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DOE OSTI2022

Microbial Curing of Cement for Energy Applications

Rutgers University, Lawrence Livermore National Laboratory, and the University of Arizona executed this program over 36 months with a 4-Task Program: (M1)-Microbial Engineering (M2)-Microstructure Modelling, (M3) Cement and Concrete Formulation, (M4)-Techno-economic analysis (TEA) and lifecycle assessment (LCA). This program developed a new carbonate cement concrete manufacturing process called microbial curing (MBC). MBC utilizes in-situ microbial production of CO 2 that dissolves into pore-bound water to carbonate a cementitious material creating a bonding matrix of CaCO 3 and SiO 2 that hardens and densifies the material. This is the first work of this type where calcium silicate was used in microbial studies. All other work reported in the literature always used a soluble form of calcium. This final report describes the work done in the final quarter, the best procedures and results, and the final techno-economic and lifecycle analyses. This quarter, we cast and cured twenty-five (4”x8”) cylinder samples. The compressive strength, split tensile, Young’s modulus, chloride permeability, and creep measurements were performed. These measurements demonstrated that MBC of calcium silicate concrete exhibits scaling problems due to the escape of ammonia gas, a product of the microbial reaction to generate CO 2 . As curing proceeds, the ability for the gas to escape from within the cylinder is restricted by the outer cylindrical portions densifying, making the outer portion highly impermeable to gas flow. In contrast, the small samples cured are uniformly cured, forming materials whose mechanical properties are 7x better than the large samples. This problem needs to be solved before this technology can be commercialized. The techno-economic and lifecycle analyses indicate that the technology developed in this program exhibits a significant opportunity to reduce the cost of cement and CO 2 emissions associated with concrete, provided the curing issue associated with larger samples can be addressed.

36 MATERIALS SCIENCE↗

DOE OSTI2025

Ocelot: An Interactive, Efficient Distributed Compression-As-a-Service Platform With Optimized Data Compression Techniques

Large volumes of data generated by scientific simulations, genome sequencing, and other applications need to be moved among clusters for data collection/analysis. Data compression techniques have effectively reduced data storage and transfer costs. However, users' requirements on interactively controlling both data quality and compression ratios are non-trivial to fulfill. Here, we propose a novel Compression-as-a-Service (CaaS) platform called Ocelot with four important contributions: (1) It offers real-time visualization, interactive compression, and transfer of scientific datasets. (2) It incorporates new strategies for compressing diverse types of datasets more effectively than traditional methods. (3) It provides an effective method for estimating the compression ratio and execution time of compression tasks. (4) Experiments on multiple real-world datasets on geographically distributed computers show that Ocelot can significantly improve data transfer efficiency with a performance gain of more than 10x in computing clusters with relatively slow networks.

compression as a service (CaaS)↗

DOE OSTI2020

Advanced Simulation and Experiments of Strongly Coupled Geomechanics and Flow for Gas Hydrate Deposits: Validation and Field Application. Final Report

The objectives of the proposed research are (1) to investigate geomechanical responses induced by depressurization experimentally and numerically; (2) to enhance the current numerical simulation technology in order to simulate complex physically coupled processes by depressurization and (3) to perform in-depth numerical analyses of two selected potential production test sites: one based on the deposits observed at the Ulleung basin UBGH2-6 site; and the other based on well-characterized accumulations from the westend Prudhoe Bay. To these ends, the recipient will have the following specific objectives: 1). Information obtained from multi-scale experiments previously conducted at the recipient’s research partner (the Korean Institute of Geoscience and Mineral Resources (KIGAM)) that were designed to represent the most promising known Ulleung Basin gas hydrate deposit as drilled at site UBGH2-6 will be evaluated (Task 2). These findings will be further tested by new experimental studies at Lawrence Berkeley National Laboratory (LBNL) and Texas A&M (TAMU) (Task 3) that are designed capture complex coupled physical processes between flow and geomechanics, such as sand production, capillarity, and formation of secondary hydrates. The findings of Tasks 2 and 3 will be used to further improve numerical codes. 2) Develop (in Tasks 4 through 6) an advanced coupled geomechanics and non-isothermal flow simulator (T+MAM) to account for large deformation and strong capillarity. This new code will be validated using data from the literature, from previous work by the project team, and with the results of the proposed experimental studies. The developed simulator will be applied to both Ulleung Basin and Prudhoe Bay sites, effectively addressing complex geomechanical and petrophysical changes induced by depressurization (e.g., frost-heave, strong capillarity, cryo-suction, induced fracturing, and dynamic permeability).

02 PETROLEUM↗

DOE OSTI2020

UNESE Data Analysis-Disko Elm Gas Transport Characteristics (NA-22 Quarterly Report)

Recently published papers have demonstrated the impact of sorption mechanisms on gas transport in the subsurface following an underground nuclear explosion. To include sorption processes in the multi-physics models of noble gas production and transport, researchers have conducted experiments of gas sorption in geologic materials and calibrated a linear (Henry’s law) sorption model for all gases in various geologic materials. As a part of Task #4, we requested the experimental data from Sandia Laboratories and derived a dual-mode (Henry’s absorption and Langmuir adsorption) sorption model. The derived model better describes the nonlinear sorption mechanism with much higher fitness with the experimental data. When gas concentrations are relatively low (in the conditions of field experiments or underground nuclear explosions) compared to those used sorption experiments, the nonlinear sorption model can be approximated as a linear sorption model. The equivalent Henry’s constant, which equals the product of Langmuir capacity and affinity, is systematically higher than the literature values. Further analyses and comparison of sorption models are planned in FY2020 Q4 and the sorption model will be coupled in models of nonisothermal multiphase transport for studying noble gas detectability.

58 GEOSCIENCES↗

DOE OSTI2020

SECARB-USA: A Sub-Basin Framework for Future CO 2 Infrastructure Development

Task 4 of the SECARB-USA Project is designed to evaluate the regional needs and challenges for the development of a safe and environmentally sound CO 2 transport infrastructure. This infrastructure would transport CO 2 capture from power generating plants and/or industrial sources and distribute it to oil fields for associated storage in EOR operations, saline storage, and/or other suitable storage sites. The objective of this report on Sub-Basin Prospective Areas (Deliverable 4.1.a), is to provide the framework for understanding how regional infrastructure development could occur. The sub-basin prospective areas, in conjunction with the locations of CO 2 sources and pipeline infrastructure (for source-sink matching networks), form the basis for the analysis that will be performed in the Techno-Economic Analysis of Infrastructure Buildout Scenarios (Deliverable 4.1.b).

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2021

Autonomous Tools for Attack Surface Reduction (Final Report)

The electric power grid is a complex critical infrastructure that forms the lifeline of modern society, and its secure and reliable operation is of paramount importance to national security and economic wellbeing. However, recent findings documented in authoritative sources indicate the threat of cyber-based attacks growing in numbers and sophistication. However, securing the grid against stealthy cyberattacks is a challenging task due to legacy nature of the infrastructure coupled with dynamic nature of threat landscape and ever-growing sophistication of the adversaries. Additionally, the grid’s attack surface continues to grow with the increased dependence on digital communications and control that now extends to each consumer through smart meters and distributed energy resources. Unfortunately, this expansive surface increases the grid’s vulnerability and further exposes critical control systems in both substations and control centers. To respond to this emerging need, we had successfully assembled an interdisciplinary team with academic- industry partnership to successfully conduct research, development, evaluation, demonstration, and commercialization of attack surface reduction tools, whose goal was to significantly reduce the cyber attack surface in the North American power grid. Our proposed project was a synergistic collaborative effort leveraging the synergistic expertise of the team members across power systems, cyber security and CPS security, testbeds, field deployments and demonstration, and successful commercialization. The following are the specific tasks that have been successfully completed two phases (2016-2020). Phase I: Task 1: Developed and implemented a robust Project Management and Data Management Plan, coupled with a well thought out Risk Mitigation Plan. Task 2.1: Developed a comprehensive framework that continually assesses and autonomously reduces the attack surface for the power grid control environment spanning across substations, control center and the SCADA network to significantly reduce the risks of cyber attacks. Task 2.2: Developed attack surface analysis techniques, metrics, and tools that assess the attack surface at multiple levels including the control center, substations, and the SCADA network. Task 2.3: Developed attack surface reduction techniques and tools that dynamically reduce attack surface and hence increase attacker’s cost without interfering in the critical functions of the system. Task 2.4: Prototyped, implemented, and quantitatively evaluated/validated the techniques and tools on a realistic industrial CPS security testbed environment by leveraging the unique resources of the team. Task 3: Developed Commercialization plan to transition the developed tools into power system industry stakeholders for a broader adoption by leveraging the expertise of our industrial members. Phase II: Task 4: Successfully completed field demonstration, verification, and evaluation of the effectiveness of the attack surface analysis and reduction techniques on a realistic utility testbed environment. This also involved the development of realistic scenarios, sound metrics, data sets, evaluation criteria, and documentation. Technology integration & Field demonstration: The project had significantly advanced the state-of-the-art research and practice in improving the cybersecurity of our nation’s power grid infrastructure against cyber threats. In particular, the proposed, designed, and deployed attack surface analysis and reduction algorithms and tools have contributed to significantly reducing the exposure and risk of the devices, substations, and the integrated SCADA/EMS/ DMS grid environment to cyber threat. Strong demonstration and evaluation techniques have verified the feasibility of the developed techniques on realistic cyber-physical testbeds and utility partner's real grid environment, and collaborative research and evaluation of attack surface reduction techniques (for wide-are monitoring and control) within a vendor (GE) EMS platform. The Attack Host Analyzer (AHA) tool that was developed through this project was made available through GitHub.

24 POWER TRANSMISSION AND DISTRIBUTION↗

DOE OSTI2024

Phase Field Modeling of Near-Wellbore Hydraulic Fracture Nucleation and Propagation

The goal of Task 2 of the project titled "Closing the loop between in situ stress complexity and EGS fracture complexity" is to model fracture nucleation and propagation in the near wellbore region and, in combination with the experimental study conducted as part of Task 4, investigate the relationship between the in situ stress and the near-wellbore fracture patterns. To this end, We have identified phase field as a promising modeling approach to model the nucleation and propagation process in the near wellbore region. In phase field, fractures are represented by a diffuse variable, i.e the damage. Compared to approaches that model fractures as sharp interfaces, phase field does not require any re-meshing or element insertion algorithm, which makes the treatment of complex fracture geometries straightforward, even with simple meshes.

15 GEOTHERMAL ENERGY↗

DOE OSTI2026

Scaling Spectroradiometric Monitoring to an Algal Factory Farm

This report briefly summarizes the spectroradiometric approach adapted and deployed as part of Task 4.2 within the BETO-funded D evelopment of I ntegrated S creening, C ultivar O ptimization, and V erification R esearch (DISCOVR) project, specifically task 4, “Increase crop protection and culture stability.” The goals of this subtask were to monitor ponds cultivating a variety of DISCOVR strains at the Arizona Center for Algae Technology and Innovation (AzCATI) with spectroradiometric technology to: • Predict biomass concentrations with high temporal frequency. • Optimize automated analysis methods that enabled feedback for pond automation strategies • Identify pond crash indicators from primary (pest/predator) and indirect (change in algal host) spectroscopic signals with potential for early treatment/intervention • Provide recommendations for technology deployment at scale. This report fulfills the deliverable requirement for the final bullet “provide recommendations for technology deployment at scale”.

09 BIOMASS FUELS↗

DOE OSTI2025

District Geothermal Heating + Cooling Deployment in a CT Environmental Justice Community

The report marks the team’s completion of all required tasks and milestones. Work completed for Task 1 (Technical and Economic Feasibility Assessment & Procurement Drafting) included development of analysis and design model; completion of technical, economic, and environmental assessments; and technical outreach and coalition design. Components for Task 2 (Outreach & Community Engagement) involved broad outreach and community-engagement efforts (including stakeholder meetings and a webinar as well as development of a formal engagement plan) and development of a web page and a case study. For Task 3 (Workforce Transition, Development, & Training Plan), the team undertook a formal statewide geothermal workforce needs assessment, developed corresponding recommendations for both the state as a whole and the Wallingford project, and held several workshops. For Task 4 (Project Management & Data Sharing), the team drafted a data-sharing plan.

15 GEOTHERMAL ENERGY↗

NASA NTRS1982

Creep-fatigue life prediction for engine hot section materials (isotropic)

The objectives of this program are the investigation of fundamental approaches to high temperature crack initiation life prediction, identification of specific modeling strategies and the development of specific models for component relevant loading conditions. A survey of the hot section material/coating systems used throughout the gas turbine industry is included. Two material/coating systems will be identified for the program. The material/coating system designated as the base system shall be used throughout Tasks 1-12. The alternate material/coating system will be used only in Task 12 for further evaluation of the models developed on the base material. In Task II, candidate life prediction approaches will be screened based on a set of criteria that includes experience of the approaches within the literature, correlation with isothermal data generated on the base material, and judgements relative to the applicability of the approach for the complex cycles to be considered in the option program. The two most promising approaches will be identified. Task 3 further evaluates the best approach using additional base material fatigue testing including verification tests. Task 4 consists of technical, schedular, financial and all other reporting requirements in accordance with the Reports of Work clause.

Moreno, V.↗

NASA NTRS1987

Crew interface with a telerobotic control station

A method for apportioning crew-telerobot tasks has been derived to facilitate the design of a crew-friendly telerobot control station. To identify the most appropriate state-of-the-art hardware for the control station, task apportionment must first be conducted to identify if an astronaut or a telerobot is best to execute the task and which displays and controls are required for monitoring and performance. Basic steps that comprise the task analysis process are: (1) identify space station tasks; (2) define tasks; (3) define task performance criteria and perform task apportionment; (4) verify task apportionment; (5) generate control station requirements; (6) develop design concepts to meet requirements; and (7) test and verify design concepts.

Mok, Eva↗

NASA NTRS1989

Space station Simulation Computer System (SCS) study for NASA/MSFC. Volume 5: Study analysis report

The Simulation Computer System (SCS) is the computer hardware, software, and workstations that will support the Payload Training Complex (PTC) at the Marshall Space Flight Center (MSFC). The PTC will train the space station payload scientists, station scientists, and ground controllers to operate the wide variety of experiments that will be on-board the Freedom Space Station. The further analysis performed on the SCS study as part of task 2-Perform Studies and Parametric Analysis-of the SCS study contract is summarized. These analyses were performed to resolve open issues remaining after the completion of task 1, and the publishing of the SCS study issues report. The results of these studies provide inputs into SCS task 3-Develop and present SCS requirements, and SCS task 4-develop SCS conceptual designs. The purpose of these studies is to resolve the issues into usable requirements given the best available information at the time of the study. A list of all the SCS study issues is given.

Source record↗

NASA NTRS1990

Characterization of space station multilayer insulation damage due to hypervelocity space debris impact

Four main tasks were accomplished. The first three tasks were related to the goal of measuring the degradation of the insulating capabilities of Space Station multilayer insulation (MLI) due to simulated space debris impacts at hypervelocities. The last task was associated with critically reviewing a Boeing document on the fracture characteristics of the Space Station pressure wall when subjected to a simulated hypervelocity space debris impact. In Task 1, a thermal test procedure for impact damaged MLI specimens was written. In Task 2, damaged MLI specimens were prepared. In Task 3, a computer program was written to simulate MLI thermal tests. In Task 4, the author reviewed a Boeing document describing hypervelocity impact testing on biaxially stressed plates.

Rule, William Keith↗

NASA NTRS1993

An efficient liner cooling scheme for advanced small gas turbine combustors

A joint Army/NASA program was conducted to design, fabricate, and test an advanced, small gas turbine, reverse-flow combustor utilizing a compliant metal/ceramic (CMC) wall cooling concept. The objectives of this effort were to develop a design method (basic design data base and analysis) for the CMC cooling technique and then demonstrate its application to an advanced cycle, small, reverse-flow combustor with 3000 F burner outlet temperature. The CMC concept offers significant improvements in wall cooling effectiveness resulting in a large reduction in cooling air requirements. Therefore, more air is available for control of burner outlet temperature pattern in addition to the benefits of improved efficiency, reduced emissions, and lower smoke levels. The program was divided into four tasks. Task 1 defined component materials and localized design of the composite wall structure in conjunction with development of basic design models for the analysis of flow and heat transfer through the wall. Task 2 included implementation of the selected materials and validated design models during combustor preliminary design. Detail design of the selected combustor concept and its refinement with 3D aerothermal analysis were completed in Task 3. Task 4 covered detail drawings, process development and fabrication, and a series of burner rig tests. The purpose of this paper is to provide details of the investigation into the fundamental flow and heat transfer characteristics of the CMC wall structure as well as implementation of the fundamental analysis method for full-scale combustor design.

Paskin, Marc D.↗

NASA NTRS1994

Rocketdyne Safety Algorithm: Space Shuttle Main Engine Fault Detection

The Rocketdyne Safety Algorithm (RSA) has been developed to the point of use on the TTBE at MSFC on Task 4 of LeRC contract NAS3-25884. This document contains a description of the work performed, the results of the nominal test of the major anomaly test cases and a table of the resulting cutoff times, a plot of the RSA value vs. time for each anomaly case, a logic flow description of the algorithm, the algorithm code, and a development plan for future efforts.

Norman, Arnold M., Jr.↗

NASA NTRS2009

Lunar Surface Operations: Surface Duration - Part 2

The objectives of this slide presentation are to review the activities on the lunar surface during the stay. The objectives include (1) Summarize Lunar Module Basics emphasizing module layout and storage. (2) Identify the primary activities occurring during each of the lunar s urface timelines, (3) List the EVA Prep tasks, (4) Identify the EVA Objectives, (5) Identify the activities associated with Post EVA (6) Describe the lessons learned during both EVA and Non EVA activities. Included are overview drawings of the Lunar Roving Vehicle, pictures of the tools, and sample return containers. There are also time lines for the Apollo 11, and Apollo 12 through 14, Apollo 15, Apollo 16 and Apollo 17. Diagrams of the EVA suits are shown, including the Liquid Cooling Garment, and the Pressure Garment Assembly. The activity prior to the EVA are reviewed. The science mission assignments of each mission are viewed. The activities after the EVA are reviewed

Interbartolo, Michael↗

DOE OSTI2022

Effect of Catalyst Pretreatment on Methane Conversion under Microwave-assisted and Conventional Thermal Methods

The presentation was delivered from work performed in NETL's Upcycling of Associated Natural Gas FWP Task 4 Benzene, Toluene, Xylene Synthesis via Microwave-assisted catalyst. The objective of this project is to develop a modular, microwave-assisted reactor to upcycle flare gas into valuable chemicals. The presentation discusses important work researchers have performed to compare the pre-treatment of a benchmark Mo/ZSM-5 catalyst under microwaves to traditional thermal heating. Pre-treatment is required to enable to catalyst to produce benzene. This study provided insights into how the exposure impacts the structure and activity of the catalyst and will be used to help design better catalysts.

Abdelsayed, Victor↗

DOE OSTI2023

Machine Learning Based Fracture Network Quantification at the IBDP CO2 Sequestration Site

This poster presents the latest results highlighted in SMART phase II task 4 of fracture network and mapping based on IBDP field data measurement. The results will be coupled into the dynamic modeling and simulation study to insight the impact of the fracture in the reservoir system. Such impacts will be applied to AI/ML development for training and test for science-informed decision making support for CO2 storage.

Kumar, Abhash↗