA substrate layer) revealing a solar radiation molecular damage zone depth below the SiO2 native oxide layer ranging from 392 to 613 . This bulk solar wind radiation penetration depth is comparable to the depth of solar wind implantation depth of Mg measured by SIMS and SARISA.

Calaway, Michael J.↗

The abundances of H-3 and C-14 in the solar wind

Tritium is measured as a function of depth in a Surveyor 3 sample. The upper limit for solar-wind-implanted tritium gives a H-3/H-1 limit for the solar wind of 1 part in one hundred billion. The temperature release patterns of C-14 from lunar soils are measured. The C-14 release patterns from surface soils differ from a trench-bottom soil and give evidence for the presence of C-14 in the solar wind with a C-14/H-1 ratio of approximately 4 parts in one hundred billion. The implications of these radionuclide abundances in the solar wind are discussed.

Fireman, E. L.↗

Radial evolution of the high/low frequency breakpoint in magnetic field spectra

The spectra of magnetic field variations in the solar wind show different behavior in two frequency regions; a high frequency region in which the spectral exponent is about -5/3 and a low frequency region in which it is typically -1. The two types of variations must arise from different processes and a clue to the relationship between the spectral regions lies in understanding the behavior of the breakpoint between the spectral regions. Studies of the average behavior of spectra have shown that the break point occurs at about 3.5 hours at 1 AU. It is also known that, on average, the breakpoint occurs at lower frequencies with larger heliocentric distances. Ideally however, instead of the average properties of the spectra, we would like to know how the breakpoint evolves in particular samples of the solar wind as they propagate to larger heliocentric distances. In the study reported here we take advantage of the fact that, in 1974, Pioneer 10 (4.4 AU) and Pioneer 11 (5.6 AU) were close to being co-aligned and being aligned with the Earth. Solar wind observed at Earth can be closely matched with solar wind later observed at P10 and P11. We here compare the breakpoint observed at Earth with that observed at Pioneers 10 and 11 for matched samples of the wind.

Feynman, J.↗

Interplanetary Radiation and Internal Charging Environment Models for Solar Sails

A Solar Sail Radiation Environment (SSRE) model has been developed for characterizing the radiation dose and internal charging environments in the solar wind. The SSRE model defines the 0.01 keV to 1 MeV charged particle environment for use in testing the radiation dose vulnerability of candidate solar sail materials and for use in evaluating the internal charging effects in the interplanetary environment. Solar wind and energetic particle instruments aboard the Ulysses spacecraft provide the particle data used to derive the environments for the high inclination 0.5 AU Solar Polar Imager mission and the 1.0 AU L1 solar sail missions. Ulysses is the only spacecraft to sample high latitude solar wind environments far from the ecliptic plane and is therefore uniquely capable of providing the information necessary for defining radiation environments for the Solar Polar Imager spacecraft. Cold plasma moments are used to derive differential flux spectra based on Kappa distribution functions. Energetic particle flux measurements are used to constrain the high energy, non-thermal tails of the distribution functions providing a comprehensive electron, proton, and helium spectra from less than 0.01 keV to a few MeV.

Minow, Joseph I.↗

Genesis Solar Wind – Capture, Return, Curate and Analyze: Looking Backward Reviewing Sample Collection Hardware

Genesis, as the first U.S. spacecraft to return astromaterial samples since Apollo, not only integrated the mission planning and flight teams, but also the science and sample curation teams during the mission development period. Since Genesis is a sample return mission, the Science Team was essential in certifying the collectors (sample containers for solar atoms). Burnett and the science team defined the purity of collector materials and ability to analyze solar wind composition to the precision required for planetary science. The science team’s choices included a variety of very pure materials which are described, including rationale for selection. The JPL Project Scientist networked with specialty vendors refining specifications and fabricating several of the materials. JPL engineering team designed and fabricated the collector arrays. LANL designed and built an electrostatic concentrator. JSC procured these materials with exacting specifications.

SOLAR WIND↗